Crystallographic preferred orientation in wüstite (FeO) through the cubic-to-rhombohedral phase transition
Magnesiowüstite, (Mg 0.08 Fe 0.88 )O, and wüstite, Fe 0.94 O, were compressed to ~36 GPa at ambient temperature in the diamond anvil cell (DAC) at the Advanced Light Source. X-ray diffraction patterns were taken in situ in radial geometry in order to study the evolution of crystallographic preferred...
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Published in | Physics and chemistry of minerals Vol. 39; no. 8; pp. 613 - 626 |
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Main Authors | , , , , |
Format | Journal Article |
Language | English |
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Springer-Verlag
01.09.2012
Springer Nature B.V |
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Abstract | Magnesiowüstite, (Mg
0.08
Fe
0.88
)O, and wüstite, Fe
0.94
O, were compressed to ~36 GPa at ambient temperature in the diamond anvil cell (DAC) at the Advanced Light Source. X-ray diffraction patterns were taken in situ in radial geometry in order to study the evolution of crystallographic preferred orientation through the cubic-to-rhombohedral phase transition. Under uniaxial stress in the DAC, {100}
c
planes aligned perpendicular to the compression direction. The {100}
c
in cubic became {
}
r
in rhombohedral and remained aligned perpendicular to the compression direction. However, the {101}
c
and {111}
c
planes in the cubic phase split into {
}
r
and {
}
r
, and (0001)
r
and {
}
r
, respectively, in the rhombohedral phase. The {
}
r
planes preferentially aligned perpendicular to the compression direction while {
}
r
oriented at a low angle to the compression direction. Similarly, {
}
r
showed a slight preference to align more closely perpendicular to the compression direction than (0001)
r
. This variant selection may occur because the 〈
〉
r
and [0001]
r
directions are the softer of the two sets of directions. The rhombohedral texture distortion may also be due to subsequent deformation. Indeed, polycrystal plasticity simulations indicate that for preferred {
}〈
〉
r
and {
}〈
〉
r
slip and slightly less active {
}〈
〉
r
slip, the observed texture pattern can be obtained. |
---|---|
AbstractList | Magnesiowüstite, (Mg0.08Fe0.88)O, and wüstite, Fe0.94O, were compressed to ~36 GPa at ambient temperature in the diamond anvil cell (DAC) at the Advanced Light Source. X-ray diffraction patterns were taken in situ in radial geometry in order to study the evolution of crystallographic preferred orientation through the cubic-to-rhombohedral phase transition. Under uniaxial stress in the DAC, {100}c planes aligned perpendicular to the compression direction. The {100}c in cubic became {\[\left\{ {10\bar 14} \right\}\]}r in rhombohedral and remained aligned perpendicular to the compression direction. However, the {101}c and {111}c planes in the cubic phase split into {\[{10{\bar{1}}4}\]}r and {\[{11{\bar{2}}0}\]}r, and (0001)r and {\[{10{\bar{1}}1}\]}r, respectively, in the rhombohedral phase. The {\[{11{\bar{2}}0}\]}r planes preferentially aligned perpendicular to the compression direction while {\[{10{\bar{1}}4}\]}r oriented at a low angle to the compression direction. Similarly, {\[{10{\bar{1}}1}\]}r showed a slight preference to align more closely perpendicular to the compression direction than (0001)r. This variant selection may occur because the 〈\[{10{\bar{1}}4}\]〉r and [0001]r directions are the softer of the two sets of directions. The rhombohedral texture distortion may also be due to subsequent deformation. Indeed, polycrystal plasticity simulations indicate that for preferred {\[{10{\bar{1}}4}\]}〈\[{1{\bar{2}}10}\]〉r and {\[{11{\bar{2}}0}\]}〈\[{{\bar{1}}101}\]〉r slip and slightly less active {\[{10{\bar{1}}1}\]}〈\[{{\bar{1}}2{\bar{1}}0}\]〉r slip, the observed texture pattern can be obtained. Magnesiowüstite, (Mg 0.08 Fe 0.88 )O, and wüstite, Fe 0.94 O, were compressed to ~36 GPa at ambient temperature in the diamond anvil cell (DAC) at the Advanced Light Source. X-ray diffraction patterns were taken in situ in radial geometry in order to study the evolution of crystallographic preferred orientation through the cubic-to-rhombohedral phase transition. Under uniaxial stress in the DAC, {100} c planes aligned perpendicular to the compression direction. The {100} c in cubic became { } r in rhombohedral and remained aligned perpendicular to the compression direction. However, the {101} c and {111} c planes in the cubic phase split into { } r and { } r , and (0001) r and { } r , respectively, in the rhombohedral phase. The { } r planes preferentially aligned perpendicular to the compression direction while { } r oriented at a low angle to the compression direction. Similarly, { } r showed a slight preference to align more closely perpendicular to the compression direction than (0001) r . This variant selection may occur because the 〈 〉 r and [0001] r directions are the softer of the two sets of directions. The rhombohedral texture distortion may also be due to subsequent deformation. Indeed, polycrystal plasticity simulations indicate that for preferred { }〈 〉 r and { }〈 〉 r slip and slightly less active { }〈 〉 r slip, the observed texture pattern can be obtained. |
Author | Kaercher, P. Kanitpanyacharoen, W. Wenk, H.-R. Speziale, S. Miyagi, L. |
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Keywords | Diamond anvil cell Wüstite Preferred orientation Phase transition |
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Snippet | Magnesiowüstite, (Mg
0.08
Fe
0.88
)O, and wüstite, Fe
0.94
O, were compressed to ~36 GPa at ambient temperature in the diamond anvil cell (DAC) at the Advanced... Magnesiowüstite, (Mg0.08Fe0.88)O, and wüstite, Fe0.94O, were compressed to ~36 GPa at ambient temperature in the diamond anvil cell (DAC) at the Advanced Light... |
SourceID | proquest crossref springer |
SourceType | Aggregation Database Publisher |
StartPage | 613 |
SubjectTerms | Alignment Ambient temperature Crystallography Crystallography and Scattering Methods Deformation Diamond anvil cells Diffraction patterns Earth and Environmental Science Earth Sciences Geochemistry Light diffraction Light sources Mineral Resources Mineralogy Original Paper Phase transitions Planes Polycrystals Preferred orientation Slip Texture Wustite X-ray diffraction |
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Title | Crystallographic preferred orientation in wüstite (FeO) through the cubic-to-rhombohedral phase transition |
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