Role of Ferrate(IV) and Ferrate(V) in Activating Ferrate(VI) by Calcium Sulfite for Enhanced Oxidation of Organic Contaminants
Although the Fe(VI)–sulfite process has shown great potential for the rapid removal of organic contaminants, the major active oxidants (Fe(IV)/Fe(V) versus SO4 •–/•OH) involved in this process are still under debate. By employing sparingly soluble CaSO3 as a slow-releasing source of SO3 2–, this...
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| Published in | Environmental science & technology Vol. 53; no. 2; pp. 894 - 902 |
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| Main Authors | , , , |
| Format | Journal Article |
| Language | English |
| Published |
United States
American Chemical Society
15.01.2019
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| Subjects | |
| Online Access | Get full text |
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| Abstract | Although the Fe(VI)–sulfite process has shown great potential for the rapid removal of organic contaminants, the major active oxidants (Fe(IV)/Fe(V) versus SO4 •–/•OH) involved in this process are still under debate. By employing sparingly soluble CaSO3 as a slow-releasing source of SO3 2–, this study evaluated the oxidation performance of the Fe(VI)–CaSO3 process and identified the active oxidants involved in this process. The process exhibited efficient oxidation of a variety of compounds, including antibiotics, pharmaceuticals, and pesticides, at rates that were 6.1–173.7-fold faster than those measured for Fe(VI) alone, depending on pH, CaSO3 dosage, and the properties of organic contaminants. Many lines of evidence verified that neither SO4 •– nor •OH was the active species in the Fe(VI)–CaSO3 process. The accelerating effect of CaSO3 was ascribed to the direct generation of Fe(IV)/Fe(V) species from the reaction of Fe(VI) with soluble SO3 2– via one-electron steps as well as the indirect generation of Fe(IV)/Fe(V) species from the self-decay of Fe(VI) and Fe(VI) reaction with H2O2, which could be catalyzed by uncomplexed Fe(III). Besides, the Fe(VI)–CaSO3 process exhibited satisfactory removal of organic contaminants in real water, and inorganic anions showed negligible effects on organic contaminant decomposition in this process. Thus, the Fe(VI)–CaSO3 process with Fe(IV)/Fe(V) as reactive oxidants may be a promising method for abating various micropollutants in water treatment. |
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| AbstractList | Although the Fe(VI)–sulfite process has shown great potential for the rapid removal of organic contaminants, the major active oxidants (Fe(IV)/Fe(V) versus SO4•–/•OH) involved in this process are still under debate. By employing sparingly soluble CaSO3 as a slow-releasing source of SO32–, this study evaluated the oxidation performance of the Fe(VI)–CaSO3 process and identified the active oxidants involved in this process. The process exhibited efficient oxidation of a variety of compounds, including antibiotics, pharmaceuticals, and pesticides, at rates that were 6.1–173.7-fold faster than those measured for Fe(VI) alone, depending on pH, CaSO3 dosage, and the properties of organic contaminants. Many lines of evidence verified that neither SO4•– nor •OH was the active species in the Fe(VI)–CaSO3 process. The accelerating effect of CaSO3 was ascribed to the direct generation of Fe(IV)/Fe(V) species from the reaction of Fe(VI) with soluble SO32– via one-electron steps as well as the indirect generation of Fe(IV)/Fe(V) species from the self-decay of Fe(VI) and Fe(VI) reaction with H2O2, which could be catalyzed by uncomplexed Fe(III). Besides, the Fe(VI)–CaSO3 process exhibited satisfactory removal of organic contaminants in real water, and inorganic anions showed negligible effects on organic contaminant decomposition in this process. Thus, the Fe(VI)–CaSO3 process with Fe(IV)/Fe(V) as reactive oxidants may be a promising method for abating various micropollutants in water treatment. Although the Fe(VI)-sulfite process has shown great potential for the rapid removal of organic contaminants, the major active oxidants (Fe(IV)/Fe(V) versus SO / OH) involved in this process are still under debate. By employing sparingly soluble CaSO as a slow-releasing source of SO , this study evaluated the oxidation performance of the Fe(VI)-CaSO process and identified the active oxidants involved in this process. The process exhibited efficient oxidation of a variety of compounds, including antibiotics, pharmaceuticals, and pesticides, at rates that were 6.1-173.7-fold faster than those measured for Fe(VI) alone, depending on pH, CaSO dosage, and the properties of