Catalytic fixation of hydrogen sulfide over CuO-CaCO3 co-impregnated tea stalk-derived biochar

Effective treatment of hydrogen sulfide (H2S) is crucial for minimizing nuisance odors from intensive livestock and poultry operations. The development of high-performance desulfurizers holds practical significance in this context. Herein, a novel CuO-CaCO3 co-impregnated biochar desulfurizer (CuxCa...

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Published inJournal of environmental chemical engineering Vol. 12; no. 5; p. 113320
Main Authors Lin, Fangcong, Wang, Leiping, Dai, Xiaorong, Man, Zun, Meng, Yang, Chu, Dongtao, Yang, Yuting, Wang, Wei, Xiao, Hang, Wang, Kaiying
Format Journal Article
LanguageEnglish
Published Elsevier Ltd 01.10.2024
Subjects
Adsorption
Biochar
Catalytic oxidation
CuO-CaCO3 co-impregnated
H2S
H2S
CuO-CaCO3 co-impregnated
Catalytic oxidation
Adsorption
Biochar
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Abstract Effective treatment of hydrogen sulfide (H2S) is crucial for minimizing nuisance odors from intensive livestock and poultry operations. The development of high-performance desulfurizers holds practical significance in this context. Herein, a novel CuO-CaCO3 co-impregnated biochar desulfurizer (CuxCay/BCT) was synthesized by impregnation-pyrolysis method, using waste tea stalks and metal salts as raw materials, and it is intended for the treatment of H2S at room temperature. The optimized Cu0.75Ca0.25/BC800 shows an excellent H2S removal capacity of 182.67 mg/g, which is 31 times and 5.6 times that of inactivated biochar (BC800) and copper-oxide-impregnated biochar (Cu0.75/BC800). The desulfurization mechanism of Cu0.75Ca0.25/BC800 involves synergistic effect of reactive adsorption and catalytic oxidation. CaCO3’s alkaline adsorption sites and copper-mediated activation of superoxide radicals (∙O2-) were critical in this reaction. Besides, Cu0.75Ca0.25/BC800 demonstrated excellent reusability, retaining approximately 85 % of its initial H2S removal capacity after seven cycles of desulfurization and regeneration. This study aims to develop a metal oxide- and carbonate-impregnated biochar-based desulfurizer, with the goal of advancing the technology for catalytic removal of H2S in a more environmentally friendly and effective manner. [Display omitted] •Desulfurizer (CuxCay/BCT) was prepared successfully from waste tea stalks and metal salts.•Cu0.75Ca0.25/BC800 exhibits good desulfurization and reusability properties.•Co-impregnation with CaCO3 increased the alkaline sites on the surface of the desulfurizer.•The co-impregnating of CuO activates the superoxide ion (∙O2-), which promotes the oxidation of H2S.•The desulphurization process includes reactive adsorption and catalytic oxidation.
AbstractList Effective treatment of hydrogen sulfide (H2S) is crucial for minimizing nuisance odors from intensive livestock and poultry operations. The development of high-performance desulfurizers holds practical significance in this context. Herein, a novel CuO-CaCO3 co-impregnated biochar desulfurizer (CuxCay/BCT) was synthesized by impregnation-pyrolysis method, using waste tea stalks and metal salts as raw materials, and it is intended for the treatment of H2S at room temperature. The optimized Cu0.75Ca0.25/BC800 shows an excellent H2S removal capacity of 182.67 mg/g, which is 31 times and 5.6 times that of inactivated biochar (BC800) and copper-oxide-impregnated biochar (Cu0.75/BC800). The desulfurization mechanism of Cu0.75Ca0.25/BC800 involves synergistic effect of reactive adsorption and catalytic oxidation. CaCO3’s alkaline adsorption sites and copper-mediated activation of superoxide radicals (∙O2-) were critical in this reaction. Besides, Cu0.75Ca0.25/BC800 demonstrated excellent reusability, retaining approximately 85 % of its initial H2S removal capacity after seven cycles of desulfurization and regeneration. This study aims to develop a metal oxide- and carbonate-impregnated biochar-based desulfurizer, with the goal of advancing the technology for catalytic removal of H2S in a more environmentally friendly and effective manner. [Display omitted] •Desulfurizer (CuxCay/BCT) was prepared successfully from waste tea stalks and metal salts.•Cu0.75Ca0.25/BC800 exhibits good desulfurization and reusability properties.•Co-impregnation with CaCO3 increased the alkaline sites on the surface of the desulfurizer.•The co-impregnating of CuO activates the superoxide ion (∙O2-), which promotes the oxidation of H2S.•The desulphurization process includes reactive adsorption and catalytic oxidation.
ArticleNumber 113320
Author Dai, Xiaorong
Man, Zun
Wang, Wei
Xiao, Hang
Meng, Yang
Chu, Dongtao
Wang, Leiping
Lin, Fangcong
Yang, Yuting
Wang, Kaiying
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CuO-CaCO3 co-impregnated
Catalytic oxidation
Adsorption
Biochar
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Snippet Effective treatment of hydrogen sulfide (H2S) is crucial for minimizing nuisance odors from intensive livestock and poultry operations. The development of...
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elsevier
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Publisher
StartPage 113320
SubjectTerms Adsorption
Biochar
Catalytic oxidation
CuO-CaCO3 co-impregnated
H2S
Title Catalytic fixation of hydrogen sulfide over CuO-CaCO3 co-impregnated tea stalk-derived biochar
URI https://dx.doi.org/10.1016/j.jece.2024.113320
Volume 12
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