Controlling the Optical Properties of Gold Nanorods in One-Pot Syntheses

We present the characterization of the CTAB-oleate controlled synthesis of gold nanorods (AuNRs). Concentrations of key compounds in the synthetic system were varied in the presence of oleate, including HCl, borohydride, silver nitrate, and ascorbic acid. The longitudinal surface plasmon resonance p...

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Published inJournal of physical chemistry. C Vol. 126; no. 6; pp. 3235 - 3243
Main Authors Roach, Lucien, Coletta, P. Louise, Critchley, Kevin, Evans, Stephen D
Format Journal Article
LanguageEnglish
Published United States American Chemical Society 17.02.2022
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C: Physical Properties of Materials and Interfaces
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Abstract We present the characterization of the CTAB-oleate controlled synthesis of gold nanorods (AuNRs). Concentrations of key compounds in the synthetic system were varied in the presence of oleate, including HCl, borohydride, silver nitrate, and ascorbic acid. The longitudinal surface plasmon resonance peak was sensitive to changes in all concentrations. Reducing the concentration of Ag ions below 66 μM led to slower reaction kinetics and incomplete Au reduction. Variation of the ascorbic acid concentration revealed that oleate is responsible for around 44% of reduction of Au3+ to Au+ before nucleation in these experiments. Increasing the oleate concentration significantly slows the growth kinetics and leads to much longer synthesis times of above 12 h for reaction completion. These observations will enable the design of better methods of synthesizing of AuNRs using binary surfactants.
AbstractList We present the characterization of the CTAB-oleate controlled synthesis of gold nanorods (AuNRs). Concentrations of key compounds in the synthetic system were varied in the presence of oleate, including HCl, borohydride, silver nitrate, and ascorbic acid. The longitudinal surface plasmon resonance peak was sensitive to changes in all concentrations. Reducing the concentration of Ag ions below 66 μM led to slower reaction kinetics and incomplete Au reduction. Variation of the ascorbic acid concentration revealed that oleate is responsible for around 44% of reduction of Au to Au before nucleation in these experiments. Increasing the oleate concentration significantly slows the growth kinetics and leads to much longer synthesis times of above 12 h for reaction completion. These observations will enable the design of better methods of synthesizing of AuNRs using binary surfactants.
We present the characterization of the CTAB-oleate controlled synthesis of gold nanorods (AuNRs). Concentrations of key compounds in the synthetic system were varied in the presence of oleate, including HCl, borohydride, silver nitrate, and ascorbic acid. The longitudinal surface plasmon resonance peak was sensitive to changes in all concentrations. Reducing the concentration of Ag ions below 66 μM led to slower reaction kinetics and incomplete Au reduction. Variation of the ascorbic acid concentration revealed that oleate is responsible for around 44% of reduction of Au3+ to Au+ before nucleation in these experiments. Increasing the oleate concentration significantly slows the growth kinetics and leads to much longer synthesis times of above 12 h for reaction completion. These observations will enable the design of better methods of synthesizing of AuNRs using binary surfactants.
We present the characterization of the CTAB-oleate controlled synthesis of gold nanorods (AuNRs). Concentrations of key compounds in the synthetic system were varied in the presence of oleate, including HCl, borohydride, silver nitrate, and ascorbic acid. The longitudinal surface plasmon resonance peak was sensitive to changes in all concentrations. Reducing the concentration of Ag ions below 66 μM led to slower reaction kinetics and incomplete Au reduction. Variation of the ascorbic acid concentration revealed that oleate is responsible for around 44% of reduction of Au 3+ to Au + before nucleation in these experiments. Increasing the oleate concentration significantly slows the growth kinetics and leads to much longer synthesis times of above 12 h for reaction completion. These observations will enable the design of better methods of synthesizing of AuNRs using binary surfactants.
Author Roach, Lucien
Critchley, Kevin
Evans, Stephen D
Coletta, P. Louise
AuthorAffiliation University of Leeds
School of Physics and Astronomy
Leeds Institute for Medical Research
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  givenname: Lucien
  orcidid: 0000-0002-9166-6662
  surname: Roach
  fullname: Roach, Lucien
  organization: School of Physics and Astronomy
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  givenname: P. Louise
  surname: Coletta
  fullname: Coletta, P. Louise
  organization: University of Leeds
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  givenname: Kevin
  orcidid: 0000-0002-0112-8626
  surname: Critchley
  fullname: Critchley, Kevin
  organization: School of Physics and Astronomy
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  givenname: Stephen D
  orcidid: 0000-0001-8342-5335
  surname: Evans
  fullname: Evans, Stephen D
  email: s.d.evans@leeds.ac.uk
  organization: School of Physics and Astronomy
BackLink https://www.ncbi.nlm.nih.gov/pubmed/35432690$$D View this record in MEDLINE/PubMed
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This paper was published on February 3, 2022, with an outdated version of the Supporting Information. The corrected version was posted on February 4, 2022.
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Snippet We present the characterization of the CTAB-oleate controlled synthesis of gold nanorods (AuNRs). Concentrations of key compounds in the synthetic system were...
We present the characterization of the CTAB-oleate controlled synthesis of gold nanorods (AuNRs). Concentrations of key compounds in the synthetic system were...
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SubjectTerms C: Physical Properties of Materials and Interfaces
Title Controlling the Optical Properties of Gold Nanorods in One-Pot Syntheses
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