Crystal Growth and Electrical Properties of Pb((Zn 1/3 Nb 2/3 ) 0.91 Ti 0.09 )O 3 Single Crystals Produced by Solution Bridgman Method
Piezoelectric Pb((Zn 1/3 Nb 2/3 ) 0.91 Ti 0.09 )O 3 (PZNT 91/9) single crystals 40 mm in diameter were successfully grown from solution by the Bridgman method with a PbO flux. The crystals were grown in a platinum crucible heated to 1130°C. Growth rate was 0.35 mm/h. The obtained crystals were ~40 m...
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| Published in | Journal of the American Ceramic Society Vol. 81; no. 11; pp. 2785 - 2788 |
|---|---|
| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
01.11.1998
|
| Online Access | Get full text |
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| Abstract | Piezoelectric Pb((Zn
1/3
Nb
2/3
)
0.91
Ti
0.09
)O
3
(PZNT 91/9) single crystals 40 mm in diameter were successfully grown from solution by the Bridgman method with a PbO flux. The crystals were grown in a platinum crucible heated to 1130°C. Growth rate was 0.35 mm/h. The obtained crystals were ~40 mm in diameter 20 mm in length and were a rust‐brown color. The Curie temperature,
T
C
, ranged from 175° to 185°C, and the dielectric constant before poling at room temperature was 2000‐8900 within a wafer. After electrical poling, specimens had electromechanical coupling coefficients in rectangular bar mode,
k
33´
, of 79%‐88%, which were larger than for PZT ceramics (
k
33´
< 70%). These PZNT 91/9 single crystals grown by the Bridgman process satisfy the requirements for array‐type transducers used in echocardiographic equipment. Results confirm that the Bridgman method is useful for mass‐producing large crystals of PZNT 91/9. |
|---|---|
| AbstractList | Piezoelectric Pb((Zn
1/3
Nb
2/3
)
0.91
Ti
0.09
)O
3
(PZNT 91/9) single crystals 40 mm in diameter were successfully grown from solution by the Bridgman method with a PbO flux. The crystals were grown in a platinum crucible heated to 1130°C. Growth rate was 0.35 mm/h. The obtained crystals were ~40 mm in diameter 20 mm in length and were a rust‐brown color. The Curie temperature,
T
C
, ranged from 175° to 185°C, and the dielectric constant before poling at room temperature was 2000‐8900 within a wafer. After electrical poling, specimens had electromechanical coupling coefficients in rectangular bar mode,
k
33´
, of 79%‐88%, which were larger than for PZT ceramics (
k
33´
< 70%). These PZNT 91/9 single crystals grown by the Bridgman process satisfy the requirements for array‐type transducers used in echocardiographic equipment. Results confirm that the Bridgman method is useful for mass‐producing large crystals of PZNT 91/9. |
| Author | Yamashita, Yohachi Shimanuki, Senji Harada, Kouichi Saitoh, Shiroh Kobayashi, Tsuyoshi |
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| Cites_doi | 10.1117/12.271324 10.1143/JJAP.36.6035 10.1143/JJAP.37.3382 10.2109/jcersj.106.116 10.1143/JJAP.21.1298 |
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| References | e_1_2_1_6_2 e_1_2_1_7_2 Harada K. (e_1_2_1_11_2) 1996 Lopath P. D. (e_1_2_1_4_2) 1996 e_1_2_1_5_2 e_1_2_1_2_2 e_1_2_1_10_2 Harada K. (e_1_2_1_12_2) 1997 Park S. E. (e_1_2_1_3_2) 1994; 33 e_1_2_1_13_2 e_1_2_1_8_2 e_1_2_1_9_2 |
| References_xml | – ident: e_1_2_1_6_2 doi: 10.1117/12.271324 – start-page: 398 volume-title: Proceedings of 1997 Japan International Electronic Manufacturing Technology Symposium year: 1997 ident: e_1_2_1_12_2 contributor: fullname: Harada K. – ident: e_1_2_1_5_2 – ident: e_1_2_1_7_2 – ident: e_1_2_1_9_2 doi: 10.1143/JJAP.36.6035 – ident: e_1_2_1_10_2 doi: 10.1143/JJAP.37.3382 – volume: 33 start-page: 5328 year: 1994 ident: e_1_2_1_3_2 article-title: Ultrahigh Strain and Piezoelectric Behavior in Relaxor Based Ferroelectric Single Crystal publication-title: J. Appl. Phys. contributor: fullname: Park S. E. – ident: e_1_2_1_13_2 doi: 10.2109/jcersj.106.116 – start-page: 95 volume-title: Proceedings of 16th Electronics Division Meeting of The Ceramic Society of Japan year: 1996 ident: e_1_2_1_11_2 contributor: fullname: Harada K. – start-page: 543 volume-title: Proceedings of the 1996 International Symposium on the Application of Ferroelectrics (East Brunswick year: 1996 ident: e_1_2_1_4_2 contributor: fullname: Lopath P. D. – ident: e_1_2_1_2_2 doi: 10.1143/JJAP.21.1298 – ident: e_1_2_1_8_2 |
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| Snippet | Piezoelectric Pb((Zn
1/3
Nb
2/3
)
0.91
Ti
0.09
)O
3
(PZNT 91/9) single crystals 40 mm in diameter were successfully grown from solution by the Bridgman method... |
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| Title | Crystal Growth and Electrical Properties of Pb((Zn 1/3 Nb 2/3 ) 0.91 Ti 0.09 )O 3 Single Crystals Produced by Solution Bridgman Method |
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