Characterization of Free-Standing PEDOT:PSS/Iron Oxide Nanoparticle Composite Thin Films and Application As Conformable Humidity Sensors

In this study, a new simple, fast, and inexpensive technique for the preparation of free-standing nanocomposite ultrathin films based on the conductive polymer poly(3,4-ethylenedioxythiophene):polystyrene sulfonate (PEDOT:PSS) and embedding iron oxide nanoparticles (NPs) is presented. These nanofilm...

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Published in	ACS applied materials & interfaces Vol. 5; no. 13; pp. 6324 - 6332
Main Authors	Taccola, Silvia, Greco, Francesco, Zucca, Alessandra, Innocenti, Claudia, de Julián Fernández, César, Campo, Giulio, Sangregorio, Claudio, Mazzolai, Barbara, Mattoli, Virgilio
Format	Journal Article
Language	English
Published	United States American Chemical Society 10.07.2013
Subjects	Biosensing Techniques - instrumentation Biosensing Techniques - methods Bridged Bicyclo Compounds, Heterocyclic - chemistry Ferric Compounds - chemistry functional properties Humidity iron oxides nanocomposites Nanocomposites - chemistry nanoparticles polymers Polymers - chemical synthesis Polymers - chemistry Polystyrenes - chemistry relative humidity topography Water - analysis PSS iron oxide nanocomposite thin film humidity sensor
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Abstract	In this study, a new simple, fast, and inexpensive technique for the preparation of free-standing nanocomposite ultrathin films based on the conductive polymer poly(3,4-ethylenedioxythiophene):polystyrene sulfonate (PEDOT:PSS) and embedding iron oxide nanoparticles (NPs) is presented. These nanofilms were fabricated by a single step of spin-coated assisted deposition in conjunction with a release technique (“supporting layer technique”) to detach them from the substrate. Free-standing nanofilms can be easily transferred onto several substrates due to their high conformability, preserving their functionalities. The effect of the addition of iron oxide nanoparticles on the structural and functional properties of the PEDOT:PSS nanofilms is investigated through topography, thickness, magnetic, magneto-optical activity, and conductivity characterizations. PEDOT:PSS and PEDOT:PSS/iron oxide NP nanofilms were tested as resistive humidity sensors. Their sensitivity to humidity was found to increase with increasing nanoparticle concentration. On the basis of these results, it is expected that these composites may furnish inexpensive and reliable means for relative humidity detection.
AbstractList	In this study, a new simple, fast, and inexpensive technique for the preparation of free-standing nanocomposite ultrathin films based on the conductive polymer poly(3,4-ethylenedioxythiophene):polystyrene sulfonate (PEDOT:PSS) and embedding iron oxide nanoparticles (NPs) is presented. These nanofilms were fabricated by a single step of spin-coated assisted deposition in conjunction with a release technique (“supporting layer technique”) to detach them from the substrate. Free-standing nanofilms can be easily transferred onto several substrates due to their high conformability, preserving their functionalities. The effect of the addition of iron oxide nanoparticles on the structural and functional properties of the PEDOT:PSS nanofilms is investigated through topography, thickness, magnetic, magneto-optical activity, and conductivity characterizations. PEDOT:PSS and PEDOT:PSS/iron oxide NP nanofilms were tested as resistive humidity sensors. Their sensitivity to humidity was found to increase with increasing nanoparticle concentration. On the basis of these results, it is expected that these composites may furnish inexpensive and reliable means for relative humidity detection. In this study, a new simple, fast, and inexpensive technique for the preparation of free-standing nanocomposite ultrathin films based on the conductive polymer poly(3,4-ethylenedioxythiophene):polystyrene sulfonate (PEDOT:PSS) and embedding iron oxide nanoparticles (NPs) is presented. These nanofilms were fabricated by a single step of spin-coated assisted deposition in conjunction with a release technique ("supporting layer technique") to detach them from the substrate. Free-standing nanofilms can