organic contaminants. Many lines of evidence verified that neither SO nor OH was the active species in the Fe(VI)-CaSO process. The accelerating effect of CaSO was ascribed to the direct generation of Fe(IV)/Fe(V) species from the reaction of Fe(VI) with soluble SO via one-electron steps as well as the indirect generation of Fe(IV)/Fe(V) species from the self-decay of Fe(VI) and Fe(VI) reaction with H O , which could be catalyzed by uncomplexed Fe(III). Besides, the Fe(VI)-CaSO process exhibited satisfactory removal of organic contaminants in real water, and inorganic anions showed negligible effects on organic contaminant decomposition in this process. Thus, the Fe(VI)-CaSO process with Fe(IV)/Fe(V) as reactive oxidants may be a promising method for abating various micropollutants in water treatment. Although the Fe(VI)–sulfite process has shown great potential for the rapid removal of organic contaminants, the major active oxidants (Fe(IV)/Fe(V) versus SO4 •–/•OH) involved in this process are still under debate. By employing sparingly soluble CaSO3 as a slow-releasing source of SO3 2–, this study evaluated the oxidation performance of the Fe(VI)–CaSO3 process and identified the active oxidants involved in this process. The process exhibited efficient oxidation of a variety of compounds, including antibiotics, pharmaceuticals, and pesticides, at rates that were 6.1–173.7-fold faster than those measured for Fe(VI) alone, depending on pH, CaSO3 dosage, and the properties of organic contaminants. Many lines of evidence verified that neither SO4 •– nor •OH was the active species in the Fe(VI)–CaSO3 process. The accelerating effect of CaSO3 was ascribed to the direct generation of Fe(IV)/Fe(V) species from the reaction of Fe(VI) with soluble SO3 2– via one-electron steps as well as the indirect generation of Fe(IV)/Fe(V) species from the self-decay of Fe(VI) and Fe(VI) reaction with H2O2, which could be catalyzed by uncomplexed Fe(III). Besides, the Fe(VI)–CaSO3 process exhibited satisfactory removal of organic contaminants in real water, and inorganic anions showed negligible effects on organic contaminant decomposition in this process. Thus, the Fe(VI)–CaSO3 process with Fe(IV)/Fe(V) as reactive oxidants may be a promising method for abating various micropollutants in water treatment. Although the Fe(VI)-sulfite process has shown great potential for the rapid removal of organic contaminants, the major active oxidants (Fe(IV)/Fe(V) versus SO4•-/•OH) involved in this process are still under debate. By employing sparingly soluble CaSO3 as a slow-releasing source of SO32-, this study evaluated the oxidation performance of the Fe(VI)-CaSO3 process and identified the active oxidants involved in this process. The process exhibited efficient oxidation of a variety of compounds, including antibiotics, pharmaceuticals, and pesticides, at rates that were 6.1-173.7-fold faster than those measured for Fe(VI) alone, depending on pH, CaSO3 dosage, and the properties of organic contaminants. Many lines of evidence verified that neither SO4•- nor •OH was the active species in the Fe(VI)-CaSO3 process. The accelerating effect of CaSO3 was ascribed to the direct generation of Fe(IV)/Fe(V) species from the reaction of Fe(VI) with soluble SO32- via one-electron steps as well as the indirect generation of Fe(IV)/Fe(V) species from the self-decay of Fe(VI) and Fe(VI) reaction with H2O2, which could be catalyzed by uncomplexed Fe(III). Besides, the Fe(VI)-CaSO3 process exhibited satisfactory removal of organic contaminants in real water, and inorganic anions showed negligible effects on organic contaminant decomposition in this process. Thus, the Fe(VI)-CaSO3 process with Fe(IV)/Fe(V) as reactive oxidants may be a promising method for abating various micropollutants in water treatment.Although the Fe(VI)-sulfite process has shown great potential for the rapid removal of organic contaminants, the major active oxidants (Fe(IV)/Fe(V) versus SO4•-/•OH) involved in this process are still under debate. By employing sparingly soluble CaSO3 as a slow-releasing source of SO32-, this study evaluated the oxidation performance of the Fe(VI)-CaSO3 process and identified the active oxidants involved in this process. The process exhibited efficient oxidation of a variety of compounds, including antibiotics, pharmaceuticals, and pesticides, at rates that were 6.1-173.7-fold faster than those measured for Fe(VI) alone, depending on pH, CaSO3 dosage, and the properties of organic contaminants. Many lines of evidence verified that neither SO4•- nor •OH was the active species in the Fe(VI)-CaSO3 process. The accelerating effect of CaSO3 was ascribed to