Interface-Promoted Direct Oxidation of p‑Arsanilic Acid and Removal of Total Arsenic by the Coupling of Peroxymonosulfate and Mn-Fe-Mixed Oxide

As one of the extensively used feed additives in livestock and poultry breeding, p-arsanilic acid (p-ASA) has become an organoarsenic pollutant with great concern. For the efficient removal of p-ASA from water, the combination of chemical oxidation and adsorption is recognized as a promising process...

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Published inEnvironmental science & technology Vol. 55; no. 10; pp. 7063 - 7071
Main Authors Ke, Ming-Kun, Huang, Gui-Xiang, Mei, Shu-Chuan, Wang, Zhao-Hua, Zhang, Ying-Jie, Hua, Tian-Wei, Zheng, Li-Rong, Yu, Han-Qing
Format Journal Article
LanguageEnglish
Published United States American Chemical Society 18.05.2021
Subjects
Acidic oxides
Additives
adsorption
Animal husbandry
Arsenic
Coupling
Feed additives
Food additives
Livestock
Livestock breeding
Livestock feeds
Manganese
Oxidation
Oxidation process
Pollutant removal
Pollutants
Pollution abatement
Reactive oxygen species
Recyclability
Treatment and Resource Recovery
Water analysis
Water pollution
Water pollution control
Water sampling
Water treatment
direct oxidation
total arsenic
p-arsanilic acid
interface
Mn−Fe-mixed oxide
peroxymonosulfate
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Abstract As one of the extensively used feed additives in livestock and poultry breeding, p-arsanilic acid (p-ASA) has become an organoarsenic pollutant with great concern. For the efficient removal of p-ASA from water, the combination of chemical oxidation and adsorption is recognized as a promising process. Herein, hollow/porous Mn–Fe-mixed oxide (MnFeO) nanocubes were synthesized and used in coupling with peroxymonosulfate (PMS) to oxidize p-ASA and remove the total arsenic (As). Under acidic conditions, both p-ASA and total As could be completely removed in the PMS/MnFeO process and the overall performance was substantially better than that of the Mn/Fe monometallic system. More importantly, an interface-promoted direct oxidation mechanism was found in the p-ASA-involved PMS/MnFeO system. Rather than activate PMS to generate reactive oxygen species (i.e., SO4 ·–, ·OH, and 1O2), the MnFeO nanocubes first adsorbed p-ASA to form a ligand–oxide interface, which improved the oxidation of the adsorbed p-ASA by PMS and ultimately enhanced the removal of the total As. Such a direct oxidation process achieved selective oxidation of p-ASA and avoidance of severe interference from the commonly present constituents in real water samples. After facile elution with dilute alkali solution, the used MnFeO nanocubes exhibited superior recyclability in the repeated p-ASA removal experiments. Therefore, this work provides a promising approach for efficient abatement of phenylarsenical-caused water pollution based on the PMS/MnFeO oxidation process.
AbstractList As one of the extensively used feed additives in livestock and poultry breeding, p-arsanilic acid (p-ASA) has become an organoarsenic pollutant with great concern. For the efficient removal of p-ASA from water, the combination of chemical oxidation and adsorption is recognized as a promising process. Herein, hollow/porous Mn–Fe-mixed oxide (MnFeO) nanocubes were synthesized and used in coupling with peroxymonosulfate (PMS) to oxidize p-ASA and remove the total arsenic (As). Under acidic conditions, both p-ASA and total As could be completely removed in the PMS/MnFeO process and the overall performance was substantially better than that of the Mn/Fe monometallic system. More importantly, an interface-promoted direct oxidation mechanism was found in the p-ASA-involved PMS/MnFeO system. Rather than activate PMS to generate reactive oxygen species (i.e., SO4·–, ·OH, and 1O2), the MnFeO nanocubes first adsorbed p-ASA to form a ligand–oxide interface, which improved the oxidation of the adsorbed p-ASA by PMS and ultimately enhanced the removal of the total As. Such a direct oxidation process achieved selective oxidation of p-ASA and avoidance of severe interference from the commonly present constituents in real water samples. After facile elution with dilute alkali solution, the used MnFeO nanocubes exhibited superior recyclability in the repeated p-ASA removal experiments. Therefore, this work provides a promising approach for efficient abatement of phenylarsenical-caused water pollution based on the PMS/MnFeO oxidation process.
