Unit cell parameters of 32S8 – 34S8 solid mixtures and their extremal behavior
The behavior of isotopic mixtures of polyatomic molecular compounds can have a critical character. Orthorhombic sulfur α-S8 is a typical representative of polyatomic molecular compounds among simple substances. Samples comprised of orthorhombic sulfur of different 32S and 34S ratio have been prepare...
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Published in | The Journal of physics and chemistry of solids Vol. 139; p. 109316 |
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Abstract | The behavior of isotopic mixtures of polyatomic molecular compounds can have a critical character. Orthorhombic sulfur α-S8 is a typical representative of polyatomic molecular compounds among simple substances. Samples comprised of orthorhombic sulfur of different 32S and 34S ratio have been prepared and examined with powder X-Ray diffractometry in the temperature region from −100 to +90 °С. Unit cell parameters of sulfur samples with intermolecular isotopic substitution, containing 0.4 to 0.5 parts of 34S8 molecules, differ radically from the samples of the isotopic composition close to pure α-32S8 and α-34S8. Maximal deviation of unit cell volume −0.17% at −100.0 °C is observed for the sample with a part of 34S8 molecules being 0.45. Such a behavior could well be attributed to the ordering between 32S8 and 34S8 molecules in the crystal that can be triggered by lowering temperature.
•Inter- and intramolecular isotope substituted compounds of sulfur were obtained.•Unit cell parameters of α-32S8, α-34S8 and mixtures with 25 and 75 mol.% 34S8 are not different.•Unit cell parameters of mixtures with 40–50 mol.% 34S8 demonstrate extremal contraction.•Ordering of monoisotopic molecules S8 in the mixed crystal. |
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AbstractList | The behavior of isotopic mixtures of polyatomic molecular compounds can have a critical character. Orthorhombic sulfur α-S8 is a typical representative of polyatomic molecular compounds among simple substances. Samples comprised of orthorhombic sulfur of different 32S and 34S ratio have been prepared and examined with powder X-Ray diffractometry in the temperature region from −100 to +90 °С. Unit cell parameters of sulfur samples with intermolecular isotopic substitution, containing 0.4 to 0.5 parts of 34S8 molecules, differ radically from the samples of the isotopic composition close to pure α-32S8 and α-34S8. Maximal deviation of unit cell volume −0.17% at −100.0 °C is observed for the sample with a part of 34S8 molecules being 0.45. Such a behavior could well be attributed to the ordering between 32S8 and 34S8 molecules in the crystal that can be triggered by lowering temperature.
•Inter- and intramolecular isotope substituted compounds of sulfur were obtained.•Unit cell parameters of α-32S8, α-34S8 and mixtures with 25 and 75 mol.% 34S8 are not different.•Unit cell parameters of mixtures with 40–50 mol.% 34S8 demonstrate extremal contraction.•Ordering of monoisotopic molecules S8 in the mixed crystal. |
ArticleNumber | 109316 |
Author | Dmitrienko, Anton S. Churbanov, Mikhail F. Sukhanov, Maksim V. Velmuzhov, Aleksandr P. Knyazev, Aleksandr V. Kotereva, Tatyana V. |
Author_xml | – sequence: 1 givenname: Maksim V. surname: Sukhanov fullname: Sukhanov, Maksim V. email: mrmaks@yandex.ru organization: Devyatykh Institute of Chemistry of High-Purity Substances, Tropinina 49, Nizhni Novgorod, 603950, Russia – sequence: 2 givenname: Aleksandr P. surname: Velmuzhov fullname: Velmuzhov, Aleksandr P. organization: Devyatykh Institute of Chemistry of High-Purity Substances, Tropinina 49, Nizhni Novgorod, 603950, Russia – sequence: 3 givenname: Tatyana V. surname: Kotereva fullname: Kotereva, Tatyana V. organization: Devyatykh Institute of Chemistry of High-Purity Substances, Tropinina 49, Nizhni Novgorod, 603950, Russia – sequence: 4 givenname: Mikhail F. surname: Churbanov fullname: Churbanov, Mikhail F. organization: Devyatykh Institute of Chemistry of High-Purity Substances, Tropinina 49, Nizhni Novgorod, 603950, Russia – sequence: 5 givenname: Aleksandr V. surname: Knyazev fullname: Knyazev, Aleksandr V. organization: Department of Chemistry, Lobachevsky State University of Nizhni Novgorod, Gagarina 23, Nizhniy Novgorod, 603950, Russia – sequence: 6 givenname: Anton S. surname: Dmitrienko fullname: Dmitrienko, Anton S. organization: Brock University, 1812 Sir Isaac Brock Way, St. Catharines, ON, L2S 3A1, Canada |
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Keywords | Sulfur isotopes Extremal behavior Lattice parameters Solid solution Molecular adduct Isotope ordering |
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SubjectTerms | Extremal behavior Isotope ordering Lattice parameters Molecular adduct Solid solution Sulfur isotopes |
Title | Unit cell parameters of 32S8 – 34S8 solid mixtures and their extremal behavior |
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