Characterization of Key Aroma-Active Compounds in Black Garlic by Sensory-Directed Flavor Analysis
Black garlic is a new garlic product produced through fermentation of fresh garlic and is very popular in Asia countries due to its health benefits. Its key aroma-active compounds were characterized by gas chromatography–olfactometry–mass spectrometry (GC-O-MS), gas chromatography–time-of-flight mas...
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Published in | Journal of agricultural and food chemistry Vol. 67; no. 28; pp. 7926 - 7934 |
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Main Authors | , , , |
Format | Journal Article |
Language | English |
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American Chemical Society
17.07.2019
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Abstract | Black garlic is a new garlic product produced through fermentation of fresh garlic and is very popular in Asia countries due to its health benefits. Its key aroma-active compounds were characterized by gas chromatography–olfactometry–mass spectrometry (GC-O-MS), gas chromatography–time-of-flight mass spectrometry (GC-TOFMS), and sensory evaluation. In total 52 aroma compounds were identified, and 15 of them with high flavor dilution (FD) factors based on aroma extract dilution analysis (AEDA) were selected and quantitated. Finally, 9 key aroma-active compounds, including acetic acid (sour), allyl methyl trisulfide (cooked garlic), Furaneol (caramel), diallyldisulfide (garlic), diallyltrisulfide (sulfur), (E,Z)-2,6-nonadien-1-ol (cucumber), 3-methylbutanoic acid (sweat), 5-heptyldihydro-2(3H)-furanone (apricot), and diallyl sulfide (garlic), were determined through aroma recombination and omission experiment. In addition to the sulfur-containing compounds, heterocyclic compounds were the major aroma contributors in black garlic. Sensory evaluation revealed that the flavor profile of black garlic mainly consisted of sulfur, sour, sweet, fresh, sauce, gasoline, and roasted odors. |
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AbstractList | Black garlic is a new garlic product produced through fermentation of fresh garlic and is very popular in Asia countries due to its health benefits. Its key aroma-active compounds were characterized by gas chromatography–olfactometry–mass spectrometry (GC-O-MS), gas chromatography–time-of-flight mass spectrometry (GC-TOFMS), and sensory evaluation. In total 52 aroma compounds were identified, and 15 of them with high flavor dilution (FD) factors based on aroma extract dilution analysis (AEDA) were selected and quantitated. Finally, 9 key aroma-active compounds, including acetic acid (sour), allyl methyl trisulfide (cooked garlic), Furaneol (caramel), diallyldisulfide (garlic), diallyltrisulfide (sulfur), (E,Z)-2,6-nonadien-1-ol (cucumber), 3-methylbutanoic acid (sweat), 5-heptyldihydro-2(3H)-furanone (apricot), and diallyl sulfide (garlic), were determined through aroma recombination and omission experiment. In addition to the sulfur-containing compounds, heterocyclic compounds were the major aroma contributors in black garlic. Sensory evaluation revealed that the flavor profile of black garlic mainly consisted of sulfur, sour, sweet, fresh, sauce, gasoline, and roasted odors. Black garlic is a new garlic product produced through fermentation of fresh garlic and very popular in Asia countries due to its health benefits. Its key aroma-active compounds were characterized by gas chromatography-olfactometry-mass spectrometry (GC-O-MS), gas chromatography-time-of-flight-mass spectrometry (GC-TOF-MS), and sensory evaluation. Totally 52 aroma compounds were identified, and 15 of them with high FD factors based on aroma extract dilution analysis (AEDA) were selected and quantitated. Finally, nine key aroma-active compounds, including acetic acid (sour), allyl methyl trisulfide (cooked garlic), furaneol (caramel), diallyldisulfide (garlic), diallyltrisulfide (sulfur), (E,Z)-2,6-nonadien-1-ol (cucumber), 3-methylbutanoic acid (sweat), 5-heptyldihydro-2(3H)-furanone (apricot), and diallyl sulfide (garlic), were determined through aroma recombination and omission experiment. In addition to the sulfur-containing compounds, heterocyclic compounds were the major aroma contributors in black garlic. Sensory evaluation revealed that the flavor profile of black garlic mainly consisted of sulfur, sour, sweet, fresh, sauce, gasoline, and roasted odors. |
Author | Yang, Ping Wang, Lijin Song, Huanlu Jing, Hao |
AuthorAffiliation | China Agricultural University (CAU) Beijing Advanced Innovation Center for Food Nutrition and Human Health, Beijing Research Center for Food Additive Engineering Technology, Laboratory of Molecular Sensory Science College of Food Science and Nutritional Engineering |
AuthorAffiliation_xml | – name: Beijing Advanced Innovation Center for Food Nutrition and Human Health, Beijing Research Center for Food Additive Engineering Technology, Laboratory of Molecular Sensory Science – name: China Agricultural University (CAU) – name: College of Food Science and Nutritional Engineering |
Author_xml | – sequence: 1 givenname: Ping surname: Yang fullname: Yang, Ping organization: Beijing Advanced Innovation Center for Food Nutrition and Human Health, Beijing Research Center for Food Additive Engineering Technology, Laboratory of Molecular Sensory Science – sequence: 2 givenname: Huanlu orcidid: 0000-0001-8513-3299 surname: Song fullname: Song, Huanlu organization: Beijing Advanced Innovation Center for Food Nutrition and Human Health, Beijing Research Center for Food Additive Engineering Technology, Laboratory of Molecular Sensory Science – sequence: 3 givenname: Lijin orcidid: 0000-0003-3434-3362 surname: Wang fullname: Wang, Lijin email: wanglijin@btbu.edu.cn organization: Beijing Advanced Innovation Center for Food Nutrition and Human Health, Beijing Research Center for Food Additive Engineering Technology, Laboratory of Molecular Sensory Science – sequence: 4 givenname: Hao surname: Jing fullname: Jing, Hao organization: China Agricultural University (CAU) |
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Keywords | gas chromatography−olfactometry−mass spectrometry black garlic odor activity value aroma-active compounds aroma extraction dilution analysis |
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Snippet | Black garlic is a new garlic product produced through fermentation of fresh garlic and is very popular in Asia countries due to its health benefits. Its key... Black garlic is a new garlic product produced through fermentation of fresh garlic and very popular in Asia countries due to its health benefits. Its key... |
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Title | Characterization of Key Aroma-Active Compounds in Black Garlic by Sensory-Directed Flavor Analysis |
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