As one of the extensively used feed additives in livestock and poultry breeding, p-arsanilic acid (p-ASA) has become an organoarsenic pollutant with great concern. For the efficient removal of p-ASA from water, the combination of chemical oxidation and adsorption is recognized as a promising process. Herein, hollow/porous Mn–Fe-mixed oxide (MnFeO) nanocubes were synthesized and used in coupling with peroxymonosulfate (PMS) to oxidize p-ASA and remove the total arsenic (As). Under acidic conditions, both p-ASA and total As could be completely removed in the PMS/MnFeO process and the overall performance was substantially better than that of the Mn/Fe monometallic system. More importantly, an interface-promoted direct oxidation mechanism was found in the p-ASA-involved PMS/MnFeO system. Rather than activate PMS to generate reactive oxygen species (i.e., SO4 ·–, ·OH, and 1O2), the MnFeO nanocubes first adsorbed p-ASA to form a ligand–oxide interface, which improved the oxidation of the adsorbed p-ASA by PMS and ultimately enhanced the removal of the total As. Such a direct oxidation process achieved selective oxidation of p-ASA and avoidance of severe interference from the commonly present constituents in real water samples. After facile elution with dilute alkali solution, the used MnFeO nanocubes exhibited superior recyclability in the repeated p-ASA removal experiments. Therefore, this work provides a promising approach for efficient abatement of phenylarsenical-caused water pollution based on the PMS/MnFeO oxidation process.
As one of the extensively used feed additives in livestock and poultry breeding, -arsanilic acid ( -ASA) has become an organoarsenic pollutant with great concern. For the efficient removal of -ASA from water, the combination of chemical oxidation and adsorption is recognized as a promising process. Herein, hollow/porous Mn-Fe-mixed oxide (MnFeO) nanocubes were synthesized and used in coupling with peroxymonosulfate (PMS) to oxidize -ASA and remove the total arsenic (As). Under acidic conditions, both -ASA and total As could be completely removed in the PMS/MnFeO process and the overall performance was substantially better than that of the Mn/Fe monometallic system. More importantly, an interface-promoted direct oxidation mechanism was found in the -ASA-involved PMS/MnFeO system. Rather than activate PMS to generate reactive oxygen species (i.e., SO , ·OH, and O ), the MnFeO nanocubes first adsorbed -ASA to form a ligand-oxide interface, which improved the oxidation of the adsorbed -ASA by PMS and ultimately enhanced the removal of the total As. Such a direct oxidation process achieved selective oxidation of -ASA and avoidance of severe interference from the commonly present constituents in real water samples. After facile elution with dilute alkali solution, the used MnFeO nanocubes exhibited superior recyclability in the repeated -ASA removal experiments. Therefore, this work provides a promising approach for efficient abatement of phenylarsenical-caused water pollution based on the PMS/MnFeO oxidation process.
As one of the extensively used feed additives in livestock and poultry breeding, p-arsanilic acid (p-ASA) has become an organoarsenic pollutant with great concern. For the efficient removal of p-ASA from water, the combination of chemical oxidation and adsorption is recognized as a promising process. Herein, hollow/porous Mn-Fe-mixed oxide (MnFeO) nanocubes were synthesized and used in coupling with peroxymonosulfate (PMS) to oxidize p-ASA and remove the total arsenic (As). Under acidic conditions, both p-ASA and total As could be completely removed in the PMS/MnFeO process and the overall performance was substantially better than that of the Mn/Fe monometallic system. More importantly, an interface-promoted direct oxidation mechanism was found in the p-ASA-involved PMS/MnFeO system. Rather than activate PMS to generate reactive oxygen species (i.e., SO4·-, ·OH, and 1O2), the MnFeO nanocubes first adsorbed p-ASA to form a ligand-oxide interface, which improved the oxidation of the adsorbed p-ASA by PMS and ultimately enhanced the removal of the total As. Such a direct oxidation process achieved selective oxidation of p-ASA and avoidance of severe interference from the commonly present constituents in real water samples. After facile elution with dilute alkali solution, the used MnFeO nanocubes exhibited superior recyclability in the repeated p-ASA removal experiments. Therefore, this work provides a promising approach for efficient abatement of phenylarsenical-caused water pollution based on the PMS/MnFeO oxidation process.As one of the extensively used feed additives in livestock and poultry breeding, p-arsanilic acid (p-ASA) has become an organoarsenic pollutant with great concern. For the efficient removal of p-ASA from water, the combination of chemical oxidation and adsorption is recognized as a promising process. Herein, hollow/porous Mn-Fe-mixed oxide (MnFeO) nanocubes were synthesized and used in coupling with peroxymonosulfate (PMS) to oxidize p-ASA and remove the total arsenic (As). Under acidic conditions, both p-ASA and total As could be completely removed in the PMS/MnFeO process and the overall performance was substantially better than that of the Mn/Fe monometallic system. More importantly, an interface-promoted direct oxidation mechanism was found in the p-ASA-involved PMS/MnFeO system. Rather than activate PMS to generate reactive oxygen species (i.e., SO4·-, ·OH, and 1O2), the MnFeO nanocubes first adsorbed p-ASA to form a ligand-oxide interface, which improved the oxidation of the adsorbed p-ASA by PMS and ultimately enhanced the removal of the total As. Such a direct oxidation process achieved selective oxidation of p-ASA and avoidance of severe interference from the commonly present constituents in real water samples. After facile elution with dilute alkali solution, the used MnFeO nanocubes exhibited superior recyclability in the repeated p-ASA removal experiments. Therefore, this work provides a promising approach for efficient abatement of phenylarsenical-caused water pollution based on the PMS/MnFeO oxidation process.
