Chemical Expansion and Change in Lattice Constant of Y‐Doped BaZrO 3 by Hydration/Dehydration Reaction and Final Heat‐Treating Temperature
Knowledge of thermal behavior of electrolyte is important for fuel cell fabrication. In this study, using high‐temperature X ‐ray diffraction analysis ( HT ‐ XRD ) and thermo‐mechanical analysis ( TMA ), a systematic investigation of lattice constants was performed on Y‐doped BaZrO 3 , which is a pr...
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| Published in | Journal of the American Ceramic Society Vol. 96; no. 3; pp. 879 - 884 |
|---|---|
| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
01.03.2013
|
| Online Access | Get full text |
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| Abstract | Knowledge of thermal behavior of electrolyte is important for fuel cell fabrication. In this study, using high‐temperature
X
‐ray diffraction analysis (
HT
‐
XRD
) and thermo‐mechanical analysis (
TMA
), a systematic investigation of lattice constants was performed on Y‐doped
BaZrO
3
, which is a promising candidate for electrolyte in protonic ceramic fuel cells. The results revealed that a chemical expansion was observed between 300°C and 450°C during the heating process in
HT
‐
XRD
, and was attributed to the dehydration of
BZY
. Furthermore, it was found that the lattice constants of the samples doped with Y, Sm, Eu, and Dy were larger for the ones finally heat‐treated at 1600°C for sintering than those heat‐treated at 1300°C for synthesizing. The similar behavior was not observed in Sc‐doped samples. |
|---|---|
| AbstractList | Knowledge of thermal behavior of electrolyte is important for fuel cell fabrication. In this study, using high‐temperature
X
‐ray diffraction analysis (
HT
‐
XRD
) and thermo‐mechanical analysis (
TMA
), a systematic investigation of lattice constants was performed on Y‐doped
BaZrO
3
, which is a promising candidate for electrolyte in protonic ceramic fuel cells. The results revealed that a chemical expansion was observed between 300°C and 450°C during the heating process in
HT
‐
XRD
, and was attributed to the dehydration of
BZY
. Furthermore, it was found that the lattice constants of the samples doped with Y, Sm, Eu, and Dy were larger for the ones finally heat‐treated at 1600°C for sintering than those heat‐treated at 1300°C for synthesizing. The similar behavior was not observed in Sc‐doped samples. |
| Author | Han, Donglin Kuramitsu, Akiko Hiraiwa, Chihiro Majima, Masatoshi Takeuchi, Hisao Uda, Tetsuya Kuwabara, Akihide |
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X
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HT
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