Study on performance of Ag-modified layered copper silicate catalyst for hydrogenation of dimethyl oxalate to methyl glycolate

Methyl glycolate (MG) is a high value-added chemical intermediate and widely used in the fields of medicine, chemical industry, fodder and dyes. A series of CuAg/SiO2 catalysts were prepared by sol-gel method for hydrogenation of dimethyl oxalate to MG. The structure of catalysts was characterized b...

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Published inJournal of fuel chemistry and technology Vol. 50; no. 8; pp. 1014 - 1022
Main Authors XUE, Jing, WU, Meng-meng, SONG, You-wei, ZHAO, Jin-xian, WU, Jian-bin, QUAN, Yan-hong, REN, Jun
Format Journal Article
LanguageEnglish
Published Elsevier Ltd 2022
Subjects
hydrogenation of dimethyl oxalate
lamellar copper silicate
methyl glycolate
silver promoter
sol-gel
lamellar copper silicate
methyl glycolate
silver promoter
hydrogenation of dimethyl oxalate
sol-gel
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Abstract Methyl glycolate (MG) is a high value-added chemical intermediate and widely used in the fields of medicine, chemical industry, fodder and dyes. A series of CuAg/SiO2 catalysts were prepared by sol-gel method for hydrogenation of dimethyl oxalate to MG. The structure of catalysts was characterized by XRD, N2-physical adsorption, FT-IR, TEM, H2-TPR, and XPS, and the influence of Ag loading on catalytic performance was investigated. The 5Ag-Cu/SiO2 catalyst with Ag loading of 5% exhibited the best catalytic performance with DMO conversion of 83.7% and MG selectivity of 72.2%. The characterization results showed that introducing appropriate amount of Ag not only improved the dispersion of copper species, but also increased the content of Cu+, thereby improving the catalytic activity of CuAg/SiO2 catalysts. In addition, the electron transfer between Ag and Cu could effectively stabilize Cu+, and eventually improved the stability of the catalyst.
AbstractList Methyl glycolate (MG) is a high value-added chemical intermediate and widely used in the fields of medicine, chemical industry, fodder and dyes. A series of CuAg/SiO2 catalysts were prepared by sol-gel method for hydrogenation of dimethyl oxalate to MG. The structure of catalysts was characterized by XRD, N2-physical adsorption, FT-IR, TEM, H2-TPR, and XPS, and the influence of Ag loading on catalytic performance was investigated. The 5Ag-Cu/SiO2 catalyst with Ag loading of 5% exhibited the best catalytic performance with DMO conversion of 83.7% and MG selectivity of 72.2%. The characterization results showed that introducing appropriate amount of Ag not only improved the dispersion of copper species, but also increased the content of Cu+, thereby improving the catalytic activity of CuAg/SiO2 catalysts. In addition, the electron transfer between Ag and Cu could effectively stabilize Cu+, and eventually improved the stability of the catalyst.
Author REN, Jun
WU, Meng-meng
WU, Jian-bin
QUAN, Yan-hong
ZHAO, Jin-xian
XUE, Jing
SONG, You-wei
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Keywords lamellar copper silicate
methyl glycolate
silver promoter
hydrogenation of dimethyl oxalate
sol-gel
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  article-title: A boron-doped carbon aerogel-supported Cu catalyst for the selective hydrogenation of dimethyl oxalate
  publication-title: New J Chem
  doi: 10.1039/C9NJ05956C
  contributor:
    fullname: Lu
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Snippet Methyl glycolate (MG) is a high value-added chemical intermediate and widely used in the fields of medicine, chemical industry, fodder and dyes. A series of...
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elsevier
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SubjectTerms hydrogenation of dimethyl oxalate
lamellar copper silicate
methyl glycolate
silver promoter
sol-gel
Title Study on performance of Ag-modified layered copper silicate catalyst for hydrogenation of dimethyl oxalate to methyl glycolate
URI https://dx.doi.org/10.1016/S1872-5813(21)60011-2
Volume 50
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