Effect of Modified Cardanol as Secondary Plasticizer on Thermal and Mechanical Properties of Soft Polyvinyl Chloride

This study represents the first attempt to prepare a novel cardanol-based plasticizer. Modified cardanol (MC, i.e., phosphorylated cardanol) containing nitrogen and phosphoric acid groups was synthesized and then incorporated into polyvinyl chloride (PVC) as the secondary plasticizer for partial sub...

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Published inACS omega Vol. 5; no. 28; pp. 17111 - 17117
Main Authors Ali, Muhammad, Lu, Yunhua, Ahmed, Saad, Khanal, Santosh, Xu, Shiai
Format Journal Article
LanguageEnglish
Published American Chemical Society 21.07.2020
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Abstract This study represents the first attempt to prepare a novel cardanol-based plasticizer. Modified cardanol (MC, i.e., phosphorylated cardanol) containing nitrogen and phosphoric acid groups was synthesized and then incorporated into polyvinyl chloride (PVC) as the secondary plasticizer for partial substitution of dioctyl phthalate (DOP). The molecular structure of MC was characterized by Fourier transform infrared spectroscopy, 1H nuclear magnetic resonance (NMR), and 31P NMR spectroscopy. The thermal degradation behavior, mechanical performance, and compatibility of MC were also investigated. The substitution of DOP with MC enables PVC blends to have higher thermal stability, tensile strength, and leaching resistance. The tensile strength is increased from 17.7 MPa for DOP/PVC blend (MC-0) to 25.7 MPa for MC/PVC blend (MC-4), and the elongation at break is increased from 256 to 432%, respectively. The microstructure of the tensile fractured surface was studied by scanning electron microscopy. The results show that the addition of MC allows PVC blends to have well-balanced properties of flexibility and strength and excellent migration resistance.
AbstractList This study represents the first attempt to prepare a novel cardanol-based plasticizer. Modified cardanol (MC, i.e., phosphorylated cardanol) containing nitrogen and phosphoric acid groups was synthesized and then incorporated into polyvinyl chloride (PVC) as the secondary plasticizer for partial substitution of dioctyl phthalate (DOP). The molecular structure of MC was characterized by Fourier transform infrared spectroscopy, 1 H nuclear magnetic resonance (NMR), and 31 P NMR spectroscopy. The thermal degradation behavior, mechanical performance, and compatibility of MC were also investigated. The substitution of DOP with MC enables PVC blends to have higher thermal stability, tensile strength, and leaching resistance. The tensile strength is increased from 17.7 MPa for DOP/PVC blend (MC-0) to 25.7 MPa for MC/PVC blend (MC-4), and the elongation at break is increased from 256 to 432%, respectively. The microstructure of the tensile fractured surface was studied by scanning electron microscopy. The results show that the addition of MC allows PVC blends to have well-balanced properties of flexibility and strength and excellent migration resistance.
This study represents the first attempt to prepare a novel cardanol-based plasticizer. Modified cardanol (MC, i.e., phosphorylated cardanol) containing nitrogen and phosphoric acid groups was synthesized and then incorporated into polyvinyl chloride (PVC) as the secondary plasticizer for partial substitution of dioctyl phthalate (DOP). The molecular structure of MC was characterized by Fourier transform infrared spectroscopy, 1H nuclear magnetic resonance (NMR), and 31P NMR spectroscopy. The thermal degradation behavior, mechanical performance, and compatibility of MC were also investigated. The substitution of DOP with MC enables PVC blends to have higher thermal stability, tensile strength, and leaching resistance. The tensile strength is increased from 17.7 MPa for DOP/PVC blend (MC-0) to 25.7 MPa for MC/PVC blend (MC-4), and the elongation at break is increased from 256 to 432%, respectively. The microstructure of the tensile fractured surface was studied by scanning electron microscopy. The results show that the addition of MC allows PVC blends to have well-balanced properties of flexibility and strength and excellent migration resistance.
Author Ali, Muhammad
Xu, Shiai
Lu, Yunhua
Ahmed, Saad
Khanal, Santosh
AuthorAffiliation School of Chemical Engineering
Qinghai University
Shanghai Key Laboratory for Advanced Polymeric Materials, School of Materials Science and Engineering
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Snippet This study represents the first attempt to prepare a novel cardanol-based plasticizer. Modified cardanol (MC, i.e., phosphorylated cardanol) containing...
This study represents the first attempt to prepare a novel cardanol-based plasticizer. Modified cardanol (MC, i.e., phosphorylated cardanol) containing...
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Title Effect of Modified Cardanol as Secondary Plasticizer on Thermal and Mechanical Properties of Soft Polyvinyl Chloride
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