Acridinium-Based Photocatalysts: A Sustainable Option in Photoredox Catalysis
The emergence of visible light photoredox catalysis has enabled the productive use of lower energy radiation, leading to highly selective reaction platforms. Polypyridyl complexes of iridium and ruthenium have served as popular photocatalysts in recent years due to their long excited state lifetimes...
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| Published in | Journal of organic chemistry Vol. 81; no. 16; pp. 7244 - 7249 |
|---|---|
| Main Authors | , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
WASHINGTON
American Chemical Society
19.08.2016
Amer Chemical Soc |
| Subjects | |
| Online Access | Get full text |
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| Abstract | The emergence of visible light photoredox catalysis has enabled the productive use of lower energy radiation, leading to highly selective reaction platforms. Polypyridyl complexes of iridium and ruthenium have served as popular photocatalysts in recent years due to their long excited state lifetimes and useful redox windows, leading to the development of diverse photoredox-catalyzed transformations. The low abundances of Ir and Ru in the earth’s crust and, hence, cost make these catalysts nonsustainable and have limited their application in industrial-scale manufacturing. Herein, we report a series of novel acridinium salts as alternatives to iridium photoredox catalysts and show their comparability to the ubiquitous [Ir(dF-CF3-ppy)2(dtbpy)](PF6). |
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| AbstractList | The emergence of visible light photoredox catalysis has enabled the productive use of lower energy radiation, leading to highly selective reaction platforms. Polypyridyl complexes of iridium and ruthenium have served as popular photocatalysts in recent years due to their long excited state lifetimes and useful redox windows, leading to the development of diverse photoredox-catalyzed transformations. The low abundances of Ir and Ru in the earth's crust and, hence, cost make these catalysts nonsustainable and have limited their application in industrial-scale manufacturing. Herein, we report a series of novel acridinium salts as alternatives to iridium photoredox catalysts and show their comparability to the ubiquitous [Ir(dF-CF3-ppy)(2)(dtbpy)](PF6). The emergence of visible light photoredox catalysis has enabled the productive use of lower energy radiation, leading to highly selective reaction platforms. Polypyridyl complexes of iridium and ruthenium have served as popular photocatalysts in recent years due to their long excited state lifetimes and useful redox windows, leading to the development of diverse photoredox-catalyzed transformations. The low abundances of Ir and Ru in the earth’s crust and, hence, cost make these catalysts nonsustainable and have limited their application in industrial-scale manufacturing. Herein, we report a series of novel acridinium salts as alternatives to iridium photoredox catalysts and show their comparability to the ubiquitous [Ir(dF-CF3-ppy)2(dtbpy)](PF6). |
| Author | Campeau, Louis-Charles Lévesque, François DiRocco, Daniel A Oliver, Steven F Nicewicz, David Roth, Hudson G Joshi-Pangu, Amruta |
| AuthorAffiliation | Department of Chemistry Merck Research Laboratories Process Research & Development University of North Carolina at Chapel Hill |
| AuthorAffiliation_xml | – name: Merck Research Laboratories – name: Department of Chemistry – name: University of North Carolina at Chapel Hill – name: Process Research & Development |
| Author_xml | – sequence: 1 givenname: Amruta surname: Joshi-Pangu fullname: Joshi-Pangu, Amruta – sequence: 2 givenname: François surname: Lévesque fullname: Lévesque, François – sequence: 3 givenname: Hudson G surname: Roth fullname: Roth, Hudson G – sequence: 4 givenname: Steven F surname: Oliver fullname: Oliver, Steven F – sequence: 5 givenname: Louis-Charles surname: Campeau fullname: Campeau, Louis-Charles – sequence: 6 givenname: David surname: Nicewicz fullname: Nicewicz, David – sequence: 7 givenname: Daniel A surname: DiRocco fullname: DiRocco, Daniel A email: daniel.dirocco@merck.com |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/27454776$$D View this record in MEDLINE/PubMed |
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| Snippet | The emergence of visible light photoredox catalysis has enabled the productive use of lower energy radiation, leading to highly selective reaction platforms.... |
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| SubjectTerms | Chemistry Chemistry, Organic Physical Sciences Science & Technology |
| Title | Acridinium-Based Photocatalysts: A Sustainable Option in Photoredox Catalysis |
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