Temperature Dependence of Lithium Anode Voiding in Argyrodite Solid-State Batteries
Void formation at the Li/ceramic electrolyte interface of an all-solid-state battery on discharge results in high local current densities, dendrites on charge, and cell failure. Here, we show that such voiding is reduced at the Li/Li6PS5Cl interface at elevated temperatures, sufficient to increase t...
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Published in | ACS applied materials & interfaces Vol. 13; no. 19; pp. 22708 - 22716 |
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Main Authors | , , , , , , , |
Format | Journal Article |
Language | English |
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American Chemical Society
19.05.2021
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Abstract | Void formation at the Li/ceramic electrolyte interface of an all-solid-state battery on discharge results in high local current densities, dendrites on charge, and cell failure. Here, we show that such voiding is reduced at the Li/Li6PS5Cl interface at elevated temperatures, sufficient to increase the critical current before voiding and cell failure from <0.25 mA cm–2 at 25 °C to 0.25 mA cm–2 at 60 °C and 0.5 mA cm–2 at 80 °C under a relatively low stack-pressure of 1 MPa. Increasing the stack-pressure to 5 MPa and temperature to 80 °C permits stable cycling at 2.5 mA cm–2. It is also shown that the charge-transfer resistance at the Li/Li6PS5Cl interface depends on pressure and temperature, with relatively high pressures required to maintain low charge-transfer resistance at −20 °C. These results are consistent with the plastic deformation of Li metal dominating the performance of the Li anode, posing challenges for the implementation of solid-state cells with Li anodes. |
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AbstractList | Void formation at the Li/ceramic electrolyte interface of an all-solid-state battery on discharge results in high local current densities, dendrites on charge, and cell failure. Here, we show that such voiding is reduced at the Li/Li
PS
Cl interface at elevated temperatures, sufficient to increase the critical current before voiding and cell failure from <0.25 mA cm
at 25 °C to 0.25 mA cm
at 60 °C and 0.5 mA cm
at 80 °C under a relatively low stack-pressure of 1 MPa. Increasing the stack-pressure to 5 MPa and temperature to 80 °C permits stable cycling at 2.5 mA cm
. It is also shown that the charge-transfer resistance at the Li/Li
PS
Cl interface depends on pressure and temperature, with relatively high pressures required to maintain low charge-transfer resistance at -20 °C. These results are consistent with the plastic deformation of Li metal dominating the performance of the Li anode, posing challenges for the implementation of solid-state cells with Li anodes. Void formation at the Li/ceramic electrolyte interface of an all-solid-state battery on discharge results in high local current densities, dendrites on charge, and cell failure. Here, we show that such voiding is reduced at the Li/Li6PS5Cl interface at elevated temperatures, sufficient to increase the critical current before voiding and cell failure from <0.25 mA cm–2 at 25 °C to 0.25 mA cm–2 at 60 °C and 0.5 mA cm–2 at 80 °C under a relatively low stack-pressure of 1 MPa. Increasing the stack-pressure to 5 MPa and temperature to 80 °C permits stable cycling at 2.5 mA cm–2. It is also shown that the charge-transfer resistance at the Li/Li6PS5Cl interface depends on pressure and temperature, with relatively high pressures required to maintain low charge-transfer resistance at −20 °C. These results are consistent with the plastic deformation of Li metal dominating the performance of the Li anode, posing challenges for the implementation of solid-state cells with Li anodes. |
Author | Liu, Boyang Melvin, Dominic L. R Bruce, Peter G Hartley, Gareth O Spencer Jolly, Dominic Ning, Ziyang Adamson, Paul Marrow, James |
AuthorAffiliation | Department of Chemistry The Faraday Institution University of Oxford Department of Materials The Henry Royce Institute |
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Title | Temperature Dependence of Lithium Anode Voiding in Argyrodite Solid-State Batteries |
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