Regulating the Inner Helmholtz Plane for Stable Solid Electrolyte Interphase on Lithium Metal Anodes
The stability of a battery is strongly dependent on the feature of solid electrolyte interphase (SEI). The electrical double layer forms prior to the formation of SEI at the interface between the Li metal anode and the electrolyte. The fundamental understanding on the regulation of the SEI structure...
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| Published in | Journal of the American Chemical Society Vol. 141; no. 23; pp. 9422 - 9429 |
|---|---|
| Main Authors | , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
United States
American Chemical Society
12.06.2019
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| Subjects | |
| Online Access | Get full text |
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| Abstract | The stability of a battery is strongly dependent on the feature of solid electrolyte interphase (SEI). The electrical double layer forms prior to the formation of SEI at the interface between the Li metal anode and the electrolyte. The fundamental understanding on the regulation of the SEI structure and stability on Li surface through the structure of the electrical double layer is highly necessary for safe batteries. Herein, the interfacial chemistry of the SEI is correlated with the initial Li surface adsorption electrical double layer at the nanoscale through theoretical and experimental analysis. Under the premise of the constant solvation sheath structure of Li+ in bulk electrolyte, a trace amount of lithium nitrate (LiNO3) and copper fluoride (CuF2) were employed in electrolytes to build robust electric double layer structures on a Li metal surface. The distinct results were achieved with the initial competitive adsorption of bis(fluorosulfonyl)imide ion (FSI–), fluoride ion (F–), and nitrate ion (NO3 –) in the inner Helmholtz plane. As a result, Cu–NO3 – complexes are preferentially adsorbed and reduced to form the SEI. The modified Li metal electrode can achieve an average Coulombic efficiency of 99.5% over 500 cycles, enabling a long lifespan and high capacity retention of practical rechargeable batteries. The as-proposed mechanism bridges the gap between Li+ solvation and the adsorption about the electrode interface formation in a working battery. |
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| AbstractList | The stability of a battery is strongly dependent on the feature of solid electrolyte interphase (SEI). The electrical double layer forms prior to the formation of SEI at the interface between the Li metal anode and the electrolyte. The fundamental understanding on the regulation of the SEI structure and stability on Li surface through the structure of the electrical double layer is highly necessary for safe batteries. Herein, the interfacial chemistry of the SEI is correlated with the initial Li surface adsorption electrical double layer at the nanoscale through theoretical and experimental analysis. Under the premise of the constant solvation sheath structure of Li+ in bulk electrolyte, a trace amount of lithium nitrate (LiNO3) and copper fluoride (CuF2) were employed in electrolytes to build robust electric double layer structures on a Li metal surface. The distinct results were achieved with the initial competitive adsorption of bis(fluorosulfonyl)imide ion (FSI-), fluoride ion (F-), and nitrate ion (NO3-) in the inner Helmholtz plane. As a result, Cu-NO3- complexes are preferentially adsorbed and reduced to form the SEI. The modified Li metal electrode can achieve an average Coulombic efficiency of 99.5% over 500 cycles, enabling a long lifespan and high capacity retention of practical rechargeable batteries. The as-proposed mechanism bridges the gap between Li+ solvation and the adsorption about the electrode interface formation in a working battery.The stability of a battery is strongly dependent on the feature of solid electrolyte interphase (SEI). The electrical double layer forms prior to the formation of SEI at the interface between the Li metal anode and the electrolyte. The fundamental understanding on the regulation of the SEI structure and stability on Li surface through the structure of the electrical double layer is highly necessary for safe batteries. Herein, the interfacial chemistry of the SEI is correlated with the initial Li surface adsorption electrical double layer at the nanoscale through theoretical and experimental analysis. Under the premise of the constant solvation sheath structure of Li+ in bulk electrolyte, a trace amount of lithium nitrate (LiNO3) and copper fluoride (CuF2) were employed in electrolytes to build robust electric double layer structures on a Li metal surface. The distinct results were achieved with the initial competitive adsorption of bis(fluorosulfonyl)imide ion (FSI-), fluoride ion (F-), and nitrate ion (NO3-) in the inner Helmholtz plane. As a result, Cu-NO3- complexes are preferentially adsorbed and reduced to form the SEI. The modified Li metal electrode can achieve an average Coulombic efficiency of 99.5% over 500 cycles, enabling a long lifespan and high capacity retention of practical rechargeable batteries. The as-proposed mechanism bridges the gap between Li+ solvation and the adsorption about the electrode interface formation in a working battery. The stability of a battery is strongly dependent on the feature of solid electrolyte interphase (SEI). The electrical double layer forms prior to the formation of SEI at the interface between the Li metal anode and the electrolyte. The fundamental understanding on the regulation of the SEI structure and stability on Li surface through the structure of the electrical double layer is highly necessary for safe batteries. Herein, the interfacial chemistry of the SEI is correlated with the initial Li surface adsorption electrical double layer at the nanoscale through theoretical and experimental analysis. Under the premise of the constant solvation sheath structure of Li+ in bulk electrolyte, a trace amount of lithium nitrate (LiNO3) and copper fluoride (CuF2) were employed in electrolytes to build robust electric double layer structures on a Li metal surface. The distinct results were achieved with the initial competitive adsorption of bis(fluorosulfonyl)imide ion (FSI–), fluoride