Effects on the structure and electrochemical reactivity of surface modified magnesium cobalt oxide

[Display omitted] •A thin film of conducting polyaniline layer is formed on the surface of MgCoO2.•The PANI@MgCoO2 composites are used in hybrid Na/Mg batteries.•This coating facilitates the Mg2+/Na+ transportation and enhances electron transfer.•A single-phase insertion reaction is found and preser...

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Published inJournal of electroanalytical chemistry (Lausanne, Switzerland) Vol. 971; p. 118561
Main Authors Missaoui, Kahla, Ferchichi, Karima, Amdouni, Noureddine, Cosano, Daniel, Liu, Rui, Pan, Siyuan, Zhanning, He, Su, Yu, Luo, Mingzeng, Yang, Yong, Ortiz, Gregorio F.
Format Journal Article
LanguageEnglish
Published Elsevier B.V 15.10.2024
Subjects
Composite materials
Conductive Polymer
Hybrid battery
MgCoO2
Pickering emulsion
Hybrid battery
Conductive Polymer
MgCoO2
Pickering emulsion
Composite materials
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Abstract [Display omitted] •A thin film of conducting polyaniline layer is formed on the surface of MgCoO2.•The PANI@MgCoO2 composites are used in hybrid Na/Mg batteries.•This coating facilitates the Mg2+/Na+ transportation and enhances electron transfer.•A single-phase insertion reaction is found and preserved original cubic phase. Polyaniline coated magnesium cobalt oxide nanocomposites (PANI@MgCoO2) are synthesized by a cost-effective method. The structural, chemical, morphological, thermal and surface characterizations (X-ray diffraction, electron microscopy, thermogravimetry, Raman and X-ray photoelectron spectroscopies) confirm the presence of a thin layer of conducting polymer (∼40 nm) in which the benzenoid and quinoid (C6H4) rings are surrounded by imine (=N-) and amine (–NH-) nitrogen on the particles of the cubic oxide. Their electrochemical reactions are studied in magnesium cells using the dual combination of sodium and magnesium ions in the electrolyte. A strong interaction at the interface of PANI and MgCoO2 improved the electrochemical properties and revealed a single-phase insertion/extraction reaction mechanism into/from the cubic structure. These PANI@MgCoO2 nanocomposites exhibited enhanced reversible capacity (103.4 – 153mAhg−1) at ∼ 1 V vs. Mg2+/Mg, Warburg (26.5 Ω s−1/2) and diffusion (6.92·10-14 cm2 s−1) coefficients as compared to pristine material. These results show that the proposed coating can be used for electrodes in the field of rechargeable magnesium hybrid batteries (MHRBs).
AbstractList [Display omitted] •A thin film of conducting polyaniline layer is formed on the surface of MgCoO2.•The PANI@MgCoO2 composites are used in hybrid Na/Mg batteries.•This coating facilitates the Mg2+/Na+ transportation and enhances electron transfer.•A single-phase insertion reaction is found and preserved original cubic phase. Polyaniline coated magnesium cobalt oxide nanocomposites (PANI@MgCoO2) are synthesized by a cost-effective method. The structural, chemical, morphological, thermal and surface characterizations (X-ray diffraction, electron microscopy, thermogravimetry, Raman and X-ray photoelectron spectroscopies) confirm the presence of a thin layer of conducting polymer (∼40 nm) in which the benzenoid and quinoid (C6H4) rings are surrounded by imine (=N-) and amine (–NH-) nitrogen on the particles of the cubic oxide. Their electrochemical reactions are studied in magnesium cells using the dual combination of sodium and magnesium ions in the electrolyte. A strong interaction at the interface of PANI and MgCoO2 improved the electrochemical properties and revealed a single-phase insertion/extraction reaction mechanism into/from the cubic structure. These PANI@MgCoO2 nanocomposites exhibited enhanced reversible capacity (103.4 – 153mAhg−1) at ∼ 1 V vs. Mg2+/Mg, Warburg (26.5 Ω s−1/2) and diffusion (6.92·10-14 cm2 s−1) coefficients as compared to pristine material. These results show that the proposed coating can be used for electrodes in the field of rechargeable magnesium hybrid batteries (MHRBs).
ArticleNumber 118561
Author Liu, Rui
Pan, Siyuan
Ortiz, Gregorio F.
Ferchichi, Karima
Cosano, Daniel
Su, Yu
Amdouni, Noureddine
Missaoui, Kahla
Zhanning, He
Luo, Mingzeng
Yang, Yong
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  givenname: He
  surname: Zhanning
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  givenname: Yu
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  givenname: Yong
  surname: Yang
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  givenname: Gregorio F.
  surname: Ortiz
  fullname: Ortiz, Gregorio F.
  email: gregorio.ortiz@hqu.edu.cn
  organization: Xiamen Key Laboratory of Optoelectronic Materials and Advanced Manufacturing, Institute of Luminescent Materials and Information Displays, College of Materials Science and Engineering, Huaqiao University, Xiamen 361021, China
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  doi: 10.1002/cphc.200500619
  contributor:
    fullname: Chadwick
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Snippet [Display omitted] •A thin film of conducting polyaniline layer is formed on the surface of MgCoO2.•The PANI@MgCoO2 composites are used in hybrid Na/Mg...
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elsevier
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StartPage 118561
SubjectTerms Composite materials
Conductive Polymer
Hybrid battery
MgCoO2
Pickering emulsion
Title Effects on the structure and electrochemical reactivity of surface modified magnesium cobalt oxide
URI https://dx.doi.org/10.1016/j.jelechem.2024.118561
Volume 971
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