Laser-Induced Breakdown Spectroscopy – A geochemical tool for the 21st century

Laser-induced breakdown spectroscopy (LIBS) is a simple, straightforward, and versatile form of atomic emission spectroscopy that focuses a rapidly-pulsed laser beam onto a sample to form a plasma containing its constituent elements and then uses spectral analysis of the emitted light to detect the...

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Published inApplied geochemistry Vol. 128; p. 104929
Main Authors Harmon, Russell S., Senesi, Giorgio S.
Format Journal Article
LanguageEnglish
Published Elsevier Ltd 01.05.2021
Subjects
atomic absorption spectrometry
chemical analysis
Chemometrics
Geochemical fingerprinting
geochemistry
GeoLIBS
instrumentation
Laser-induced breakdown spectroscopy
LIBS
quantitative analysis
spectral analysis
Geochemical fingerprinting
GeoLIBS
LIBS
Chemometrics
Laser-induced breakdown spectroscopy
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Abstract Laser-induced breakdown spectroscopy (LIBS) is a simple, straightforward, and versatile form of atomic emission spectroscopy that focuses a rapidly-pulsed laser beam onto a sample to form a plasma containing its constituent elements and then uses spectral analysis of the emitted light to detect the elements present. In theory, LIBS is capable of qualitative, semi-quantitative, and quantitative analysis of all elements in the periodic table. LIBS can be performed in the laboratory or outside in the ambient environment for on-site analysis in situ; LIBS can also be used for rapid microscale compositional imaging. This review first presents a description of the LIBS technique and then discusses and illustrates through a historic literature review how LIBS has been used to analyze gases, natural waters, minerals, rocks, sediments, and soils. Given the persistent need of analytical instrumentation for the rapid chemical analysis of geologic materials in the field, and the capability of LIBS to analyze any type of sample in real time with little to no preparation, there is a vast potential for the routine application of LIBS across a broad spectrum of the geosciences that is as yet only minimally realized. [Display omitted] •LIBS has specific advantages for rapid chemical analysis in the laboratory and the field, plus vast potential for application across geosciences.•LIBS principles, technology, and chemometric methods for data analysis are described.•The applications of LIBS is reviewed for the chemical analysis of different types of geological media.•Recent trends are highlighted for chemical imaging and microscale elemental analysis minerals and rocks by LIBS.
AbstractList Laser-induced breakdown spectroscopy (LIBS) is a simple, straightforward, and versatile form of atomic emission spectroscopy that focuses a rapidly-pulsed laser beam onto a sample to form a plasma containing its constituent elements and then uses spectral analysis of the emitted light to detect the elements present. In theory, LIBS is capable of qualitative, semi-quantitative, and quantitative analysis of all elements in the periodic table. LIBS can be performed in the laboratory or outside in the ambient environment for on-site analysis in situ; LIBS can also be used for rapid microscale compositional imaging. This review first presents a description of the LIBS technique and then discusses and illustrates through a historic literature review how LIBS has been used to analyze gases, natural waters, minerals, rocks, sediments, and soils. Given the persistent need of analytical instrumentation for the rapid chemical analysis of geologic materials in the field, and the capability of LIBS to analyze any type of sample in real time with little to no preparation, there is a vast potential for the routine application of LIBS across a broad spectrum of the geosciences that is as yet only minimally realized.
Laser-induced breakdown spectroscopy (LIBS) is a simple, straightforward, and versatile form of atomic emission spectroscopy that focuses a rapidly-pulsed laser beam onto a sample to form a plasma containing its constituent elements and then uses spectral analysis of the emitted light to detect the elements present. In theory, LIBS is capable of qualitative, semi-quantitative, and quantitative analysis of all elements in the periodic table. LIBS can be performed in the laboratory or outside in the ambient environment for on-site analysis in situ; LIBS can also be used for rapid microscale compositional imaging. This review first presents a description of the LIBS technique and then discusses and illustrates through a historic literature review how LIBS has been used to analyze gases, natural waters, minerals, rocks, sediments, and soils. Given the persistent need of analytical instrumentation for the rapid chemical analysis of geologic materials in the field, and the capability of LIBS to analyze any type of sample in real time with little to no preparation, there is a vast potential for the routine application of LIBS across a broad spectrum of the geosciences that is as yet only minimally realized. [Display omitted] •LIBS has specific advantages for rapid chemical analysis in the laboratory and the field, plus vast potential for application across geosciences.•LIBS principles, technology, and chemometric methods for data analysis are described.•The applications of LIBS is reviewed for the chemical analysis of different types of geological media.•Recent trends are highlighted for chemical imaging and microscale elemental analysis minerals and rocks by LIBS.
ArticleNumber 104929
Author Senesi, Giorgio S.
Harmon, Russell S.
Author_xml – sequence: 1
  givenname: Russell S.
  orcidid: 0000-0003-1967-3611
  surname: Harmon
  fullname: Harmon, Russell S.
  email: rsharmon@ncsu.edu
  organization: Department of Marine, Earth, and Atmospheric Sciences, North Carolina State University, Raleigh, NC, 27695, USA
– sequence: 2
  givenname: Giorgio S.
  surname: Senesi
  fullname: Senesi, Giorgio S.
  email: giorgio.senesi@cnr.it
  organization: CNR - Istituto per la Scienza e Tecnologia dei Plasmi (ISTP), Sede di Bari, Bari, 70126, Italy
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Snippet Laser-induced breakdown spectroscopy (LIBS) is a simple, straightforward, and versatile form of atomic emission spectroscopy that focuses a rapidly-pulsed...
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SubjectTerms atomic absorption spectrometry
chemical analysis
Chemometrics
Geochemical fingerprinting
geochemistry
GeoLIBS
instrumentation
Laser-induced breakdown spectroscopy
LIBS
quantitative analysis
spectral analysis
Title Laser-Induced Breakdown Spectroscopy – A geochemical tool for the 21st century
URI https://dx.doi.org/10.1016/j.apgeochem.2021.104929
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