ion (F–), and nitrate ion (NO3 –) in the inner Helmholtz plane. As a result, Cu–NO3 – complexes are preferentially adsorbed and reduced to form the SEI. The modified Li metal electrode can achieve an average Coulombic efficiency of 99.5% over 500 cycles, enabling a long lifespan and high capacity retention of practical rechargeable batteries. The as-proposed mechanism bridges the gap between Li+ solvation and the adsorption about the electrode interface formation in a working battery. The stability of a battery is strongly dependent on the feature of solid electrolyte interphase (SEI). The electrical double layer forms prior to the formation of SEI at the interface between the Li metal anode and the electrolyte. The fundamental understanding on the regulation of the SEI structure and stability on Li surface through the structure of the electrical double layer is highly necessary for safe batteries. Herein, the interfacial chemistry of the SEI is correlated with the initial Li surface adsorption electrical double layer at the nanoscale through theoretical and experimental analysis. Under the premise of the constant solvation sheath structure of Li⁺ in bulk electrolyte, a trace amount of lithium nitrate (LiNO₃) and copper fluoride (CuF₂) were employed in electrolytes to build robust electric double layer structures on a Li metal surface. The distinct results were achieved with the initial competitive adsorption of bis(fluorosulfonyl)imide ion (FSI–), fluoride ion (F–), and nitrate ion (NO₃–) in the inner Helmholtz plane. As a result, Cu–NO₃– complexes are preferentially adsorbed and reduced to form the SEI. The modified Li metal electrode can achieve an average Coulombic efficiency of 99.5% over 500 cycles, enabling a long lifespan and high capacity retention of practical rechargeable batteries. The as-proposed mechanism bridges the gap between Li⁺ solvation and the adsorption about the electrode interface formation in a working battery. The stability of a battery is strongly dependent on the feature of solid electrolyte interphase (SEI). The electrical double layer forms prior to the formation of SEI at the interface between the Li metal anode and the electrolyte. The fundamental understanding on the regulation of the SEI structure and stability on Li surface through the structure of the electrical double layer is highly necessary for safe batteries. Herein, the interfacial chemistry of the SEI is correlated with the initial Li surface adsorption electrical double layer at the nanoscale through theoretical and experimental analysis. Under the premise of the constant solvation sheath structure of Li in bulk electrolyte, a trace amount of lithium nitrate (LiNO ) and copper fluoride (CuF ) were employed in electrolytes to build robust electric double layer structures on a Li metal surface. The distinct results were achieved with the initial competitive adsorption of bis(fluorosulfonyl)imide ion (FSI ), fluoride ion (F ), and nitrate ion (NO ) in the inner Helmholtz plane. As a result, Cu-NO complexes are preferentially adsorbed and reduced to form the SEI. The modified Li metal electrode can achieve an average Coulombic efficiency of 99.5% over 500 cycles, enabling a long lifespan and high capacity retention of practical rechargeable batteries. The as-proposed mechanism bridges the gap between Li solvation and the adsorption about the electrode interface formation in a working battery. |
| Author | Zhang, Xue-Qiang Li, Hao-Ran Xu, Rui Zhang, Qiang Huang, Jia-Qi Cheng, Xin-Bing Yan, Chong Chen, Xiang |
| AuthorAffiliation | School of Materials Science & Engineering Advanced Research Institute of Multidisciplinary Science Beijing Key Laboratory of Green Chemical Reaction Engineering and Technology, Department of Chemical Engineering |
| AuthorAffiliation_xml | – name: Advanced Research Institute of Multidisciplinary Science – name: School of Materials Science & Engineering – name: Beijing Key Laboratory of Green Chemical Reaction Engineering and Technology, Department of Chemical Engineering |
| Author_xml | – sequence: 1 givenname: Chong orcidid: 0000-0001-9521-4981 surname: Yan fullname: Yan, Chong organization: Advanced Research Institute of Multidisciplinary Science – sequence: 2 givenname: Hao-Ran surname: Li fullname: Li, Hao-Ran organization: Beijing Key Laboratory of Green Chemical Reaction Engineering and Technology, Department of Chemical Engineering – sequence: 3 givenname: Xiang orcidid: 0000-0002-7686-6308 surname: Chen fullname: Chen, Xiang organization: Beijing Key Laboratory of Green Chemical Reaction Engineering and Technology, Department of Chemical Engineering – sequence: 4 givenname: Xue-Qiang orcidid: 0000-0003-2856-1881 surname: Zhang fullname: Zhang, Xue-Qiang organization: Beijing Key Laboratory of Green Chemical Reaction Engineering and Technology, Department of Chemical Engineering – sequence: 5 givenname: Xin-Bing orcidid: 0000-0001-7567-1210 surname: Cheng fullname: Cheng, Xin-Bing organization: Beijing Key Laboratory of Green Chemical Reaction Engineering and Technology, Department of Chemical Engineering – sequence: 6 givenname: Rui surname: Xu fullname: Xu, Rui organization: Advanced Research Institute of Multidisciplinary Science – sequence: 7 givenname: Jia-Qi orcidid: 0000-0001-7394-9186 surname: Huang fullname: Huang, Jia-Qi email: jqhuang@bit.edu.cn organization: Advanced Research Institute of Multidisciplinary Science – sequence: 8 givenname: Qiang orcidid: 0000-0002-3929-1541 surname: Zhang fullname: Zhang, Qiang organization: Beijing Key Laboratory of Green Chemical Reaction Engineering and Technology, Department of Chemical Engineering |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/31117672$$D View this record in MEDLINE/PubMed |
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| Snippet | The stability of a battery is strongly dependent on the feature of solid electrolyte interphase (SEI). The electrical double layer forms prior to the formation... |
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| SubjectTerms | adsorption anodes batteries copper electrolytes fluorides lithium longevity nitrates solvation |
| Title | Regulating the Inner Helmholtz Plane for Stable Solid Electrolyte Interphase on Lithium Metal Anodes |
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