Transitional Adsorption and Partition of Nonpolar and Polar Aromatic Contaminants by Biochars of Pine Needles with Different Pyrolytic Temperatures

The combined adsorption and partition effects of biochars with varying fractions of noncarbonized organic matter have not been clearly defined. Biochars, produced by pyrolysis of pine needles at different temperatures (100−700 °C, referred as P100−P700), were characterized by elemental analysis, BET...

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Published in	Environmental science & technology Vol. 42; no. 14; pp. 5137 - 5143
Main Authors	Chen, Baoliang, Zhou, Dandan, Zhu, Lizhong
Format	Journal Article
Language	English
Published	Washington, DC American Chemical Society 15.07.2008
Subjects	Adsorption Applied sciences Biomass Chemical contaminants Environmental Processes Exact sciences and technology Hydrocarbons, Aromatic - chemistry Incineration Molecules Particulate Matter - chemistry Pinus - anatomy & histology Pinus - chemistry Plant Leaves - chemistry Pollution Sorption Spectroscopy, Fourier Transform Infrared Temperature Elementary analysis Pyrolysis Organic matter Chemical analysis Hydrocarbon Aliphatic compound Pollutant behavior Adsorption isotherm Biological indicator Sorption Pollution Adsorption Surface properties Polarity Aromatic compound Phase partition Porosity Sorbent Organic compounds Low temperature
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Abstract	The combined adsorption and partition effects of biochars with varying fractions of noncarbonized organic matter have not been clearly defined. Biochars, produced by pyrolysis of pine needles at different temperatures (100−700 °C, referred as P100−P700), were characterized by elemental analysis, BET-N2 surface areas and FTIR. Sorption isotherms of naphthalene, nitrobenzene, and m-dinitrobenzene from water to the biochars were compared. Sorption parameters (N and logK f) are linearly related to sorbent aromaticities, which increase with the pyrolytic temperature. Sorption mechanisms of biochars are evolved from partitioning-dominant at low pyrolytic temperatures to adsorption-dominant at higher pyrolytic temperatures. The quantitative contributions of adsorption and partition are determined by the relative carbonized and noncarbonized fractions and their surface and bulk properties. The partition of P100−P300 biochars originates from an amorphous aliphatic fraction, which is enhanced with a reduction of the substrate polarity; for P400−P600, the partition occurs with a condensed aromatic core that diminishes with a further reduction of the polarity. Simultaneously, the adsorption component exhibits a transition from a polarity-selective (P200−P400) to a porosity-selective (P500−P600) process, and displays no selectivity with P700 and AC in which the adsorptive saturation capacities are comparable to predicted values based on the monolayer surface coverage of molecule.
AbstractList	The combined adsorption and partition effects of biochars with varying fractions of noncarbonized organic matter have not been clearly defined. Biochars, produced by pyrolysis of pine needles at different temperatures (100−700 °C, referred as P100−P700), were characterized by elemental analysis, BET-N2 surface areas and FTIR. Sorption isotherms of naphthalene, nitrobenzene, and m-dinitrobenzene from water to the biochars were compared. Sorption parameters (N and logK f) are linearly related to sorbent aromaticities, which increase with the pyrolytic temperature. Sorption mechanisms of biochars are evolved from partitioning-dominant at low pyrolytic temperatures to adsorption-dominant at higher pyrolytic temperatures. The quantitative contributions of adsorption and partition are determined by the relative carbonized and noncarbonized fractions and their surface and bulk properties. The partition of P100−P300 biochars originates from an amorphous aliphatic fraction, which is enhanced with a reduction of the substrate polarity; for P400−P600, the partition occurs with a condensed aromatic core that diminishes with a further reduction of the polarity. Simultaneously, the adsorption component exhibits a transition from a polarity-selective (P200−P400) to a porosity-selective (P500−P600) process, and displays no selectivity with P700 and AC in which the adsorptive saturation capacities are comparable to predicted values based on the monolayer surface coverage of molecule. The combined adsorption and partition effects of biochars with varying fractions of noncarbonized organic matter have not been clearly defined. Biochars, produced by pyrolysis of pine needles at different temperatures (100-700 ...C, referred as P100-P700), were characterized by elemental analysis, BET-N... surface areas and FTIR. Sorption