Residue Dynamic of Pyrimorph on Tomatoes, Cucumbers and Soil under Greenhouse Trails
A modified QuEChERS method for analysis of pyrimorph residue in tomatoes, cucumbers and soil was developed and validated. Residue dynamics and final residues in greenhouse vegetables and soil were studied. At fortification levels of 0.05, 0.1 and 1 mg kg⁻¹ in tomatoes, cucumbers and soil, the method...
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Published in | Bulletin of environmental contamination and toxicology Vol. 86; no. 3; pp. 326 - 330 |
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Main Authors | , , , , , , |
Format | Journal Article |
Language | English |
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01.03.2011
Springer-Verlag Springer Nature B.V |
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Abstract | A modified QuEChERS method for analysis of pyrimorph residue in tomatoes, cucumbers and soil was developed and validated. Residue dynamics and final residues in greenhouse vegetables and soil were studied. At fortification levels of 0.05, 0.1 and 1 mg kg⁻¹ in tomatoes, cucumbers and soil, the method got recoveries ranged from 86.1% to 99.3% with relative standard deviations of 1.0%-7.7%, in agreement with directives for method validation in residue analysis. The limit of determination in tomatoes, cucumbers and soil was 0.05 mg kg⁻¹. The proposed method was successfully employed for the determination of pyrimorph residue levels and dissipation rates in vegetables and soil. At six experimental sites, pyrimorph residues in tomatoes and cucumbers showed relatively fast dissipation rates, with half-lives of 5.8-7.7 days and 5.7-7.1 days respectively. Half-lives of pyrimorph in soil were 8.5-11.0 days. The final residues of pyrimorph in tomatoes ranged from 0.19 to 3.66 mg kg⁻¹, 0.18 to 4.35 mg kg⁻¹ in cucumbers and 0.22 to 16.5 mg kg⁻¹ in soil with pre-harvest interval of 3-7 days. 5 mg kg⁻¹ was proposed as the MRL of pyrimorph in tomatoes and cucumbers. |
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AbstractList | A modified QuEChERS method for analysis of pyrimorph residue in tomatoes, cucumbers and soil was developed and validated. Residue dynamics and final residues in greenhouse vegetables and soil were studied. At fortification levels of 0.05, 0.1 and 1 mg kg^sup -1^ in tomatoes, cucumbers and soil, the method got recoveries ranged from 86.1% to 99.3% with relative standard deviations of 1.0%-7.7%, in agreement with directives for method validation in residue analysis. The limit of determination in tomatoes, cucumbers and soil was 0.05 mg kg^sup -1^. The proposed method was successfully employed for the determination of pyrimorph residue levels and dissipation rates in vegetables and soil. At six experimental sites, pyrimorph residues in tomatoes and cucumbers showed relatively fast dissipation rates, with half-lives of 5.8-7.7 days and 5.7-7.1 days respectively. Half-lives of pyrimorph in soil were 8.5-11.0 days. The final residues of pyrimorph in tomatoes ranged from 0.19 to 3.66 mg kg^sup -1^, 0.18 to 4.35 mg kg^sup -1^ in cucumbers and 0.22 to 16.5 mg kg^sup -1^ in soil with pre-harvest interval of 3-7 days. 5 mg kg^sup -1^ was proposed as the MRL of pyrimorph in tomatoes and cucumbers.[PUBLICATION ABSTRACT] A modified QuEChERS method for analysis of pyrimorph residue in tomatoes, cucumbers and soil was developed and validated. Residue dynamics and final residues in greenhouse vegetables and soil were studied. At fortification levels of 0.05, 0.1 and 1 mg kg(-1) in tomatoes, cucumbers and soil, the method got recoveries ranged from 86.1% to 99.3% with relative standard deviations of 1.0%-7.7%, in agreement with directives for method validation in residue analysis. The limit of determination in tomatoes, cucumbers and soil was 0.05 mg kg(-1). The proposed method was successfully employed for the determination of pyrimorph residue levels and dissipation rates in vegetables and soil. At six experimental sites, pyrimorph residues in tomatoes and cucumbers showed relatively fast dissipation rates, with half-lives of 5.8-7.7 days and 5.7-7.1 days respectively. Half-lives of pyrimorph in soil were 8.5-11.0 days. The final residues of pyrimorph in tomatoes ranged from 0.19 to 3.66 mg kg(-1), 0.18 to 4.35 mg kg(-1) in cucumbers and 0.22 to 16.5 mg kg(-1) in soil with pre-harvest interval of 3-7 days. 5 mg kg(-1) was proposed as the MRL of pyrimorph in tomatoes and cucumbers. A modified QuEChERS method for analysis of pyrimorph residue in tomatoes, cucumbers and soil was developed and validated. Residue dynamics and final residues in greenhouse vegetables and soil were studied. At fortification levels of 0.05, 0.1 and 1mgkg super(-1) in tomatoes, cucumbers and soil, the method got recoveries ranged from 86.1% to 99.3% with relative standard deviations of 1.0%-7.7%, in agreement with directives for method validation in residue analysis. The limit of determination in