be easily transferred onto several substrates due to their high conformability, preserving their functionalities. The effect of the addition of iron oxide nanoparticles on the structural and functional properties of the PEDOT:PSS nanofilms is investigated through topography, thickness, magnetic, magneto-optical activity, and conductivity characterizations. PEDOT:PSS and PEDOT:PSS/iron oxide NP nanofilms were tested as resistive humidity sensors. Their sensitivity to humidity was found to increase with increasing nanoparticle concentration. On the basis of these results, it is expected that these composites may furnish inexpensive and reliable means for relative humidity detection.In this study, a new simple, fast, and inexpensive technique for the preparation of free-standing nanocomposite ultrathin films based on the conductive polymer poly(3,4-ethylenedioxythiophene):polystyrene sulfonate (PEDOT:PSS) and embedding iron oxide nanoparticles (NPs) is presented. These nanofilms were fabricated by a single step of spin-coated assisted deposition in conjunction with a release technique ("supporting layer technique") to detach them from the substrate. Free-standing nanofilms can be easily transferred onto several substrates due to their high conformability, preserving their functionalities. The effect of the addition of iron oxide nanoparticles on the structural and functional properties of the PEDOT:PSS nanofilms is investigated through topography, thickness, magnetic, magneto-optical activity, and conductivity characterizations. PEDOT:PSS and PEDOT:PSS/iron oxide NP nanofilms were tested as resistive humidity sensors. Their sensitivity to humidity was found to increase with increasing nanoparticle concentration. On the basis of these results, it is expected that these composites may furnish inexpensive and reliable means for relative humidity detection.
Author	Greco, Francesco Mattoli, Virgilio Taccola, Silvia Mazzolai, Barbara Zucca, Alessandra Innocenti, Claudia Sangregorio, Claudio Campo, Giulio de Julián Fernández, César
AuthorAffiliation	The Biorobotics Institute Istituto Italiano di Tecnologia Università degli Studi di Firenze
AuthorAffiliation_xml	– name: Istituto Italiano di Tecnologia – name: Università degli Studi di Firenze – name: The Biorobotics Institute
Author_xml	– sequence: 1 givenname: Silvia surname: Taccola fullname: Taccola, Silvia email: silvia.taccola@iit.it, virgilio.mattoli@iit.it – sequence: 2 givenname: Francesco surname: Greco fullname: Greco, Francesco – sequence: 3 givenname: Alessandra surname: Zucca fullname: Zucca, Alessandra – sequence: 4 givenname: Claudia surname: Innocenti fullname: Innocenti, Claudia – sequence: 5 givenname: César surname: de Julián Fernández fullname: de Julián Fernández, César – sequence: 6 givenname: Giulio surname: Campo fullname: Campo, Giulio – sequence: 7 givenname: Claudio surname: Sangregorio fullname: Sangregorio, Claudio – sequence: 8 givenname: Barbara surname: Mazzolai fullname: Mazzolai, Barbara – sequence: 9 givenname: Virgilio surname: Mattoli fullname: Mattoli, Virgilio email: silvia.taccola@iit.it, virgilio.mattoli@iit.it
BackLink	https://www.ncbi.nlm.nih.gov/pubmed/23802632$$D View this record in MEDLINE/PubMed
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Snippet	In this study, a new simple, fast, and inexpensive technique for the preparation of free-standing nanocomposite ultrathin films based on the conductive polymer...
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SubjectTerms	Biosensing Techniques - instrumentation Biosensing Techniques - methods Bridged Bicyclo Compounds, Heterocyclic - chemistry Ferric Compounds - chemistry functional properties Humidity iron oxides nanocomposites Nanocomposites - chemistry nanoparticles polymers Polymers - chemical synthesis Polymers - chemistry Polystyrenes - chemistry relative humidity topography Water - analysis
Title	Characterization of Free-Standing PEDOT:PSS/Iron Oxide Nanoparticle Composite Thin Films and Application As Conformable Humidity Sensors
URI	http://dx.doi.org/10.1021/am4013775 https://www.ncbi.nlm.nih.gov/pubmed/23802632 https://www.proquest.com/docview/1399503812 https://www.proquest.com/docview/2000381948
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