Alcoholic Photoinitiated Polymerization-Induced Self-Assembly (Photo-PISA): A Fast Route toward Poly(isobornyl acrylate)-Based Diblock Copolymer Nano-Objects

We report a fast alcoholic photoinitiated polymerization-induced self-assembly (photo-PISA) formulation via photoinitiated RAFT dispersion polymerization of isobornyl acrylate (IBOA) in an ethanol/water mixture at 40 °C using a monomethoxy poly­(ethylene glycol) (mPEG) based chain transfer agent. Po...

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Published inACS macro letters Vol. 5; no. 8; pp. 894 - 899
Main Authors Tan, Jianbo, Huang, Chundong, Liu, Dongdong, Zhang, Xuechao, Bai, Yuhao, Zhang, Li
Format Journal Article
LanguageEnglish
Published United States American Chemical Society 16.08.2016
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Abstract We report a fast alcoholic photoinitiated polymerization-induced self-assembly (photo-PISA) formulation via photoinitiated RAFT dispersion polymerization of isobornyl acrylate (IBOA) in an ethanol/water mixture at 40 °C using a monomethoxy poly­(ethylene glycol) (mPEG) based chain transfer agent. Polymerization proceeded rapidly via the exposure to visible light irradiation (405 nm, 0.5 mW/cm2), and high monomer conversion (>95%) was achieved within 30 min. Kinetic studies confirmed that good control was maintained during the photo-PISA process, and the polymerization can be activated or deactivated by light. Finally, we demonstrated that a diverse set of complex morphologies (spheres, worms, or vesicles) could be achieved by varying reaction parameters, and a phase diagram was constructed.
AbstractList We report a fast alcoholic photoinitiated polymerization-induced self-assembly (photo-PISA) formulation via photoinitiated RAFT dispersion polymerization of isobornyl acrylate (IBOA) in an ethanol/water mixture at 40 °C using a monomethoxy poly(ethylene glycol) (mPEG) based chain transfer agent. Polymerization proceeded rapidly via the exposure to visible light irradiation (405 nm, 0.5 mW/cm ), and high monomer conversion (>95%) was achieved within 30 min. Kinetic studies confirmed that good control was maintained during the photo-PISA process, and the polymerization can be activated or deactivated by light. Finally, we demonstrated that a diverse set of complex morphologies (spheres, worms, or vesicles) could be achieved by varying reaction parameters, and a phase diagram was constructed.
We report a fast alcoholic photoinitiated polymerization-induced self-assembly (photo-PISA) formulation via photoinitiated RAFT dispersion polymerization of isobornyl acrylate (IBOA) in an ethanol/water mixture at 40 °C using a monomethoxy poly(ethylene glycol) (mPEG) based chain transfer agent. Polymerization proceeded rapidly via the exposure to visible light irradiation (405 nm, 0.5 mW/cm2), and high monomer conversion (>95%) was achieved within 30 min. Kinetic studies confirmed that good control was maintained during the photo-PISA process, and the polymerization can be activated or deactivated by light. Finally, we demonstrated that a diverse set of complex morphologies (spheres, worms, or vesicles) could be achieved by varying reaction parameters, and a phase diagram was constructed.We report a fast alcoholic photoinitiated polymerization-induced self-assembly (photo-PISA) formulation via photoinitiated RAFT dispersion polymerization of isobornyl acrylate (IBOA) in an ethanol/water mixture at 40 °C using a monomethoxy poly(ethylene glycol) (mPEG) based chain transfer agent. Polymerization proceeded rapidly via the exposure to visible light irradiation (405 nm, 0.5 mW/cm2), and high monomer conversion (>95%) was achieved within 30 min. Kinetic studies confirmed that good control was maintained during the photo-PISA process, and the polymerization can be activated or deactivated by light. Finally, we demonstrated that a diverse set of complex morphologies (spheres, worms, or vesicles) could be achieved by varying reaction parameters, and a phase diagram was constructed.
We report a fast alcoholic photoinitiated polymerization-induced self-assembly (photo-PISA) formulation via photoinitiated RAFT dispersion polymerization of isobornyl acrylate (IBOA) in an ethanol/water mixture at 40 °C using a monomethoxy poly­(ethylene glycol) (mPEG) based chain transfer agent. Polymerization proceeded rapidly via the exposure to visible light irradiation (405 nm, 0.5 mW/cm2), and high monomer conversion (>95%) was achieved within 30 min. Kinetic studies confirmed that good control was maintained during the photo-PISA process, and the polymerization can be activated or deactivated by light. Finally, we demonstrated that a diverse set of complex morphologies (spheres, worms, or vesicles) could be achieved by varying reaction parameters, and a phase diagram was constructed.
Author Huang, Chundong
Tan, Jianbo
Liu, Dongdong
Zhang, Xuechao
Bai, Yuhao
Zhang, Li
AuthorAffiliation Department of Polymeric Materials and Engineering, School of Materials and Energy
Guangdong University of Technology
AuthorAffiliation_xml – name: Guangdong University of Technology
– name: Department of Polymeric Materials and Engineering, School of Materials and Energy
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  givenname: Jianbo
  surname: Tan
  fullname: Tan, Jianbo
  email: tanjianbo@gdut.edu.cn
– sequence: 2
  givenname: Chundong
  surname: Huang
  fullname: Huang, Chundong
– sequence: 3
  givenname: Dongdong
  surname: Liu
  fullname: Liu, Dongdong
– sequence: 4
  givenname: Xuechao
  surname: Zhang
  fullname: Zhang, Xuechao
– sequence: 5
  givenname: Yuhao
  surname: Bai
  fullname: Bai, Yuhao
– sequence: 6
  givenname: Li
  surname: Zhang
  fullname: Zhang, Li
  email: lizhang@gdut.edu.cn
BackLink https://www.ncbi.nlm.nih.gov/pubmed/35607218$$D View this record in MEDLINE/PubMed
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Snippet We report a fast alcoholic photoinitiated polymerization-induced self-assembly (photo-PISA) formulation via photoinitiated RAFT dispersion polymerization of...
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Title Alcoholic Photoinitiated Polymerization-Induced Self-Assembly (Photo-PISA): A Fast Route toward Poly(isobornyl acrylate)-Based Diblock Copolymer Nano-Objects
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