Corrosion Inhibition of AZ31-xLi (x = 4, 8, 12) magnesium alloys in sodium chloride solutions by aqueous molybdate

Corrosion of lithium-containing AZ31 magnesium alloys AZ31-xLi (x = 4, 8, and 12 wt%) has been examined in 0.05 M NaCl solution with and without 10–150 mM of Na2MoO4 inhibitor. Potentiodynamic polarization, electrochemical impedance spectroscopy (EIS), and dynamic electrochemical impedance spectrosc...

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Published inCorrosion science Vol. 241; p. 112513
Main Authors Osipenko, Maria A., Paspelau, Andrei V., Kasach, Aliaksandr A., Ryl, Jacek, Skowron, Konrad, Adamiec, Janusz, Kurilo, Irina I., Kharytonau, Dzmitry S.
Format Journal Article
LanguageEnglish
Published Elsevier Ltd 01.12.2024
Subjects
Corrosion mechanism
Dynamic electrochemical impedance spectroscopy
Inhibitor efficiency
Magnesium-lithium alloy
Molybdate inhibitor
Dynamic electrochemical impedance spectroscopy
Corrosion mechanism
Inhibitor efficiency
Molybdate inhibitor
Magnesium-lithium alloy
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Abstract Corrosion of lithium-containing AZ31 magnesium alloys AZ31-xLi (x = 4, 8, and 12 wt%) has been examined in 0.05 M NaCl solution with and without 10–150 mM of Na2MoO4 inhibitor. Potentiodynamic polarization, electrochemical impedance spectroscopy (EIS), and dynamic electrochemical impedance spectroscopy (DEIS) measurements were used to correlate the phase composition and microstructure of the alloys with their corrosion propensity and effectiveness of the molybdate inhibitor, giving high inhibition efficiency (>85%) at concentrations higher than ca. 35 mM. Post-corrosion microstructure, Raman, and X-ray photoelectron spectroscopy analyses allowed to provide the inhibition mechanism of AZ31-xLi alloys by molybdate ions. [Display omitted] •Effectiveness of molybdate inhibitor towards AZ31-xLi (x = 4, 8, and 12 wt%) Mg alloys has been examined.•Dynamic multisine impedance spectroscopy was utilized to examine corrosion and inhibition mechanisms.•Corrosion rate of AZ31-xLi alloys and the inhibition effect of molybdate strongly depend on the amount of Li in the alloys.•A mechanism of corrosion inhibition of AZ31-xLi (x = 4, 8, and 12 wt%) Mg alloys by molybdate has been proposed.
AbstractList Corrosion of lithium-containing AZ31 magnesium alloys AZ31-xLi (x = 4, 8, and 12 wt%) has been examined in 0.05 M NaCl solution with and without 10–150 mM of Na2MoO4 inhibitor. Potentiodynamic polarization, electrochemical impedance spectroscopy (EIS), and dynamic electrochemical impedance spectroscopy (DEIS) measurements were used to correlate the phase composition and microstructure of the alloys with their corrosion propensity and effectiveness of the molybdate inhibitor, giving high inhibition efficiency (>85%) at concentrations higher than ca. 35 mM. Post-corrosion microstructure, Raman, and X-ray photoelectron spectroscopy analyses allowed to provide the inhibition mechanism of AZ31-xLi alloys by molybdate ions. [Display omitted] •Effectiveness of molybdate inhibitor towards AZ31-xLi (x = 4, 8, and 12 wt%) Mg alloys has been examined.•Dynamic multisine impedance spectroscopy was utilized to examine corrosion and inhibition mechanisms.•Corrosion rate of AZ31-xLi alloys and the inhibition effect of molybdate strongly depend on the amount of Li in the alloys.•A mechanism of corrosion inhibition of AZ31-xLi (x = 4, 8, and 12 wt%) Mg alloys by molybdate has been proposed.
ArticleNumber 112513
Author Ryl, Jacek
Skowron, Konrad
Adamiec, Janusz
Kurilo, Irina I.
Kharytonau, Dzmitry S.
Osipenko, Maria A.
Paspelau, Andrei V.
Kasach, Aliaksandr A.
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  organization: Department of Physical, Colloid, and Analytical Chemistry, Belarusian State Technological University, Minsk 220006, Belarus
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  givenname: Andrei V.
  surname: Paspelau
  fullname: Paspelau, Andrei V.
  organization: Department of Physical, Colloid, and Analytical Chemistry, Belarusian State Technological University, Minsk 220006, Belarus
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  givenname: Aliaksandr A.
  surname: Kasach
  fullname: Kasach, Aliaksandr A.
  organization: Department of Chemistry, Electrochemical Production Technology, and Materials for Electronic Equipment, Belarusian State Technological University, Minsk 220006, Belarus
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  givenname: Jacek
  surname: Ryl
  fullname: Ryl, Jacek
  email: jacek.ryl@pg.edu.pl
  organization: Advanced Materials Center and Institute of Nanotechnology and Materials Engineering, Gdańsk University of Technology, Gdańsk 80-233, Poland
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  givenname: Konrad
  orcidid: 0000-0003-1933-5452
  surname: Skowron
  fullname: Skowron, Konrad
  organization: Electrochemistry and Corrosion Laboratory, Jerzy Haber Institute of Catalysis and Surface Chemistry, Polish Academy of Sciences, Krakow 30-239, Poland
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  givenname: Janusz
  orcidid: 0000-0002-9135-6138
  surname: Adamiec
  fullname: Adamiec, Janusz
  organization: Institute of Materials Science, Silesian University of Technology, Katowice 40-019, Poland
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  givenname: Irina I.
  surname: Kurilo
  fullname: Kurilo, Irina I.
  organization: Department of Physical, Colloid, and Analytical Chemistry, Belarusian State Technological University, Minsk 220006, Belarus
– sequence: 8
  givenname: Dzmitry S.
  surname: Kharytonau
  fullname: Kharytonau, Dzmitry S.
  email: dmitry.kharitonov@ikifp.edu.pl
  organization: Electrochemistry and Corrosion Laboratory, Jerzy Haber Institute of Catalysis and Surface Chemistry, Polish Academy of Sciences, Krakow 30-239, Poland
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Keywords Dynamic electrochemical impedance spectroscopy
Corrosion mechanism
Inhibitor efficiency
Molybdate inhibitor
Magnesium-lithium alloy
Language English
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Snippet Corrosion of lithium-containing AZ31 magnesium alloys AZ31-xLi (x = 4, 8, and 12 wt%) has been examined in 0.05 M NaCl solution with and without 10–150 mM of...
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SubjectTerms Corrosion mechanism
Dynamic electrochemical impedance spectroscopy
Inhibitor efficiency
Magnesium-lithium alloy
Molybdate inhibitor
Title Corrosion Inhibition of AZ31-xLi (x = 4, 8, 12) magnesium alloys in sodium chloride solutions by aqueous molybdate
URI https://dx.doi.org/10.1016/j.corsci.2024.112513
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