Spontaneous Formation of Fluorescent Nanofibers from Self-Assembly of Low-Molecular-Weight Coumarin Derivatives in Water
A solvent-exchange process was applied to three fluorescent dyes belonging to the 2-benzimidazolyl-7-diethylaminocoumarin series (namely Coumarin 7 (1), Coumarin 30 (2), and one of their derivatives bearing a butyl chain (3)). The three compounds only differ by the substitution of the nitrogen atom...
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Published in | Langmuir Vol. 24; no. 6; pp. 2671 - 2679 |
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Main Authors | , , , |
Format | Journal Article |
Language | English |
Published |
Washington, DC
American Chemical Society
18.03.2008
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Abstract | A solvent-exchange process was applied to three fluorescent dyes belonging to the 2-benzimidazolyl-7-diethylaminocoumarin series (namely Coumarin 7 (1), Coumarin 30 (2), and one of their derivatives bearing a butyl chain (3)). The three compounds only differ by the substitution of the nitrogen atom of the benzimidazolyl group. They were first dissolved in acetone and then suddenly placed in an aqueous environment where they generated molecular assemblies. The size and shape of the latter were studied by fluorescence microscopy and transmission and scanning electron microscopy. It appeared that 1 gave aggregates and flat microcrystals that evolved toward elongated structures. 2 formed straight nanofibers that are 10−20 μm long and exhibit a crystal structure. 3 gave short fibers (1 μm × 25 nm), which finally arrange into entangled solid nanofibers. The formation of fibers arising from low-molecular-weight molecules was particularly interesting. The optical properties of the free-standing particles in suspension were analyzed and compared to those of highly dilute dyes, with the aim to get additional information about the dye arrangement in the nanostructures. |
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AbstractList | A solvent-exchange process was applied to three fluorescent dyes belonging to the 2-benzimidazolyl-7-diethylaminocoumarin series (namely Coumarin 7 (1), Coumarin 30 (2), and one of their derivatives bearing a butyl chain (3)). The three compounds only differ by the substitution of the nitrogen atom of the benzimidazolyl group. They were first dissolved in acetone and then suddenly placed in an aqueous environment where they generated molecular assemblies. The size and shape of the latter were studied by fluorescence microscopy and transmission and scanning electron microscopy. It appeared that 1 gave aggregates and flat microcrystals that evolved toward elongated structures. 2 formed straight nanofibers that are 10-20 microm long and exhibit a crystal structure. 3 gave short fibers (1 micromx25 nm), which finally arrange into entangled solid nanofibers. The formation of fibers arising from low-molecular-weight molecules was particularly interesting. The optical properties of the free-standing particles in suspension were analyzed and compared to those of highly dilute dyes, with the aim to get additional information about the dye arrangement in the nanostructures. A solvent-exchange process was applied to three fluorescent dyes belonging to the 2-benzimidazolyl-7-diethylaminocoumarin series (namely Coumarin 7 (1), Coumarin 30 (2), and one of their derivatives bearing a butyl chain (3)). The three compounds only differ by the substitution of the nitrogen atom of the benzimidazolyl group. They were first dissolved in acetone and then suddenly placed in an aqueous environment where they generated molecular assemblies. The size and shape of the latter were studied by fluorescence microscopy and transmission and scanning electron microscopy. It appeared that 1 gave aggregates and flat microcrystals that evolved toward elongated structures. 2 formed straight nanofibers that are 10−20 μm long and exhibit a crystal structure. 3 gave short fibers (1 μm × 25 nm), which finally arrange into entangled solid nanofibers. The formation of fibers arising from low-molecular-weight molecules was particularly interesting. The optical properties of the free-standing particles in suspension were analyzed and compared to those of highly dilute dyes, with the aim to get additional information about the dye arrangement in the nanostructures. |
Author | Lamère, Jean-François Fery-Forgues, Suzanne Mille, Marion Rodrigues, Fernanda |
Author_xml | – sequence: 1 givenname: Marion surname: Mille fullname: Mille, Marion – sequence: 2 givenname: Jean-François surname: Lamère fullname: Lamère, Jean-François – sequence: 3 givenname: Fernanda surname: Rodrigues fullname: Rodrigues, Fernanda – sequence: 4 givenname: Suzanne surname: Fery-Forgues fullname: Fery-Forgues, Suzanne |
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Keywords | Water Self assembly Dyes Shape Fiber Nanofiber Solid Substitution Molecular assembly Optical properties Structure Molecular mass Scanning electron microscopy Crystals Nanostructure Particle suspension Nitrogen Ketone Coumarin Transmission electron microscopy Environment Aggregate Microcrystal Fluorescence microscopy Acetone |
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Snippet | A solvent-exchange process was applied to three fluorescent dyes belonging to the 2-benzimidazolyl-7-diethylaminocoumarin series (namely Coumarin 7 (1),... |
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SubjectTerms | Chemistry Colloidal state and disperse state Coumarins - chemistry Exact sciences and technology Fluorescent Dyes - chemistry General and physical chemistry Microscopy, Electron, Transmission - methods Molecular Structure Molecular Weight Nanoparticles - chemistry Particle Size Physical and chemical studies. Granulometry. Electrokinetic phenomena Spectrometry, Fluorescence - methods Spectrophotometry, Ultraviolet - methods Surface physical chemistry Surface Properties Water - chemistry |
Title | Spontaneous Formation of Fluorescent Nanofibers from Self-Assembly of Low-Molecular-Weight Coumarin Derivatives in Water |
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