isotherms of naphthalene, nitrobenzene, and m-dinitrobenzene from water to the biochars were compared. Sorption parameters (N and logK...) are linearly related to sorbent aromaticities, which increase with the pyrolytic temperature. Sorption mechanisms of biochars are evolved from partitioning-dominant at low pyrolytic temperatures to adsorption-dominant at higher pyrolytic temperatures. The quantitative contributions of adsorption and partition are determined by the relative carbonized and noncarbonized fractions and their surface and bulk properties. The partition of P100-P300 biochars originates from an amorphous aliphatic fraction, which is enhanced with a reduction of the substrate polarity; for P400-P600, the partition occurs with a condensed aromatic core that diminishes with a further reduction of the polarity. Simultaneously, the adsorption component exhibits a transition from a polarity-selective (P200-P400) to a porosity-selective (P500-P600) process, and displays no selectivity with P700 and AC in which the adsorptive saturation capacities are comparable to predicted values based on the monolayer surface coverage of molecule. (ProQuest: ... denotes formulae/symbols omitted.) The combined adsorption and partition effects of biochars with varying fractions of noncarbonized organic matter have not been clearly defined. Biochars, produced by pyrolysis of pine needles at different temperatures (100-700 degrees C, referred as P100-P700), were characterized by elemental analysis, BET-N2 surface areas and FTIR. Sorption isotherms of naphthalene, nitrobenzene, and m-dinitrobenzene from water to the biochars were compared. Sorption parameters (N and logKf) are linearly related to sorbent aromaticities, which increase with the pyrolytic temperature. Sorption mechanisms of biochars are evolved from partitioning-dominant at low pyrolytic temperatures to adsorption-dominant at higher pyrolytic temperatures. The quantitative contributions of adsorption and partition are determined by the relative carbonized and noncarbonized fractions and their surface and bulk properties. The partition of P100-P300 biochars originates from an amorphous aliphatic fraction, which is enhanced with a reduction of the substrate polarity; for P400-P600, the partition occurs with a condensed aromatic core that diminishes with a further reduction of the polarity. Simultaneously, the adsorption component exhibits a transition from a polarity-selective (P200-P400) to a porosity-selective (P500-P600) process, and displays no selectivity with P700 and AC in which the adsorptive saturation capacities are comparable to predicted values based on the monolayer surface coverage of molecule. The combined adsorption and partition effects of biochars with varying fractions of noncarbonized organic matter have not been clearly defined. Biochars, produced by pyrolysis of pine needles at different temperatures (100-700 C, referred as P100-P700), were characterized by elemental analysis, BET-N2 surface areas and FTIR. Sorption isotherms of naphthalene, nitrobenzene, and m-dinitrobenzene from water to the biochars were compared. Sorption parameters (N and logKf) are linearly related to sorbent aromaticities, which increase with the pyrolytic temperature. Sorption mechanisms of biochars are evolved from partitioning-dominant at low pyrolytic temperatures to adsorption-dominant at higher pyrolytic temperatures. The quantitative contributions of adsorption and partition are determined by the relative carbonized and noncarbonized fractions and their surface and bulk properties. The partition of P100-P300 biochars originates from an amorphous aliphatic fraction, which is enhanced with a reduction of the substrate polarity; for P400-P600, the partition occurs with a condensed aromatic core that diminishes with a further reduction of the polarity. Simultaneously, the adsorption component exhibits a transition from a polarity-selective (P200-P400) to a porosity-selective (P500-P600) process, and displays no selectivity with P700 and AC in which the adsorptive saturation capacities are comparable to predicted values based on the monolayer surface coverage of molecule. The combined adsorption and partition effects of biochars with varying fractions of noncarbonized organic matter have not been clearly defined. Biochars, produced by pyrolysis of pine needles at different temperatures (100-700 degrees C, referred as P100-P700), were characterized by elemental analysis, BET-N2 surface areas and FTIR. Sorption isotherms of naphthalene, nitrobenzene, and m-dinitrobenzene from water to the biochars were compared. Sorption parameters (N and logKf) are linearly related to sorbent aromaticities, which increase with the pyrolytic temperature. Sorption mechanisms