Study on performance of Ag-modified layered copper silicate catalyst for hydrogenation of dimethyl oxalate to methyl glycolate
Methyl glycolate (MG) is a high value-added chemical intermediate and widely used in the fields of medicine, chemical industry, fodder and dyes. A series of CuAg/SiO2 catalysts were prepared by sol-gel method for hydrogenation of dimethyl oxalate to MG. The structure of catalysts was characterized b...
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Published in | Journal of fuel chemistry and technology Vol. 50; no. 8; pp. 1014 - 1022 |
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Main Authors | , , , , , , |
Format | Journal Article |
Language | English |
Published |
Elsevier Ltd
2022
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Abstract | Methyl glycolate (MG) is a high value-added chemical intermediate and widely used in the fields of medicine, chemical industry, fodder and dyes. A series of CuAg/SiO2 catalysts were prepared by sol-gel method for hydrogenation of dimethyl oxalate to MG. The structure of catalysts was characterized by XRD, N2-physical adsorption, FT-IR, TEM, H2-TPR, and XPS, and the influence of Ag loading on catalytic performance was investigated. The 5Ag-Cu/SiO2 catalyst with Ag loading of 5% exhibited the best catalytic performance with DMO conversion of 83.7% and MG selectivity of 72.2%. The characterization results showed that introducing appropriate amount of Ag not only improved the dispersion of copper species, but also increased the content of Cu+, thereby improving the catalytic activity of CuAg/SiO2 catalysts. In addition, the electron transfer between Ag and Cu could effectively stabilize Cu+, and eventually improved the stability of the catalyst. |
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AbstractList | Methyl glycolate (MG) is a high value-added chemical intermediate and widely used in the fields of medicine, chemical industry, fodder and dyes. A series of CuAg/SiO2 catalysts were prepared by sol-gel method for hydrogenation of dimethyl oxalate to MG. The structure of catalysts was characterized by XRD, N2-physical adsorption, FT-IR, TEM, H2-TPR, and XPS, and the influence of Ag loading on catalytic performance was investigated. The 5Ag-Cu/SiO2 catalyst with Ag loading of 5% exhibited the best catalytic performance with DMO conversion of 83.7% and MG selectivity of 72.2%. The characterization results showed that introducing appropriate amount of Ag not only improved the dispersion of copper species, but also increased the content of Cu+, thereby improving the catalytic activity of CuAg/SiO2 catalysts. In addition, the electron transfer between Ag and Cu could effectively stabilize Cu+, and eventually improved the stability of the catalyst. |
Author | REN, Jun WU, Meng-meng WU, Jian-bin QUAN, Yan-hong ZHAO, Jin-xian XUE, Jing SONG, You-wei |
Author_xml | – sequence: 1 givenname: Jing surname: XUE fullname: XUE, Jing organization: State Key Laboratory of Clean and Efficient Coal Utilization, Taiyuan University of Technology, Taiyuan 030024, China – sequence: 2 givenname: Meng-meng surname: WU fullname: WU, Meng-meng organization: State Key Laboratory of Clean and Efficient Coal Utilization, Taiyuan University of Technology, Taiyuan 030024, China – sequence: 3 givenname: You-wei surname: SONG fullname: SONG, You-wei organization: State Key Laboratory of Clean and Efficient Coal Utilization, Taiyuan University of Technology, Taiyuan 030024, China – sequence: 4 givenname: Jin-xian surname: ZHAO fullname: ZHAO, Jin-xian organization: State Key Laboratory of Clean and Efficient Coal Utilization, Taiyuan University of Technology, Taiyuan 030024, China – sequence: 5 givenname: Jian-bin surname: WU fullname: WU, Jian-bin organization: School of Chemistry & Chemical Engineering, Shanxi University, Taiyuan 030006, China – sequence: 6 givenname: Yan-hong surname: QUAN fullname: QUAN, Yan-hong email: quanyanhong@tyut.edu.cn organization: State Key Laboratory of Clean and Efficient Coal Utilization, Taiyuan University of Technology, Taiyuan 030024, China – sequence: 7 givenname: Jun surname: REN fullname: REN, Jun email: renjun@tyut.edu.cn organization: State Key Laboratory of Clean and Efficient Coal Utilization, Taiyuan University of Technology, Taiyuan 030024, China |
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Keywords | lamellar copper silicate methyl glycolate silver promoter hydrogenation of dimethyl oxalate sol-gel |
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Snippet | Methyl glycolate (MG) is a high value-added chemical intermediate and widely used in the fields of medicine, chemical industry, fodder and dyes. A series of... |
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SubjectTerms | hydrogenation of dimethyl oxalate lamellar copper silicate methyl glycolate silver promoter sol-gel |
Title | Study on performance of Ag-modified layered copper silicate catalyst for hydrogenation of dimethyl oxalate to methyl glycolate |
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