Using UCST Ionic Liquid as a Draw Solute in Forward Osmosis to Treat High-Salinity Water

The concept of using a thermoresponsive ionic liquid (IL) with an upper critical solution temperature (UCST) as a draw solute in forward osmosis (FO) was successfully demonstrated here experimentally. A 3.2 M solution of protonated betaine bis­(trifluoromethylsulfonyl)­imide ([Hbet]­[Tf2N]) was obta...

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Published inEnvironmental science & technology Vol. 50; no. 2; pp. 1039 - 1045
Main Authors Zhong, Yujiang, Feng, Xiaoshuang, Chen, Wei, Wang, Xinbo, Huang, Kuo-Wei, Gnanou, Yves, Lai, Zhiping
Format Journal Article
LanguageEnglish
Published United States American Chemical Society 19.01.2016
Subjects
ambient temperature
betaine
Heating
ionic liquids
Ionic Liquids - chemistry
Ions
Osmosis
Salinity
Solubility
solutes
Solutions - chemistry
Spectrophotometry, Ultraviolet
Temperature
Temperature effects
thermal stability
Ultraviolet radiation
ultraviolet-visible spectroscopy
Water - chemistry
Water Purification - methods
water salinity
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Abstract The concept of using a thermoresponsive ionic liquid (IL) with an upper critical solution temperature (UCST) as a draw solute in forward osmosis (FO) was successfully demonstrated here experimentally. A 3.2 M solution of protonated betaine bis­(trifluoromethylsulfonyl)­imide ([Hbet]­[Tf2N]) was obtained by heating and maintaining the temperature above 56 °C. This solution successfully drew water from high-salinity water up to 3.0 M through FO. When the IL solution cooled to room temperature, it spontaneously separated into a water-rich phase and an IL-rich phase: the water-rich phase was the produced water that contained a low IL concentration, and the IL-rich phase could be used directly as the draw solution in the next cycle of the FO process. The thermal stability, thermal-responsive solubility, and UV–vis absorption spectra of the IL were also studied in detail.
AbstractList The concept of using a thermoresponsive ionic liquid (IL) with an upper critical solution temperature (UCST) as a draw solute in forward osmosis (FO) was successfully demonstrated here experimentally. A 3.2 M solution of protonated betaine bis(trifluoromethylsulfonyl)imide ([Hbet][Tf2N]) was obtained by heating and maintaining the temperature above 56 °C. This solution successfully drew water from high-salinity water up to 3.0 M through FO. When the IL solution cooled to room temperature, it spontaneously separated into a water-rich phase and an IL-rich phase: the water-rich phase was the produced water that contained a low IL concentration, and the IL-rich phase could be used directly as the draw solution in the next cycle of the FO process. The thermal stability, thermal-responsive solubility, and UV-vis absorption spectra of the IL were also studied in detail.
The concept of using a thermoresponsive ionic liquid (IL) with an upper critical solution temperature (UCST) as a draw solute in forward osmosis (FO) was successfully demonstrated here experimentally. A 3.2 M solution of protonated betaine bis(trifluoromethylsulfonyl)imide ([Hbet][Tf2N]) was obtained by heating and maintaining the temperature above 56 degree C. This solution successfully drew water from high-salinity water up to 3.0 M through FO. When the IL solution cooled to room temperature, it spontaneously separated into a water-rich phase and an IL-rich phase: the water-rich phase was the produced water that contained a low IL concentration, and the IL-rich phase could be used directly as the draw solution in the next cycle of the FO process. The thermal stability, thermal-responsive solubility, and UV-vis absorption spectra of the IL were also studied in detail.
The concept of using a thermoresponsive ionic liquid (IL) with an upper critical solution temperature (UCST) as a draw solute in forward osmosis (FO) was successfully demonstrated here experimentally. A 3.2 M solution of protonated betaine bis­(trifluoromethylsulfonyl)­imide ([Hbet]­[Tf2N]) was obtained by heating and maintaining the temperature above 56 °C. This solution successfully drew water from high-salinity water up to 3.0 M through FO. When the IL solution cooled to room temperature, it spontaneously separated into a water-rich phase and an IL-rich phase: the water-rich phase was the produced water that contained a low IL concentration, and the IL-rich phase could be used directly as the draw solution in the next cycle of the FO process. The thermal stability, thermal-responsive solubility, and UV–vis absorption spectra of the IL were also studied in detail.
