Complexation of Cobalt by Natural Ligands in Freshwater

Ligand exchange with dimethylglyoxime (DMG) and dif ferential pulse cathodic stripping voltammetry (DPCSV) was applied to determine free Co(II) ionic concentrations [Co2+] and Co(II) complexation by natural organic ligands in freshwater. [Co2+] and the complexing parameters were calculated on the ba...

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Published inEnvironmental science & technology Vol. 32; no. 14; pp. 2043 - 2050
Main Authors Qian, Jin, Xue, Han Bin, Sigg, Laura, Albrecht, Achim
Format Journal Article
LanguageEnglish
Published Washington, DC American Chemical Society 15.07.1998
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Abstract Ligand exchange with dimethylglyoxime (DMG) and dif ferential pulse cathodic stripping voltammetry (DPCSV) was applied to determine free Co(II) ionic concentrations [Co2+] and Co(II) complexation by natural organic ligands in freshwater. [Co2+] and the complexing parameters were calculated on the basis of the thermodynamic equilibria between added and natural ligands. The optimal working conditions were carefully evaluated in synthetic solutions and in natural freshwater samples. The results from samples collected at various sites from the Aare and Rhine Rivers and the Biel and Lucerne Lakes, Switzerland, are presented. The total dissolved Co concentrations are in the range of 0.5−6.5 nM, and [Co2+] is in the range of 0.05−0.5 nM. Organic complexes of Co are predominant in most samples with 80−96% of total dissolved Co. A one-ligand model could well fit the titrations of freshwater samples with Co(II) (using the FITEQL program). The conditional stability constants of the natural ligands were computed to be log K = 9.5−11.6 (pH 8.0 ± 0.1), and the ligand concentrations were [L] = 1.4−7.6 nM. The reliability and applicability of the technique and the implications of the results are discussed.
AbstractList ACo2+B and Co(II) complexation determined by ligand exchange and DPCSV show 80-96% in the form of natural organic complexes in Swiss rivers and lakes.
Ligand exchange with dimethylglyoxime (DMG) and dif ferential pulse cathodic stripping voltammetry (DPCSV) was applied to determine free Co(II) ionic concentrations [Co2+] and Co(II) complexation by natural organic ligands in freshwater. [Co2+] and the complexing parameters were calculated on the basis of the thermodynamic equilibria between added and natural ligands. The optimal working conditions were carefully evaluated in synthetic solutions and in natural freshwater samples. The results from samples collected at various sites from the Aare and Rhine Rivers and the Biel and Lucerne Lakes, Switzerland, are presented. The total dissolved Co concentrations are in the range of 0.5−6.5 nM, and [Co2+] is in the range of 0.05−0.5 nM. Organic complexes of Co are predominant in most samples with 80−96% of total dissolved Co. A one-ligand model could well fit the titrations of freshwater samples with Co(II) (using the FITEQL program). The conditional stability constants of the natural ligands were computed to be log K = 9.5−11.6 (pH 8.0 ± 0.1), and the ligand concentrations were [L] = 1.4−7.6 nM. The reliability and applicability of the technique and the implications of the results are discussed.
Ligand exchange with dimethylglyoxime (DMG) and differential pulse cathodic stripping voltammetry (DPCSV) was applied to determine free Co(II) ionic concentrations [Co super(2+)] and Co(II) complexation by natural organic ligands in freshwater. [Co super(2+)] and the complexing parameters were calculated on the basis of the thermodynamic equilibria between added and natural ligands. The optimal working conditions were carefully evaluated in synthetic solutions and in natural freshwater samples. The results from samples collected at various sites from the Aare and Rhine Rivers and the Biel and Lucerne Lakes, Switzerland, are presented. The total dissolved Co concentrations are in the range of 0.5-6.5 nM, and [Co super(2+)] is in the range of 0.05-0.5 nM. Organic complexes of Co are predominant in most samples with 80-96% of total dissolved Co. A one-ligand model could well fit the titrations of freshwater samples with Co(II) (using the FITEQL program). The conditional stability constants of the natural ligands were computed to be log K = 9.5-11.6 (pH 8.0 plus or minus 0.1), and the ligand concentrations were [L] = 1.4-7.6 nM. The reliability and applicability of the technique and the implications of the results are discussed.
Author Albrecht, Achim
Qian, Jin
Sigg, Laura
Xue, Han Bin
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Issue 14
Keywords Freshwater environment
Complexation
Nuclear industry
Radioactive pollution
Ligand
Surface water
Water pollution
Natural compound
Radioisotope
Cobalt
Organic compounds
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Snippet Ligand exchange with dimethylglyoxime (DMG) and dif ferential pulse cathodic stripping voltammetry (DPCSV) was applied to determine free Co(II) ionic...
ACo2+B and Co(II) complexation determined by ligand exchange and DPCSV show 80-96% in the form of natural organic complexes in Swiss rivers and lakes.
Ligand exchange with dimethylglyoxime (DMG) and differential pulse cathodic stripping voltammetry (DPCSV) was applied to determine free Co(II) ionic...
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SubjectTerms Animal, plant and microbial ecology
Applied ecology
Applied sciences
Biological and medical sciences
Biological and physicochemical phenomena
Chemical bonds
Chemistry
Cobalt
Earth sciences
Earth, ocean, space
Ecotoxicology, biological effects of pollution
Engineering and environment geology. Geothermics
Exact sciences and technology
Fresh water environment
Fundamental and applied biological sciences. Psychology
Natural water pollution
Pollution
Pollution, environment geology
Thermodynamics
Water
Water treatment and pollution
Title Complexation of Cobalt by Natural Ligands in Freshwater
URI http://dx.doi.org/10.1021/es971018l
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Volume 32
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