of biochars are evolved from partitioning-dominant at low pyrolytic temperatures to adsorption-dominant at higher pyrolytic temperatures. The quantitative contributions of adsorption and partition are determined by the relative carbonized and noncarbonized fractions and their surface and bulk properties. The partition of P100-P300 biochars originates from an amorphous aliphatic fraction, which is enhanced with a reduction of the substrate polarity; for P400-P600, the partition occurs with a condensed aromatic core that diminishes with a further reduction of the polarity. Simultaneously, the adsorption component exhibits a transition from a polarity-selective (P200-P400) to a porosity-selective (P500-P600) process, and displays no selectivity with P700 and AC in which the adsorptive saturation capacities are comparable to predicted values based on the monolayer surface coverage of molecule.The combined adsorption and partition effects of biochars with varying fractions of noncarbonized organic matter have not been clearly defined. Biochars, produced by pyrolysis of pine needles at different temperatures (100-700 degrees C, referred as P100-P700), were characterized by elemental analysis, BET-N2 surface areas and FTIR. Sorption isotherms of naphthalene, nitrobenzene, and m-dinitrobenzene from water to the biochars were compared. Sorption parameters (N and logKf) are linearly related to sorbent aromaticities, which increase with the pyrolytic temperature. Sorption mechanisms of biochars are evolved from partitioning-dominant at low pyrolytic temperatures to adsorption-dominant at higher pyrolytic temperatures. The quantitative contributions of adsorption and partition are determined by the relative carbonized and noncarbonized fractions and their surface and bulk properties. The partition of P100-P300 biochars originates from an amorphous aliphatic fraction, which is enhanced with a reduction of the substrate polarity; for P400-P600, the partition occurs with a condensed aromatic core that diminishes with a further reduction of the polarity. Simultaneously, the adsorption component exhibits a transition from a polarity-selective (P200-P400) to a porosity-selective (P500-P600) process, and displays no selectivity with P700 and AC in which the adsorptive saturation capacities are comparable to predicted values based on the monolayer surface coverage of molecule.
Author	Zhou, Dandan Zhu, Lizhong Chen, Baoliang
Author_xml	– sequence: 1 givenname: Baoliang surname: Chen fullname: Chen, Baoliang email: blchen@zju.edu.cn – sequence: 2 givenname: Dandan surname: Zhou fullname: Zhou, Dandan – sequence: 3 givenname: Lizhong surname: Zhu fullname: Zhu, Lizhong
BackLink	http://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=20498788$$DView record in Pascal Francis https://www.ncbi.nlm.nih.gov/pubmed/18754360$$D View this record in MEDLINE/PubMed
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Keywords	Elementary analysis Pyrolysis Organic matter Chemical analysis Hydrocarbon Aliphatic compound Pollutant behavior Adsorption isotherm Biological indicator Sorption Pollution Adsorption Surface properties Polarity Aromatic compound Phase partition Porosity Sorbent Organic compounds Low temperature
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Notes	Properties and dimensions of the selected sorbates in Table S-1 and Figure S-1. Kinetic data, isotherms and their regression parameters in Figure S-2, Figure S-3, and Table S-2. Relationships between logKf (and N)∼H/C atomic ratio, between KP∼(O+N)/C), and relative contributions of adsorption and partition in Figure S-4, Figure S-6, and Figure S-5). This material is available free of charge via the Internet at http://pubs.acs.org. ark:/67375/TPS-RGWZ9Z4C-D istex:7808DA45CBEE6D7020D19CA0BA8ABB4FEEB55C28 SourceType-Scholarly Journals-1 ObjectType-Feature-1 content type line 14 ObjectType-Article-1 ObjectType-Feature-2 content type line 23
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Snippet	The combined adsorption and partition effects of biochars with varying fractions of noncarbonized organic matter have not been clearly defined. Biochars,...
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SubjectTerms	Adsorption Applied sciences Biomass Chemical contaminants Environmental Processes Exact sciences and technology Hydrocarbons, Aromatic - chemistry Incineration Molecules Particulate Matter - chemistry Pinus - anatomy & histology Pinus - chemistry Plant Leaves - chemistry Pollution Sorption Spectroscopy, Fourier Transform Infrared Temperature
Title	Transitional Adsorption and Partition of Nonpolar and Polar Aromatic Contaminants by Biochars of Pine Needles with Different Pyrolytic Temperatures
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