The concept of using a thermoresponsive ionic liquid (IL) with an upper critical solution temperature (UCST) as a draw solute in forward osmosis (FO) was successfully demonstrated here experimentally. A 3.2 M solution of protonated betaine bis(trifluoromethylsulfonyl)imide ([Hbet][Tf2N]) was obtained by heating and maintaining the temperature above 56 °C. This solution successfully drew water from high-salinity water up to 3.0 M through FO. When the IL solution cooled to room temperature, it spontaneously separated into a water-rich phase and an IL-rich phase: the water-rich phase was the produced water that contained a low IL concentration, and the IL-rich phase could be used directly as the draw solution in the next cycle of the FO process. The thermal stability, thermal-responsive solubility, and UV-vis absorption spectra of the IL were also studied in detail.The concept of using a thermoresponsive ionic liquid (IL) with an upper critical solution temperature (UCST) as a draw solute in forward osmosis (FO) was successfully demonstrated here experimentally. A 3.2 M solution of protonated betaine bis(trifluoromethylsulfonyl)imide ([Hbet][Tf2N]) was obtained by heating and maintaining the temperature above 56 °C. This solution successfully drew water from high-salinity water up to 3.0 M through FO. When the IL solution cooled to room temperature, it spontaneously separated into a water-rich phase and an IL-rich phase: the water-rich phase was the produced water that contained a low IL concentration, and the IL-rich phase could be used directly as the draw solution in the next cycle of the FO process. The thermal stability, thermal-responsive solubility, and UV-vis absorption spectra of the IL were also studied in detail.
Author Chen, Wei
Lai, Zhiping
Wang, Xinbo
Huang, Kuo-Wei
Gnanou, Yves
Zhong, Yujiang
Feng, Xiaoshuang
AuthorAffiliation Division of Physical Science and Engineering
King Abdullah University of Science and Technology
AuthorAffiliation_xml – name: Division of Physical Science and Engineering
– name: King Abdullah University of Science and Technology
Author_xml – sequence: 1
  givenname: Yujiang
  surname: Zhong
  fullname: Zhong, Yujiang
– sequence: 2
  givenname: Xiaoshuang
  surname: Feng
  fullname: Feng, Xiaoshuang
– sequence: 3
  givenname: Wei
  surname: Chen
  fullname: Chen, Wei
– sequence: 4
  givenname: Xinbo
  surname: Wang
  fullname: Wang, Xinbo
– sequence: 5
  givenname: Kuo-Wei
  surname: Huang
  fullname: Huang, Kuo-Wei
– sequence: 6
  givenname: Yves
  surname: Gnanou
  fullname: Gnanou, Yves
– sequence: 7
  givenname: Zhiping
  surname: Lai
  fullname: Lai, Zhiping
  email: Zhiping.lai@kaust.edu.sa
BackLink https://www.ncbi.nlm.nih.gov/pubmed/26649525$$D View this record in MEDLINE/PubMed
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Snippet The concept of using a thermoresponsive ionic liquid (IL) with an upper critical solution temperature (UCST) as a draw solute in forward osmosis (FO) was...
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SubjectTerms ambient temperature
betaine
Heating
ionic liquids
Ionic Liquids - chemistry
Ions
Osmosis
Salinity
Solubility
solutes
Solutions - chemistry
Spectrophotometry, Ultraviolet
Temperature
Temperature effects
thermal stability
Ultraviolet radiation
ultraviolet-visible spectroscopy
Water - chemistry
Water Purification - methods
water salinity
Title Using UCST Ionic Liquid as a Draw Solute in Forward Osmosis to Treat High-Salinity Water
URI http://dx.doi.org/10.1021/acs.est.5b03747
https://www.ncbi.nlm.nih.gov/pubmed/26649525
https://www.proquest.com/docview/1762722097
https://www.proquest.com/docview/1760895571
https://www.proquest.com/docview/1765943717
https://www.proquest.com/docview/2000231059
Volume 50
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