Sintering of 3 D ‐Printed Glass/ HA p Composites

We report the sintering of 3 D ‐printed composites of 13‐93 bioactive glass and hydroxyapatite ( HA p) powders. The sintering process is characterized on conventionally produced powder compacts with varying HA p content. A numeric approximation of the densification kinetics is then obtained on the b...

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Published inJournal of the American Ceramic Society Vol. 95; no. 11; pp. 3387 - 3393
Main Authors Winkel, Alexander, Meszaros, Robert, Reinsch, Stefan, Müller, Ralf, Travitzky, Nahum, Fey, Tobias, Greil, Peter, Wondraczek, Lothar
Format Journal Article
LanguageEnglish
Published 01.11.2012
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Abstract We report the sintering of 3 D ‐printed composites of 13‐93 bioactive glass and hydroxyapatite ( HA p) powders. The sintering process is characterized on conventionally produced powder compacts with varying HA p content. A numeric approximation of the densification kinetics is then obtained on the basis of Frenkel, Mackenzie–Shuttleworth, and Einstein–Roscoe models, and optimized sintering conditions for 3 D ‐printed structures are derived. Fully isotropic sintering of complex cellular composites is obtained by continuous heating to 750°C at a rate of 2 K/min for a HA p content of 40 wt%. The approach can readily be generalized for printing and sintering of similar glass‐ceramic composites.
AbstractList We report the sintering of 3 D ‐printed composites of 13‐93 bioactive glass and hydroxyapatite ( HA p) powders. The sintering process is characterized on conventionally produced powder compacts with varying HA p content. A numeric approximation of the densification kinetics is then obtained on the basis of Frenkel, Mackenzie–Shuttleworth, and Einstein–Roscoe models, and optimized sintering conditions for 3 D ‐printed structures are derived. Fully isotropic sintering of complex cellular composites is obtained by continuous heating to 750°C at a rate of 2 K/min for a HA p content of 40 wt%. The approach can readily be generalized for printing and sintering of similar glass‐ceramic composites.
Author Greil, Peter
Winkel, Alexander
Travitzky, Nahum
Fey, Tobias
Meszaros, Robert
Reinsch, Stefan
Müller, Ralf
Wondraczek, Lothar
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