Spontaneous Phase and Morphology Transformations of Anodized Titania Nanotubes Induced by Water at Room Temperature
We report a spontaneous phase transformation of titania nanotubes induced by water at room temperature, which enables the as-anodized amorphous nanotubes to be crystallized into anatase mesoporous nanowires without any other post-treatments. These mesoporous TiO2 nanomaterials have a markedly improv...
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| Published in | Nano letters Vol. 11; no. 9; pp. 3649 - 3655 |
|---|---|
| Main Authors | , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Washington, DC
American Chemical Society
14.09.2011
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| Subjects | |
| Online Access | Get full text |
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| Abstract | We report a spontaneous phase transformation of titania nanotubes induced by water at room temperature, which enables the as-anodized amorphous nanotubes to be crystallized into anatase mesoporous nanowires without any other post-treatments. These mesoporous TiO2 nanomaterials have a markedly improved surface area, about 5.5 times than that of the as-anodized TiO2 nanotubes, resulting in a pronounced enhanced photocatalytic activity. The present approach not only allows a flexible control over the morphology of TiO2 nanostructures but can fundamentally eliminate the need for high temperature operations for crystallizing amorphous TiO2. |
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| AbstractList | We report a spontaneous phase transformation of titania nanotubes induced by water at room temperature, which enables the as-anodized amorphous nanotubes to be crystallized into anatase mesoporous nanowires without any other post-treatments. These mesoporous TiO2 nanomaterials have a markedly improved surface area, about 5.5 times than that of the as-anodized TiO2 nanotubes, resulting in a pronounced enhanced photocatalytic activity. The present approach not only allows a flexible control over the morphology of TiO2 nanostructures but can fundamentally eliminate the need for high temperature operations for crystallizing amorphous TiO2. We report a spontaneous phase transformation of titania nanotubes induced by water at room temperature, which enables the as-anodized amorphous nanotubes to be crystallized into anatase mesoporous nanowires without any other post-treatments. These mesoporous TiO sub(2) nanomaterials have a markedly improved surface area, about 5.5 times than that of the as-anodized TiO sub(2) nanotubes, resulting in a pronounced enhanced photocatalytic activity. The present approach not only allows a flexible control over the morphology of TiO sub(2) nanostructures but can fundamentally eliminate the need for high temperature operations for crystallizing amorphous TiO sub(2). We report a spontaneous phase transformation of titania nanotubes induced by water at room temperature, which enables the as-anodized amorphous nanotubes to be crystallized into anatase mesoporous nanowires without any other post-treatments. These mesoporous TiO(2) nanomaterials have a markedly improved surface area, about 5.5 times than that of the as-anodized TiO(2) nanotubes, resulting in a pronounced enhanced photocatalytic activity. The present approach not only allows a flexible control over the morphology of TiO(2) nanostructures but can fundamentally eliminate the need for high temperature operations for crystallizing amorphous TiO(2).We report a spontaneous phase transformation of titania nanotubes induced by water at room temperature, which enables the as-anodized amorphous nanotubes to be crystallized into anatase mesoporous nanowires without any other post-treatments. These mesoporous TiO(2) nanomaterials have a markedly improved surface area, about 5.5 times than that of the as-anodized TiO(2) nanotubes, resulting in a pronounced enhanced photocatalytic activity. The present approach not only allows a flexible control over the morphology of TiO(2) nanostructures but can fundamentally eliminate the need for high temperature operations for crystallizing amorphous TiO(2). We report a spontaneous phase transformation of titania nanotubes induced by water at room temperature, which enables the as-anodized amorphous nanotubes to be crystallized into anatase mesoporous nanowires without any other post-treatments. These mesoporous TiO(2) nanomaterials have a markedly improved surface area, about 5.5 times than that of the as-anodized TiO(2) nanotubes, resulting in a pronounced enhanced photocatalytic activity. The present approach not only allows a flexible control over the morphology of TiO(2) nanostructures but can fundamentally eliminate the need for high temperature operations for crystallizing amorphous TiO(2). |
| Author | Pippel, Eckhard Tao, Kun Wang, Daoai Domen, Kazunari Zhang, Fuxiang Liu, Lifeng |
| AuthorAffiliation | International Iberian Nanotechnology Laboratory Max Planck Institute of Microstructure Physics The University of Tokyo |
| AuthorAffiliation_xml | – name: Max Planck Institute of Microstructure Physics – name: International Iberian Nanotechnology Laboratory – name: The University of Tokyo |
| Author_xml | – sequence: 1 givenname: Daoai surname: Wang fullname: Wang, Daoai email: dwang@chemsys.t.u-tokyo.ac.jp, lifeng.liu@inl.int – sequence: 2 givenname: Lifeng surname: Liu fullname: Liu, Lifeng email: dwang@chemsys.t.u-tokyo.ac.jp, lifeng.liu@inl.int – sequence: 3 givenname: Fuxiang surname: Zhang fullname: Zhang, Fuxiang – sequence: 4 givenname: Kun surname: Tao fullname: Tao, Kun – sequence: 5 givenname: Eckhard surname: Pippel fullname: Pippel, Eckhard – sequence: 6 givenname: Kazunari surname: Domen fullname: Domen, Kazunari |
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| Keywords | mesoporous structures TiO2 nanotubes photocatalyst phase transformation Anatase Phase transformations Porous materials Photocatalysis Nanotubes Nanostructures Mesoporosity Morphology Nanowires Surface area Titanium oxide Catalyst activity Nanostructured materials |
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| Snippet | We report a spontaneous phase transformation of titania nanotubes induced by water at room temperature, which enables the as-anodized amorphous nanotubes to be... |
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| SubjectTerms | Anatase Condensed matter: structure, mechanical and thermal properties Cross-disciplinary physics: materials science; rheology Crystallization Equations of state, phase equilibria, and phase transitions Exact sciences and technology Low-dimensional structures (superlattices, quantum well structures, multilayers): structure, and nonelectronic properties Materials science Morphology Nanoscale materials and structures: fabrication and characterization Nanostructure Nanotubes Nanowires Phase transformations Physics Quantum wires Specific phase transitions Spontaneous Structural transitions in nanoscale materials Surfaces and interfaces; thin films and whiskers (structure and nonelectronic properties) Titanium dioxide |
| Title | Spontaneous Phase and Morphology Transformations of Anodized Titania Nanotubes Induced by Water at Room Temperature |
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