As one of the extensively used feed additives in livestock and poultry breeding, p-arsanilic acid (p-ASA) has become an organoarsenic pollutant with great concern. For the efficient removal of p-ASA from water, the combination of chemical oxidation and adsorption is recognized as a promising process. Herein, hollow/porous Mn–Fe-mixed oxide (MnFeO) nanocubes were synthesized and used in coupling with peroxymonosulfate (PMS) to oxidize p-ASA and remove the total arsenic (As). Under acidic conditions, both p-ASA and total As could be completely removed in the PMS/MnFeO process and the overall performance was substantially better than that of the Mn/Fe monometallic system. More importantly, an interface-promoted direct oxidation mechanism was found in the p-ASA-involved PMS/MnFeO system. Rather than activate PMS to generate reactive oxygen species (i.e., SO₄·–, ·OH, and ¹O₂), the MnFeO nanocubes first adsorbed p-ASA to form a ligand–oxide interface, which improved the oxidation of the adsorbed p-ASA by PMS and ultimately enhanced the removal of the total As. Such a direct oxidation process achieved selective oxidation of p-ASA and avoidance of severe interference from the commonly present constituents in real water samples. After facile elution with dilute alkali solution, the used MnFeO nanocubes exhibited superior recyclability in the repeated p-ASA removal experiments. Therefore, this work provides a promising approach for efficient abatement of phenylarsenical-caused water pollution based on the PMS/MnFeO oxidation process.
Author Hua, Tian-Wei
Mei, Shu-Chuan
Zhang, Ying-Jie
Yu, Han-Qing
Huang, Gui-Xiang
Ke, Ming-Kun
Zheng, Li-Rong
Wang, Zhao-Hua
AuthorAffiliation Beijing Synchrotron Radiation Laboratory
CAS Key Laboratory of Urban Pollutant Conversion, Department of Environmental Science and Engineering
AuthorAffiliation_xml – name: CAS Key Laboratory of Urban Pollutant Conversion, Department of Environmental Science and Engineering
– name: Beijing Synchrotron Radiation Laboratory
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  givenname: Ming-Kun
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  fullname: Ke, Ming-Kun
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  givenname: Gui-Xiang
  surname: Huang
  fullname: Huang, Gui-Xiang
  email: gxhuang@ustc.edu.cn
  organization: CAS Key Laboratory of Urban Pollutant Conversion, Department of Environmental Science and Engineering
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  givenname: Shu-Chuan
  surname: Mei
  fullname: Mei, Shu-Chuan
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BackLink https://www.ncbi.nlm.nih.gov/pubmed/33961405$$D View this record in MEDLINE/PubMed
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total arsenic
p-arsanilic acid
interface
Mn−Fe-mixed oxide
peroxymonosulfate
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Snippet As one of the extensively used feed additives in livestock and poultry breeding, p-arsanilic acid (p-ASA) has become an organoarsenic pollutant with great...
As one of the extensively used feed additives in livestock and poultry breeding, -arsanilic acid ( -ASA) has become an organoarsenic pollutant with great...
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SubjectTerms Acidic oxides
Additives
adsorption
Animal husbandry
Arsenic
Coupling
Feed additives
Food additives
Livestock
Livestock breeding
Livestock feeds
Manganese
Oxidation
Oxidation process
Pollutant removal
Pollutants
Pollution abatement
Reactive oxygen species
Recyclability
Treatment and Resource Recovery
Water analysis
Water pollution
Water pollution control
Water sampling
Water treatment
Title Interface-Promoted Direct Oxidation of p‑Arsanilic Acid and Removal of Total Arsenic by the Coupling of Peroxymonosulfate and Mn-Fe-Mixed Oxide
URI http://dx.doi.org/10.1021/acs.est.1c00386
https://www.ncbi.nlm.nih.gov/pubmed/33961405
https://www.proquest.com/docview/2536546447
https://www.proquest.com/docview/2524362498
https://www.proquest.com/docview/2574311307
Volume 55
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