TiO 2 / CdS nanocomposite films: fabrication, characterization, electronic and optical properties
Abstract In this work, TiO 2 nanocrystalline thin films were obtained through evaporating Ti films by electron beam deposition (EBD) followed by thermal treatment. The results show that after annealing at 300, 400 and 450 ° C for 8 h, the obtained TiO 2 thin films have nanoparticle and nanorod struc...
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Published in | Advances in natural sciences. Nanoscience and nanotechnology Vol. 1; no. 1; p. 15002 |
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Main Authors | , , , |
Format | Journal Article |
Language | English |
Published |
01.03.2010
|
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Abstract | Abstract
In this work,
TiO
2
nanocrystalline thin films were obtained through evaporating Ti films by electron beam deposition (EBD) followed by thermal treatment. The results show that after annealing at 300, 400 and 450 °
C
for 8 h, the obtained
TiO
2
thin films have nanoparticle and nanorod structures of 15–30 nm diameter and 100–300 nm length. At 750 °
C
for 8 h, the rutile phase was formed. The incorporation of cadmium sulfide (CdS) into
TiO
2
nanoparticle thin films was investigated. A CdS thin film was vacuum deposited onto the pre-deposited
TiO
2
film by a thermal evaporation technique. The obtained
TiO
2
and
TiO
2
/
CdS
nanocomposite films were characterized by x-ray diffraction (XRD) and a field emission scanning electron microscope (FE-SEM). The
TiO
2
/
CdS
composite film was used in a photo-electrochemical (PEC) cell as a working electrode and in a platinum electrode as a counter electrode. The electrolyte solution contains 1 M KCl and 0.1 M
Na
2
S
. The results show that the cell with the
TiO
2
/
CdS
composite film electrode has significantly improved photoelectric capability in comparison with that of pure
TiO
2
thin films, and the best thickness of the CdS thin film deposited on the
ITO
/
TiO
2
substrates is 70–140 nm. |
---|---|
AbstractList | Abstract
In this work,
TiO
2
nanocrystalline thin films were obtained through evaporating Ti films by electron beam deposition (EBD) followed by thermal treatment. The results show that after annealing at 300, 400 and 450 °
C
for 8 h, the obtained
TiO
2
thin films have nanoparticle and nanorod structures of 15–30 nm diameter and 100–300 nm length. At 750 °
C
for 8 h, the rutile phase was formed. The incorporation of cadmium sulfide (CdS) into
TiO
2
nanoparticle thin films was investigated. A CdS thin film was vacuum deposited onto the pre-deposited
TiO
2
film by a thermal evaporation technique. The obtained
TiO
2
and
TiO
2
/
CdS
nanocomposite films were characterized by x-ray diffraction (XRD) and a field emission scanning electron microscope (FE-SEM). The
TiO
2
/
CdS
composite film was used in a photo-electrochemical (PEC) cell as a working electrode and in a platinum electrode as a counter electrode. The electrolyte solution contains 1 M KCl and 0.1 M
Na
2
S
. The results show that the cell with the
TiO
2
/
CdS
composite film electrode has significantly improved photoelectric capability in comparison with that of pure
TiO
2
thin films, and the best thickness of the CdS thin film deposited on the
ITO
/
TiO
2
substrates is 70–140 nm. |
Author | Dang, Tran Chien Le, Ha Chi Pham, Van Hoi Pham, Duy Long |
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Snippet | Abstract
In this work,
TiO
2
nanocrystalline thin films were obtained through evaporating Ti films by electron beam deposition (EBD) followed by thermal... |
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