Production of Nanocellulose Using Hydrated Deep Eutectic Solvent Combined with Ultrasonic Treatment
Pretreatment approaches are highly desirable to improve the commercial viability of nanocellulose production. In this study, we propose a new approach to mass produce nanocellulose using a hydrated choline chloride/oxalic acid dihydrate deep eutectic solvent (DES) combined with an ultrasonic process...
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| Published in | ACS omega Vol. 4; no. 5; pp. 8539 - 8547 |
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| Main Authors | , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
United States
American Chemical Society
31.05.2019
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| Online Access | Get full text |
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| Abstract | Pretreatment approaches are highly desirable to improve the commercial viability of nanocellulose production. In this study, we propose a new approach to mass produce nanocellulose using a hydrated choline chloride/oxalic acid dihydrate deep eutectic solvent (DES) combined with an ultrasonic process. The hydrogen bond acidity, polarizability, and solvation effect reflected by the Kamlet–Taft solvatochromic parameters did not decrease even after the addition of large amounts of water. Instead, the water facilitated the ionization of H+ and delocalization of Cl– ions, forming new Cl–H2O ionic hydrogen and oxalate–H2O hydrogen bonds, which are critical for improving the solvent characteristics. One pass of kraft pulp through the hydrated DESs (80 °C, 1 h) was sufficient to dissociate the kraft pulp into cellulose nanofibers or cellulose nanocrystals using an 800 W ultrasonic treatment. The present study represents an alternative route for the kraft pulp pretreatment and the large-scale production of nanocellulose. |
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| AbstractList | Pretreatment approaches are highly desirable to improve the commercial viability of nanocellulose production. In this study, we propose a new approach to mass produce nanocellulose using a hydrated choline chloride/oxalic acid dihydrate deep eutectic solvent (DES) combined with an ultrasonic process. The hydrogen bond acidity, polarizability, and solvation effect reflected by the Kamlet–Taft solvatochromic parameters did not decrease even after the addition of large amounts of water. Instead, the water facilitated the ionization of H+ and delocalization of Cl– ions, forming new Cl–H2O ionic hydrogen and oxalate–H2O hydrogen bonds, which are critical for improving the solvent characteristics. One pass of kraft pulp through the hydrated DESs (80 °C, 1 h) was sufficient to dissociate the kraft pulp into cellulose nanofibers or cellulose nanocrystals using an 800 W ultrasonic treatment. The present study represents an alternative route for the kraft pulp pretreatment and the large-scale production of nanocellulose. Pretreatment approaches are highly desirable to improve the commercial viability of nanocellulose production. In this study, we propose a new approach to mass produce nanocellulose using a hydrated choline chloride/oxalic acid dihydrate deep eutectic solvent (DES) combined with an ultrasonic process. The hydrogen bond acidity, polarizability, and solvation effect reflected by the Kamlet–Taft solvatochromic parameters did not decrease even after the addition of large amounts of water. Instead, the water facilitated the ionization of H + and delocalization of Cl – ions, forming new Cl–H 2 O ionic hydrogen and oxalate–H 2 O hydrogen bonds, which are critical for improving the solvent characteristics. One pass of kraft pulp through the hydrated DESs (80 °C, 1 h) was sufficient to dissociate the kraft pulp into cellulose nanofibers or cellulose nanocrystals using an 800 W ultrasonic treatment. The present study represents an alternative route for the kraft pulp pretreatment and the large-scale production of nanocellulose. Pretreatment approaches are highly desirable to improve the commercial viability of nanocellulose production. In this study, we propose a new approach to mass produce nanocellulose using a hydrated choline chloride/oxalic acid dihydrate deep eutectic solvent (DES) combined with an ultrasonic process. The hydrogen bond acidity, polarizability, and solvation effect reflected by the Kamlet-Taft solvatochromic parameters did not decrease even after the addition of large amounts of water. Instead, the water facilitated the ionization of H and delocalization of Cl ions, forming new Cl-H O ionic hydrogen and oxalate-H O hydrogen bonds, which are critical for improving the solvent characteristics. One pass of kraft pulp through the hydrated DESs (80 °C, 1 h) was sufficient to dissociate the kraft pulp into cellulose nanofibers or cellulose nanocrystals using an 800 W ultrasonic treatment. The present study represents an alternative route for the kraft pulp pretreatment and the large-scale production of nanocellulose. |
| Author | Ma, Yue Yu, Haipeng Liu, Shouxin Liu, Yixing Xia, Qinqin Liu, Yongzhuang Wang, Qingwen Li, Jian Chen, Wenshuai |
| AuthorAffiliation | Key Laboratory of Bio-based Material Science and Technology of Ministry of Education |
| AuthorAffiliation_xml | – name: Key Laboratory of Bio-based Material Science and Technology of Ministry of Education |
| Author_xml | – sequence: 1 givenname: Yue surname: Ma fullname: Ma, Yue – sequence: 2 givenname: Qinqin surname: Xia fullname: Xia, Qinqin – sequence: 3 givenname: Yongzhuang surname: Liu fullname: Liu, Yongzhuang – sequence: 4 givenname: Wenshuai orcidid: 0000-0003-4428-1505 surname: Chen fullname: Chen, Wenshuai – sequence: 5 givenname: Shouxin surname: Liu fullname: Liu, Shouxin – sequence: 6 givenname: Qingwen surname: Wang fullname: Wang, Qingwen – sequence: 7 givenname: Yixing surname: Liu fullname: Liu, Yixing – sequence: 8 givenname: Jian surname: Li fullname: Li, Jian – sequence: 9 givenname: Haipeng orcidid: 0000-0003-0634-7913 surname: Yu fullname: Yu, Haipeng email: yuhaipeng20000@nefu.edu.cn |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/31459944$$D View this record in MEDLINE/PubMed |
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| Snippet | Pretreatment approaches are highly desirable to improve the commercial viability of nanocellulose production. In this study, we propose a new approach to mass... Pretreatment approaches are highly desirable to improve the commercial viability of nanocellulose production. In this study, we propose a new approach to mass... |
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| Title | Production of Nanocellulose Using Hydrated Deep Eutectic Solvent Combined with Ultrasonic Treatment |
| URI | http://dx.doi.org/10.1021/acsomega.9b00519 https://www.ncbi.nlm.nih.gov/pubmed/31459944 https://search.proquest.com/docview/2281848426 https://pubmed.ncbi.nlm.nih.gov/PMC6648160 https://doaj.org/article/1b2b3904169a41679e580fa6c84dda86 |
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