Low friction characteristics and tribochemistry analysis of novel AlTiN/a-C based nanocomposite coatings
[Display omitted] •Newly developed compositionally graded AlTiN/a-C nanocomposite coatings using magnetron sputtering.•Evaluation of tribological properties were carried out under room temperature and 673 K.•Enhanced tribological performance were observed for compositionally graded coatings because...
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Published in | Applied surface science Vol. 678; p. 161137 |
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Main Authors | , , , , , , |
Format | Journal Article |
Language | English |
Published |
Elsevier B.V
30.12.2024
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Abstract | [Display omitted]
•Newly developed compositionally graded AlTiN/a-C nanocomposite coatings using magnetron sputtering.•Evaluation of tribological properties were carried out under room temperature and 673 K.•Enhanced tribological performance were observed for compositionally graded coatings because of its refined microstructure.•Tribochemistry analysis of wear surfaces of all the coatings were carried out using XPS.
Friction reduction of AlTiN-based hard coatings is gaining much attention among researchers worldwide to broaden their tribological applications. Metal/non-metal inclusions, as well as the design of a novel coating architecture, are primarily focused on reducing friction while retaining wear resistance. This study investigates the tribological characteristics of magnetron sputtered AlTiN coatings by incorporating amorphous carbon (a–C) at different concentrations (5–25 at.%), as well as the compositionally graded AlTiN/a-C coatings (CGC). The XPS and Raman spectroscopy results confirm the presence of a-C features, while XRD reveals the formation of ceramic carbide phases in AlTiN coatings with higher carbon content and CGC coatings. The CGC AlTiN/a-C have shown a maximum hardness of 34.3 GPa and an elastic modulus of 321 GPa due to their refined grain structure. The CGC had the lowest friction (0.18 at 300 K and 0.37 at 673 K), as well as improved wear resistance (2.74 × 10−7 mm3/Nm (300 K) and 4.93 × 10−7 mm3/Nm (673 K)). The tribolayers are found to be mainly composed of sp2/sp3 bonded a-C features (including C=C/C─C, C─N, and C─O), which reduces the friction force significantly. The CGC AlTiN/a-C coating has exhibited improved wear resistance behavior due to their finely grained structure and improved mechanical properties. |
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AbstractList | [Display omitted]
•Newly developed compositionally graded AlTiN/a-C nanocomposite coatings using magnetron sputtering.•Evaluation of tribological properties were carried out under room temperature and 673 K.•Enhanced tribological performance were observed for compositionally graded coatings because of its refined microstructure.•Tribochemistry analysis of wear surfaces of all the coatings were carried out using XPS.
Friction reduction of AlTiN-based hard coatings is gaining much attention among researchers worldwide to broaden their tribological applications. Metal/non-metal inclusions, as well as the design of a novel coating architecture, are primarily focused on reducing friction while retaining wear resistance. This study investigates the tribological characteristics of magnetron sputtered AlTiN coatings by incorporating amorphous carbon (a–C) at different concentrations (5–25 at.%), as well as the compositionally graded AlTiN/a-C coatings (CGC). The XPS and Raman spectroscopy results confirm the presence of a-C features, while XRD reveals the formation of ceramic carbide phases in AlTiN coatings with higher carbon content and CGC coatings. The CGC AlTiN/a-C have shown a maximum hardness of 34.3 GPa and an elastic modulus of 321 GPa due to their refined grain structure. The CGC had the lowest friction (0.18 at 300 K and 0.37 at 673 K), as well as improved wear resistance (2.74 × 10−7 mm3/Nm (300 K) and 4.93 × 10−7 mm3/Nm (673 K)). The tribolayers are found to be mainly composed of sp2/sp3 bonded a-C features (including C=C/C─C, C─N, and C─O), which reduces the friction force significantly. The CGC AlTiN/a-C coating has exhibited improved wear resistance behavior due to their finely grained structure and improved mechanical properties. |
ArticleNumber | 161137 |
Author | Panda, Kalpataru Kirubaharan, Kamalan Arivarasan, A. Dinesh Kumar, D. Duesberg, Georg S. Kuppusami, P. Stimpel-Lindner, Tanja |
Author_xml | – sequence: 1 givenname: D. surname: Dinesh Kumar fullname: Dinesh Kumar, D. email: ddinesh.tribology@gmail.com organization: Centre for Nanoscience and Nanotechnology, Sathyabama Institute of Science and Technology, Chennai 600119, Tamil Nadu, India – sequence: 2 givenname: Kamalan surname: Kirubaharan fullname: Kirubaharan, Kamalan organization: Coating Department, FunGlass, Centre for Functional and Surface Functionalized Glass, Alexander Dubcek University of Trencin, 91150 Trencin, Slovakia – sequence: 3 givenname: Kalpataru orcidid: 0000-0003-3196-5529 surname: Panda fullname: Panda, Kalpataru organization: Department of Physics, Manipal Institute of Technology, Manipal Academy of Higher Education, Manipal, Karnataka 576104, India – sequence: 4 givenname: P. surname: Kuppusami fullname: Kuppusami, P. organization: Centre for Nanoscience and Nanotechnology, Sathyabama Institute of Science and Technology, Chennai 600119, Tamil Nadu, India – sequence: 5 givenname: A. surname: Arivarasan fullname: Arivarasan, A. organization: Department of Physics, School of Advanced Sciences, Kalasalingam Academy of Research and Education, Krishnankoil 626126, Virudhunagar, Tamil Nadu, India – sequence: 6 givenname: Tanja orcidid: 0000-0002-4864-4898 surname: Stimpel-Lindner fullname: Stimpel-Lindner, Tanja organization: Institute of Physics, Faculty of Electrical Engineering and Information Technology and SENS Research Centre, University of the Bundeswehr Munich, 85577 Neubiberg, Germany – sequence: 7 givenname: Georg S. orcidid: 0000-0002-7412-700X surname: Duesberg fullname: Duesberg, Georg S. organization: Institute of Physics, Faculty of Electrical Engineering and Information Technology and SENS Research Centre, University of the Bundeswehr Munich, 85577 Neubiberg, Germany |
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Keywords | Graded coatings Tribochemistry Low friction Wear resistance sp2/sp3 carbons a-C |
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Spectrosc. doi: 10.1016/j.saa.2014.05.045 contributor: fullname: Lubas |
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•Newly developed compositionally graded AlTiN/a-C nanocomposite coatings using magnetron sputtering.•Evaluation of tribological properties... |
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SubjectTerms | a-C Graded coatings Low friction sp2/sp3 carbons Tribochemistry Wear resistance |
Title | Low friction characteristics and tribochemistry analysis of novel AlTiN/a-C based nanocomposite coatings |
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