Synthesis and Optical Properties of Lead-Free Cesium Tin Halide Perovskite Nanocrystals
Metal halide perovskite crystal structures have emerged as a class of optoelectronic materials, which combine the ease of solution processability with excellent optical absorption and emission qualities. Restricting the physical dimensions of the perovskite crystallites to a few nanometers can also...
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| Published in | Journal of the American Chemical Society Vol. 138; no. 9; pp. 2941 - 2944 |
|---|---|
| Main Authors | , , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
United States
American Chemical Society
09.03.2016
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| Subjects | |
| Online Access | Get full text |
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| Abstract | Metal halide perovskite crystal structures have emerged as a class of optoelectronic materials, which combine the ease of solution processability with excellent optical absorption and emission qualities. Restricting the physical dimensions of the perovskite crystallites to a few nanometers can also unlock spatial confinement effects, which allow large spectral tunability and high luminescence quantum yields at low excitation densities. However, the most promising perovskite structures rely on lead as a cationic species, thereby hindering commercial application. The replacement of lead with nontoxic alternatives such as tin has been demonstrated in bulk films, but not in spatially confined nanocrystals. Here, we synthesize CsSnX3 (X = Cl, Cl0.5Br0.5, Br, Br0.5I0.5, I) perovskite nanocrystals and provide evidence of their spectral tunability through both quantum confinement effects and control of the anionic composition. We show that luminescence from Sn-based perovskite nanocrystals occurs on pico- to nanosecond time scales via two spectrally distinct radiative decay processes, which we assign to band-to-band emission and radiative recombination at shallow intrinsic defect sites. |
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| AbstractList | Metal halide perovskite crystal structures have emerged as a class of optoelectronic materials, which combine the ease of solution processability with excellent optical absorption and emission qualities. Restricting the physical dimensions of the perovskite crystallites to a few nanometers can also unlock spatial confinement effects, which allow large spectral tunability and high luminescence quantum yields at low excitation densities. However, the most promising perovskite structures rely on lead as a cationic species, thereby hindering commercial application. The replacement of lead with nontoxic alternatives such as tin has been demonstrated in bulk films, but not in spatially confined nanocrystals. Here, we synthesize CsSnX3 (X = Cl, Cl0.5Br0.5, Br, Br0.5I0.5, I) perovskite nanocrystals and provide evidence of their spectral tunability through both quantum confinement effects and control of the anionic composition. We show that luminescence from Sn-based perovskite nanocrystals occurs on pico- to nanosecond time scales via two spectrally distinct radiative decay processes, which we assign to band-to-band emission and radiative recombination at shallow intrinsic defect sites. Metal halide perovskite crystal structures have emerged as a class of optoelectronic materials, which combine the ease of solution processability with excellent optical absorption and emission qualities. Restricting the physical dimensions of the perovskite crystallites to a few nanometers can also unlock spatial confinement effects, which allow large spectral tunability and high luminescence quantum yields at low excitation densities. However, the most promising perovskite structures rely on lead as a cationic species, thereby hindering commercial application. The replacement of lead with nontoxic alternatives such as tin has been demonstrated in bulk films, but not in spatially confined nanocrystals. Here, we synthesize CsSnX₃ (X = Cl, Cl₀.₅Br₀.₅, Br, Br₀.₅I₀.₅, I) perovskite nanocrystals and provide evidence of their spectral tunability through both quantum confinement effects and control of the anionic composition. We show that luminescence from Sn-based perovskite nanocrystals occurs on pico- to nanosecond time scales via two spectrally distinct radiative decay processes, which we assign to band-to-band emission and radiative recombination at shallow intrinsic defect sites. |
| Author | Tabachnyk, Maxim Brady, Ryan Richter, Johannes M Dutton, Siân E Greenham, Neil C Friend, Richard H Rao, Akshay Böhm, Marcus L Jellicoe, Tom C Glass, Hugh F. J Credgington, Dan |
| AuthorAffiliation | Cavendish Laboratory University of Cambridge |
| AuthorAffiliation_xml | – name: University of Cambridge – name: Cavendish Laboratory |
| Author_xml | – sequence: 1 givenname: Tom C surname: Jellicoe fullname: Jellicoe, Tom C – sequence: 2 givenname: Johannes M surname: Richter fullname: Richter, Johannes M – sequence: 3 givenname: Hugh F. J surname: Glass fullname: Glass, Hugh F. J – sequence: 4 givenname: Maxim surname: Tabachnyk fullname: Tabachnyk, Maxim – sequence: 5 givenname: Ryan surname: Brady fullname: Brady, Ryan – sequence: 6 givenname: Siân E surname: Dutton fullname: Dutton, Siân E – sequence: 7 givenname: Akshay surname: Rao fullname: Rao, Akshay – sequence: 8 givenname: Richard H surname: Friend fullname: Friend, Richard H – sequence: 9 givenname: Dan surname: Credgington fullname: Credgington, Dan – sequence: 10 givenname: Neil C surname: Greenham fullname: Greenham, Neil C – sequence: 11 givenname: Marcus L surname: Böhm fullname: Böhm, Marcus L email: mb842@cam.ac.uk |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/26901659$$D View this record in MEDLINE/PubMed |
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| Title | Synthesis and Optical Properties of Lead-Free Cesium Tin Halide Perovskite Nanocrystals |
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