Development of Rapid Determination of 18 Phthalate Esters in Edible Vegetable Oils by Gas Chromatography Tandem Mass Spectrometry
A simultaneous and fast determination of 18 phthalic acid esters (PAEs) in edible vegetable oils was developed. After solvent extraction, the PAEs in the oil sample were further cleaned up by solid-phase extraction. After concentration, the extract was directly injected into gas chromatography tande...
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| Published in | Journal of agricultural and food chemistry Vol. 61; no. 6; pp. 1160 - 1164 |
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| Main Authors | , , |
| Format | Journal Article |
| Language | English |
| Published |
United States
American Chemical Society
13.02.2013
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| Subjects | |
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| Abstract | A simultaneous and fast determination of 18 phthalic acid esters (PAEs) in edible vegetable oils was developed. After solvent extraction, the PAEs in the oil sample were further cleaned up by solid-phase extraction. After concentration, the extract was directly injected into gas chromatography tandem mass spectrometry (GC–MS/MS) in positive-ion electron impact (EI) mode. Method quantification limits of 18 PAEs were between 0.01 and 0.1 mg/kg. Quantitative recoveries ranging from 63.9 to 115.3% were obtained by analysis of spiked oil. The relative standard deviations were less than 15% (n = 6). The method could potentially overcome the interference from large amounts of lipids and pigment. It was applied to real sample and shown to be a rapid and reliable alternative for determination and confirmation of PAEs in routine analysis. |
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| AbstractList | A simultaneous and fast determination of 18 phthalic acid esters (PAEs) in edible vegetable oils was developed. After solvent extraction, the PAEs in the oil sample were further cleaned up by solid-phase extraction. After concentration, the extract was directly injected into gas chromatography tandem mass spectrometry (GC-MS/MS) in positive-ion electron impact (EI) mode. Method quantification limits of 18 PAEs were between 0.01 and 0.1 mg/kg. Quantitative recoveries ranging from 63.9 to 115.3% were obtained by analysis of spiked oil. The relative standard deviations were less than 15% (n = 6). The method could potentially overcome the interference from large amounts of lipids and pigment. It was applied to real sample and shown to be a rapid and reliable alternative for determination and confirmation of PAEs in routine analysis. |
| Author | Wang, Shuhui Liu, Yinping Wang, Li |
| AuthorAffiliation | Shijiazhuang Center for Disease Control and Prevention Hebei Provincial Center for Disease Control and Prevention |
| AuthorAffiliation_xml | – name: Shijiazhuang Center for Disease Control and Prevention – name: Hebei Provincial Center for Disease Control and Prevention |
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| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/23339279$$D View this record in MEDLINE/PubMed |
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| Keywords | gas chromatography tandem mass spectrometry vegetable oil multi-residue analysis Phthalic acid esters phthalates solid-phase extraction |
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| Snippet | A simultaneous and fast determination of 18 phthalic acid esters (PAEs) in edible vegetable oils was developed. After solvent extraction, the PAEs in the oil... |
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| SubjectTerms | Esters - analysis gas chromatography Gas Chromatography-Mass Spectrometry - methods liquid-liquid extraction mass spectrometry phthalates Phthalic Acids - analysis Plant Oils - analysis solid phase extraction Tandem Mass Spectrometry - methods vegetable oil Vegetables - chemistry |
| Title | Development of Rapid Determination of 18 Phthalate Esters in Edible Vegetable Oils by Gas Chromatography Tandem Mass Spectrometry |
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