tomatoes, cucumbers and soil was 0.05mgkg super(-1). The proposed method was successfully employed for the determination of pyrimorph residue levels and dissipation rates in vegetables and soil. At six experimental sites, pyrimorph residues in tomatoes and cucumbers showed relatively fast dissipation rates, with half-lives of 5.8-7.7days and 5.7-7.1days respectively. Half-lives of pyrimorph in soil were 8.5-11.0days. The final residues of pyrimorph in tomatoes ranged from 0.19 to 3.66mg kg super(-1), 0.18 to 4.35mg kg super(-1) in cucumbers and 0.22 to 16.5mg kg super(-1) in soil with pre-harvest interval of 3-7days. 5mgkg super(-1) was proposed as the MRL of pyrimorph in tomatoes and cucumbers. A modified QuEChERS method for analysis of pyrimorph residue in tomatoes, cucumbers and soil was developed and validated. Residue dynamics and final residues in greenhouse vegetables and soil were studied. At fortification levels of 0.05, 0.1 and 1 mg kg −1 in tomatoes, cucumbers and soil, the method got recoveries ranged from 86.1% to 99.3% with relative standard deviations of 1.0%–7.7%, in agreement with directives for method validation in residue analysis. The limit of determination in tomatoes, cucumbers and soil was 0.05 mg kg −1 . The proposed method was successfully employed for the determination of pyrimorph residue levels and dissipation rates in vegetables and soil. At six experimental sites, pyrimorph residues in tomatoes and cucumbers showed relatively fast dissipation rates, with half-lives of 5.8–7.7 days and 5.7–7.1 days respectively. Half-lives of pyrimorph in soil were 8.5–11.0 days. The final residues of pyrimorph in tomatoes ranged from 0.19 to 3.66 mg kg −1 , 0.18 to 4.35 mg kg −1 in cucumbers and 0.22 to 16.5 mg kg −1 in soil with pre-harvest interval of 3–7 days. 5 mg kg −1 was proposed as the MRL of pyrimorph in tomatoes and cucumbers. A modified QuEChERS method for analysis of pyrimorph residue in tomatoes, cucumbers and soil was developed and validated. Residue dynamics and final residues in greenhouse vegetables and soil were studied. At fortification levels of 0.05, 0.1 and 1 mg kg⁻¹ in tomatoes, cucumbers and soil, the method got recoveries ranged from 86.1% to 99.3% with relative standard deviations of 1.0%-7.7%, in agreement with directives for method validation in residue analysis. The limit of determination in tomatoes, cucumbers and soil was 0.05 mg kg⁻¹. The proposed method was successfully employed for the determination of pyrimorph residue levels and dissipation rates in vegetables and soil. At six experimental sites, pyrimorph residues in tomatoes and cucumbers showed relatively fast dissipation rates, with half-lives of 5.8-7.7 days and 5.7-7.1 days respectively. Half-lives of pyrimorph in soil were 8.5-11.0 days. The final residues of pyrimorph in tomatoes ranged from 0.19 to 3.66 mg kg⁻¹, 0.18 to 4.35 mg kg⁻¹ in cucumbers and 0.22 to 16.5 mg kg⁻¹ in soil with pre-harvest interval of 3-7 days. 5 mg kg⁻¹ was proposed as the MRL of pyrimorph in tomatoes and cucumbers. |
Author | Li, Xuesheng Qin, Zhaohai Jiang, Yaping Li, Nan Zhao, Lianlian Wang, Jing Pan, Canping |
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BackLink | https://www.ncbi.nlm.nih.gov/pubmed/21298253$$D View this record in MEDLINE/PubMed |
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CitedBy_id | crossref_primary_10_1007_s00128_012_0746_0 crossref_primary_10_1039_D1AY01248G crossref_primary_10_1016_j_ejsobi_2013_02_005 crossref_primary_10_1016_j_jfca_2024_106303 crossref_primary_10_1002_jssc_201200087 crossref_primary_10_3390_molecules27134323 crossref_primary_10_1002_clen_201300140 crossref_primary_10_1002_jsfa_10350 crossref_primary_10_1007_s00128_012_0850_1 crossref_primary_10_1007_s12161_020_01956_4 crossref_primary_10_1021_jf405555w |
Cites_doi | 10.1016/j.talanta.2007.11.031 10.1016/j.foodcont.2007.09.002 10.1002/jssc.200600410 10.1016/j.aca.2008.03.031 10.1007/s00216-006-0891-6 10.1093/jaoac/88.2.595 |
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SubjectTerms | Acrylamides - analysis Acrylamides - chemistry Agricultural production Aquatic Pollution Cucumbers Cucumis sativus - chemistry Earth and Environmental Science Ecotoxicology Environment Environmental Chemistry Environmental Health Fungicides, Industrial - analysis Fungicides, Industrial - chemistry Greenhouses Half-Life Lycopersicon esculentum Lycopersicon esculentum - chemistry Morpholines - analysis Morpholines - chemistry Pesticide Residues - analysis Pesticide Residues - chemistry Pesticides Pollution Pyrimorph Residue dynamics Soil - chemistry Soil contamination Soil Pollutants - analysis Soil Pollutants - chemistry Soil Science & Conservation Tomatoes Toxicity Waste Water Technology Water Management Water Pollution Control |
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Title | Residue Dynamic of Pyrimorph on Tomatoes, Cucumbers and Soil under Greenhouse Trails |
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