Understanding the Structural Properties of a Dendrimeric Material Directly from Powder X-ray Diffraction Data
Complete structure determination of an early-generation dendrimeric material has been carried out directly from powder X-ray diffraction data, using the direct-space genetic algorithm technique for structure solution followed by Rietveld refinement. This work represents the first application of mode...
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Published in | The journal of physical chemistry. B Vol. 110; no. 24; pp. 11620 - 11623 |
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Main Authors | , , , , , |
Format | Journal Article |
Language | English |
Published |
United States
American Chemical Society
22.06.2006
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Online Access | Get full text |
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Summary: | Complete structure determination of an early-generation dendrimeric material has been carried out directly from powder X-ray diffraction data, using the direct-space genetic algorithm technique for structure solution followed by Rietveld refinement. This work represents the first application of modern direct-space techniques for structure determination from powder X-ray diffraction data in the case of a dendrimeric material and paves the way for the future application of this approach to enable complete structure determination of other dendrimeric materials that cannot be prepared as single crystal samples suitable for single crystal X-ray diffraction studies. |
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Bibliography: | istex:BE9F8F746EF42A55616CB7E16B54739E748EB457 ark:/67375/TPS-GD9G4ZQ6-L SourceType-Other Sources-1 content type line 63 ObjectType-Correspondence-1 |
ISSN: | 1520-6106 1520-5207 |
DOI: | 10.1021/jp0624348 |