Self-assembled three-dimensional NaY(WO4)2:Ln3+ architectures: Hydrothermal synthesis, growth mechanism and luminescence properties

Self-assembled 3D NaY(WO4)2:Ln3+ hierarchical microstructures with multicolor DC and UC luminescence were synthesized through a hydrothermal process and followed by a subsequent heat treatment process. [Display omitted] ► Novel self-assembled 3D NaY(WO4)2:Ln are prepared by a chemical conversion met...

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Published inJournal of alloys and compounds Vol. 529; pp. 140 - 147
Main Authors Huang, Shaohua, Wang, Dong, Wang, Yan, Wang, Liuzhen, Zhang, Xiao, Yang, Piaoping
Format Journal Article
LanguageEnglish
Published Kidlington Elsevier B.V 15.07.2012
Elsevier
Subjects
Chemical synthesis methods
Condensed matter: electronic structure, electrical, magnetic, and optical properties
Cross-disciplinary physics: materials science; rheology
Exact sciences and technology
Hydrothermal
Materials science
Methods of nanofabrication
Nanocrystals and nanoparticles
NaY(WO4)2
Optical properties and condensed-matter spectroscopy and other interactions of matter with particles and radiation
Optical properties of low-dimensional, mesoscopic, and nanoscale materials and structures
Physics
Three-dimensional
Up-conversion
Three-dimensional
NaY(WO4)2
Hydrothermal
Up-conversion
Particle size
NaY(WO
Sodium Yttrium Tungstates Mixed
Doping
Photoluminescence
Frequency conversion
)
Self-assembled layers
XRD
Heat treatments
Nanoparticles
Template method
Energy-level transitions
Hydrothermal synthesis
Growth mechanism
Rare earth additions
Chromaticity
Microstructure
Nanomaterial synthesis
Online AccessGet full text

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Abstract Self-assembled 3D NaY(WO4)2:Ln3+ hierarchical microstructures with multicolor DC and UC luminescence were synthesized through a hydrothermal process and followed by a subsequent heat treatment process. [Display omitted] ► Novel self-assembled 3D NaY(WO4)2:Ln are prepared by a chemical conversion method without using any surfactant or catalyst. ► Under UV excitation, the precursor of NaY(WO4)2:Eu3+ exhibits interesting white light emission. ► The as-annealed NaY(WO4)2:Ln3+ architectures exhibit multicolor DC and UC luminescences. ► The possible formation mechanism is well investigated. Novel three-dimensional (3D) flower-like NaY(WO4)2:Ln3+ (Ln=Eu, Yb/Er, Yb/Tm and Yb/Ho) microstructures with uniform shape and dimension have been prepared using Y(OH)CO3 nanospheres as sacrificial template through a hydrothermal process and followed by a subsequent heat treatment process. The whole process was carried out in aqueous condition without using any organic solvents, surfactant, or catalyst. The phase, morphology, size, and photoluminescence (PL) properties were well characterized by means of X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and high-resolution transmission electron microscopy (HRTEM), photoluminescence (PL) spectra, and kinetic decays, respectively. The results reveal that the as-prepared precursor of NaY(WO4)2:Eu3+ exhibits interesting white light emission under UV excitation. After annealing, the as-obtained 3D flower-like NaY(WO4)2:Eu3+ microstructures show exclusively red (Eu3+, 5D0→7F2) luminescence. Furthermore, the up-conversion (UC) luminescent properties and the emission mechanisms of NaY(WO4)2:Yb3+/Ln3+ (Ln=Er, Tm, Ho) microstructures have been systematically studied, which show respective green (Er3+, 4S3/2, 2H11/2→4I15/2), blue (Tm3+, 1G4→3H6) and yellow-green (Ho3+, 5S2→5I8) luminescence under 980nm NIR excitation.
AbstractList Self-assembled 3D NaY(WO4)2:Ln3+ hierarchical microstructures with multicolor DC and UC luminescence were synthesized through a hydrothermal process and followed by a subsequent heat treatment process. [Display omitted] ► Novel self-assembled 3D NaY(WO4)2:Ln are prepared by a chemical conversion method without using any surfactant or catalyst. ► Under UV excitation, the precursor of NaY(WO4)2:Eu3+ exhibits interesting white light emission. ► The as-annealed NaY(WO4)2:Ln3+ architectures exhibit multicolor DC and UC luminescences. ► The possible formation mechanism is well investigated. Novel three-dimensional (3D) flower-like NaY(WO4)2:Ln3+ (Ln=Eu, Yb/Er, Yb/Tm and Yb/Ho) microstructures with uniform shape and dimension have been prepared using Y(OH)CO3 nanospheres as sacrificial template through a hydrothermal process and followed by a subsequent heat treatment process. The whole process was carried out in aqueous condition without using any organic solvents, surfactant, or catalyst. The phase, morphology, size, and photoluminescence (PL) properties were well characterized by means of X-ray diffraction (XRD), scanning electron microscopy (SEM), transmission electron microscopy (TEM), and high-resolution transmission electron microscopy (HRTEM), photoluminescence (PL) spectra, and kinetic decays, respectively. The results reveal that the as-prepared precursor of NaY(WO4)2:Eu3+ exhibits interesting white light emission under UV excitation. After annealing, the as-obtained 3D flower-like NaY(WO4)2:Eu3+ microstructures show exclusively red (Eu3+, 5D0→7F2) luminescence. Furthermore, the up-conversion (UC) luminescent properties and the emission mechanisms of NaY(WO4)2:Yb3+/Ln3+ (Ln=Er, Tm, Ho) microstructures have been systematically studied, which show respective green (Er3+, 4S3/2, 2H11/2→4I15/2), blue (Tm3+, 1G4→3H6) and yellow-green (Ho3+, 5S2→5I8) luminescence under 980nm NIR excitation.
Author Zhang, Xiao
Wang, Liuzhen
Huang, Shaohua
Wang, Dong
Yang, Piaoping
Wang, Yan
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  email: yangpiaoping@hrbeu.edu.cn, piaoping@ciac.jl.cn
  organization: Key Laboratory of Superlight Materials and Surface Technology, Ministry of Education, Harbin Engineering University, Harbin 150001, PR China
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Keywords Three-dimensional
NaY(WO4)2
Hydrothermal
Up-conversion
Particle size
NaY(WO
Sodium Yttrium Tungstates Mixed
Doping
Photoluminescence
Frequency conversion
)
Self-assembled layers
XRD
Heat treatments
Nanoparticles
Template method
Energy-level transitions
Hydrothermal synthesis
Growth mechanism
Rare earth additions
Chromaticity
Microstructure
Nanomaterial synthesis
Language English
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Snippet Self-assembled 3D NaY(WO4)2:Ln3+ hierarchical microstructures with multicolor DC and UC luminescence were synthesized through a hydrothermal process and...
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elsevier
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StartPage 140
SubjectTerms Chemical synthesis methods
Condensed matter: electronic structure, electrical, magnetic, and optical properties
Cross-disciplinary physics: materials science; rheology
Exact sciences and technology
Hydrothermal
Materials science
Methods of nanofabrication
Nanocrystals and nanoparticles
NaY(WO4)2
Optical properties and condensed-matter spectroscopy and other interactions of matter with particles and radiation
Optical properties of low-dimensional, mesoscopic, and nanoscale materials and structures
Physics
Three-dimensional
Up-conversion
Title Self-assembled three-dimensional NaY(WO4)2:Ln3+ architectures: Hydrothermal synthesis, growth mechanism and luminescence properties
URI https://dx.doi.org/10.1016/j.jallcom.2012.02.156
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