the direct generation of Fe(IV)/Fe(V) species from the reaction of Fe(VI) with soluble SO32- via one-electron steps as well as the indirect generation of Fe(IV)/Fe(V) species from the self-decay of Fe(VI) and Fe(VI) reaction with H2O2, which could be catalyzed by uncomplexed Fe(III). Besides, the Fe(VI)-CaSO3 process exhibited satisfactory removal of organic contaminants in real water, and inorganic anions showed negligible effects on organic contaminant decomposition in this process. Thus, the Fe(VI)-CaSO3 process with Fe(IV)/Fe(V) as reactive oxidants may be a promising method for abating various micropollutants in water treatment. Although the Fe(VI)–sulfite process has shown great potential for the rapid removal of organic contaminants, the major active oxidants (Fe(IV)/Fe(V) versus SO₄•–/•OH) involved in this process are still under debate. By employing sparingly soluble CaSO₃ as a slow-releasing source of SO₃²–, this study evaluated the oxidation performance of the Fe(VI)–CaSO₃ process and identified the active oxidants involved in this process. The process exhibited efficient oxidation of a variety of compounds, including antibiotics, pharmaceuticals, and pesticides, at rates that were 6.1–173.7-fold faster than those measured for Fe(VI) alone, depending on pH, CaSO₃ dosage, and the properties of organic contaminants. Many lines of evidence verified that neither SO₄•– nor •OH was the active species in the Fe(VI)–CaSO₃ process. The accelerating effect of CaSO₃ was ascribed to the direct generation of Fe(IV)/Fe(V) species from the reaction of Fe(VI) with soluble SO₃²– via one-electron steps as well as the indirect generation of Fe(IV)/Fe(V) species from the self-decay of Fe(VI) and Fe(VI) reaction with H₂O₂, which could be catalyzed by uncomplexed Fe(III). Besides, the Fe(VI)–CaSO₃ process exhibited satisfactory removal of organic contaminants in real water, and inorganic anions showed negligible effects on organic contaminant decomposition in this process. Thus, the Fe(VI)–CaSO₃ process with Fe(IV)/Fe(V) as reactive oxidants may be a promising method for abating various micropollutants in water treatment. |
| Author | Shao, Binbin Guan, Xiaohong Sun, Bo Dong, Hongyu |
| AuthorAffiliation | Department of Civil and Environmental Engineering Shanghai Institute of Pollution Control and Ecological Security The Hong Kong University of Science and Technology State Key Laboratory of Pollution Control and Resources Reuse, College of Environmental Science and Engineering Tongji University International Joint Research Center for Sustainable Urban Water System |
| AuthorAffiliation_xml | – name: Shanghai Institute of Pollution Control and Ecological Security – name: Department of Civil and Environmental Engineering – name: International Joint Research Center for Sustainable Urban Water System – name: State Key Laboratory of Pollution Control and Resources Reuse, College of Environmental Science and Engineering – name: The Hong Kong University of Science and Technology – name: Tongji University |
| Author_xml | – sequence: 1 givenname: Binbin surname: Shao fullname: Shao, Binbin organization: Shanghai Institute of Pollution Control and Ecological Security – sequence: 2 givenname: Hongyu surname: Dong fullname: Dong, Hongyu organization: Shanghai Institute of Pollution Control and Ecological Security – sequence: 3 givenname: Bo surname: Sun fullname: Sun, Bo organization: The Hong Kong University of Science and Technology – sequence: 4 givenname: Xiaohong orcidid: 0000-0001-5296-423X surname: Guan fullname: Guan, Xiaohong email: guanxh@tongji.edu.cn organization: Tongji University |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/30570262$$D View this record in MEDLINE/PubMed |
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| Snippet | Although the Fe(VI)–sulfite process has shown great potential for the rapid removal of organic contaminants, the major active oxidants (Fe(IV)/Fe(V) versus... Although the Fe(VI)-sulfite process has shown great potential for the rapid removal of organic contaminants, the major active oxidants (Fe(IV)/Fe(V) versus SO... Although the Fe(VI)–sulfite process has shown great potential for the rapid removal of organic contaminants, the major active oxidants (Fe(IV)/Fe(V) versus... Although the Fe(VI)-sulfite process has shown great potential for the rapid removal of organic contaminants, the major active oxidants (Fe(IV)/Fe(V) versus... |
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| Title | Role of Ferrate(IV) and Ferrate(V) in Activating Ferrate(VI) by Calcium Sulfite for Enhanced Oxidation of Organic Contaminants |
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