Transparent and High Gas Barrier Films of Cellulose Nanofibers Prepared by TEMPO-Mediated Oxidation
Softwood and hardwood celluloses were oxidized by 2,2,6,6-tetramethylpiperidine-1-oxyl radical (TEMPO)-mediated oxidation. The TEMPO-oxidized cellulose fibers were converted to transparent dispersions in water, which consisted of individual nanofibers 3−4 nm in width. Films were then prepared from t...
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| Published in | Biomacromolecules Vol. 10; no. 1; pp. 162 - 165 |
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| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Washington, DC
American Chemical Society
12.01.2009
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| Subjects | |
| Online Access | Get full text |
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| Abstract | Softwood and hardwood celluloses were oxidized by 2,2,6,6-tetramethylpiperidine-1-oxyl radical (TEMPO)-mediated oxidation. The TEMPO-oxidized cellulose fibers were converted to transparent dispersions in water, which consisted of individual nanofibers 3−4 nm in width. Films were then prepared from the TEMPO-oxidized cellulose nanofibers (TOCN) and characterized from various aspects. AFM images showed that the TOCN film surface consisted of randomly assembled cellulose nanofibers. The TOCN films prepared from softwood cellulose were transparent and flexible and had extremely low coefficients of thermal expansion caused by high crystallinity of TOCN. Moreover, oxygen permeability of a polylactic acid (PLA) film drastically decreased to about 1/750 by forming a thin TOCN layer on the PLA film. Hydrophobization of the originally hydrophilic TOCN films was achieved by treatment with alkylketene dimer. These unique characteristics of the TOCN films are promising for potential applications in some high-tech materials. |
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| AbstractList | Softwood and hardwood celluloses were oxidized by 2,2,6,6-tetramethylpiperidine-1-oxyl radical (TEMPO)-mediated oxidation. The TEMPO-oxidized cellulose fibers were converted to transparent dispersions in water, which consisted of individual nanofibers 3−4 nm in width. Films were then prepared from the TEMPO-oxidized cellulose nanofibers (TOCN) and characterized from various aspects. AFM images showed that the TOCN film surface consisted of randomly assembled cellulose nanofibers. The TOCN films prepared from softwood cellulose were transparent and flexible and had extremely low coefficients of thermal expansion caused by high crystallinity of TOCN. Moreover, oxygen permeability of a polylactic acid (PLA) film drastically decreased to about 1/750 by forming a thin TOCN layer on the PLA film. Hydrophobization of the originally hydrophilic TOCN films was achieved by treatment with alkylketene dimer. These unique characteristics of the TOCN films are promising for potential applications in some high-tech materials. Softwood and hardwood celluloses were oxidized by 2,2,6,6-tetramethylpiperidine-1-oxyl radical (TEMPO)-mediated oxidation. The TEMPO-oxidized cellulose fibers were converted to transparent dispersions in water, which consisted of individual nanofibers 3-4 nm in width. Films were then prepared from the TEMPO-oxidized cellulose nanofibers (TOCN) and characterized from various aspects. AFM images showed that the TOCN film surface consisted of randomly assembled cellulose nanofibers. The TOCN films prepared from softwood cellulose were transparent and flexible and had extremely low coefficients of thermal expansion caused by high crystallinity of TOCN. Moreover, oxygen permeability of a polylactic acid (PLA) film drastically decreased to about 1/750 by forming a thin TOCN layer on the PLA film. Hydrophobization of the originally hydrophilic TOCN films was achieved by treatment with alkylketene dimer. These unique characteristics of the TOCN films are promising for potential applications in some high-tech materials. |
| Author | Iwata, Tadahisa Saito, Tsuguyuki Isogai, Akira Fukuzumi, Hayaka Kumamoto, Yoshiaki |
| Author_xml | – sequence: 1 givenname: Hayaka surname: Fukuzumi fullname: Fukuzumi, Hayaka – sequence: 2 givenname: Tsuguyuki surname: Saito fullname: Saito, Tsuguyuki – sequence: 3 givenname: Tadahisa surname: Iwata fullname: Iwata, Tadahisa – sequence: 4 givenname: Yoshiaki surname: Kumamoto fullname: Kumamoto, Yoshiaki – sequence: 5 givenname: Akira surname: Isogai fullname: Isogai, Akira email: aisogai@mail.ecc.u-tokyo.ac.jp |
| BackLink | http://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=21036157$$DView record in Pascal Francis https://www.ncbi.nlm.nih.gov/pubmed/19055320$$D View this record in MEDLINE/PubMed |
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| Keywords | Oxygen Transparency Transport properties Nitroxyl Film Hydrophobization Cellulose Mechanical properties Nanofiber Experimental study Surface treatment Sodium Hypochlorites Gas permeability Chemical modification Wettability Optical properties Morphology Preparation Cellulose derivatives Piperidine derivatives Surface properties Polyacid Oxidation Heterogeneous reaction |
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| Title | Transparent and High Gas Barrier Films of Cellulose Nanofibers Prepared by TEMPO-Mediated Oxidation |
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