Adsorption of bensulfuron-methyl on kaolinite as influenced by Pb contamination

Background, aim and scope The combined pollution of bensulfuron-methyl (BSM) and heavy metal Pb has been a common problem in agro-ecological environment in southern China. As an important natural clay mineral, the kaolinite structure possesses great advantages in many processes due to its high chemi...

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Published inJournal of soils and sediments Vol. 9; no. 5; pp. 476 - 481
Main Authors Wu, Wei-Hong, Xu, Jian-Ming, Feng, Zi-Song, Xie, Zheng-Miao
Format Journal Article
LanguageEnglish
Published Berlin/Heidelberg Berlin/Heidelberg : Springer-Verlag 01.10.2009
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Abstract Background, aim and scope The combined pollution of bensulfuron-methyl (BSM) and heavy metal Pb has been a common problem in agro-ecological environment in southern China. As an important natural clay mineral, the kaolinite structure possesses great advantages in many processes due to its high chemical stability and low expansion coefficient. The adsorption of BSM on kaolinite was therefore investigated at varying Pb²⁺ concentrations (0, 100, 500 and 1,000 mg kg⁻¹) and different pH levels (3, 4 and 5) using the batch equilibration experiment. Materials and methods BSM was purchased from Aldrich Chemical Co. (purity, 98%), used as the model compound in this study. The experimental kaolinite was sampled from Yuhang in Zhejiang Province. The metal salts used in the study are Pb(NO₃)₂. The kaolinite samples were spiked with Pb at a rate of 100, 500 and 1,000 mg kg⁻¹ air-dried soil, respectively. The adsorption of BSM on kaolinite was investigated using the batch equilibration experiment. The BSM concentration of the filtrate was determined by high-pressure liquid chromatography. Results and discussion The adsorption of BSM on kaolinite could be described by the Freundlich isotherm equation, with the R ² values greater than 0.959 in all experimental treatment. The presence of Pb²⁺ in kaolinite promoted the adsorption of BSM, and the higher Pb would generally lead to the stronger sorption of BSM by kaolinite based on the observed K f values. The adsorption of BSM on kaolinite declined with the increase of pH, and the spiked Pb²⁺ aggravated the reduction of adsorption of BSM. The exclusion between BSM and kaolinite was strengthened with the increase of pH, which partially elucidated the adsorption of BSM decreasing with increasing pH of the solution. Some adsorption of Pb²⁺ took place along the outer hydroxyl plane, therefore releasing H⁺ ions located there. The spiked Pb²⁺ would promote the adsorption of BSM onto kaolinite by increasing the hydrogen (H⁺) ions concentration in solution. The interactions of the heavy metal cations with the kaolinite could affect the structure and other properties such as swelling capacity, compaction capability and the double-layer behaviour of kaolinite. In addition, the substitution of H⁺ ions for metal ions could change the Van der Wals force within the kaolinite structure. All these might lead to the increased sorption of BSM onto kaolinite at the presence of Pb²⁺. Conclusions The addition of Pb²⁺ and the reduction of pH in solution would enhance the retention of BSM and thus effectively retard BSM from entering the aqueous phase. The mechanisms involved in the promotion effects of the spiked Pb²⁺ on adsorption might be primarily attributed to the increased hydrogen (H⁺) ions as a consequence of the addition of Pb²⁺. Recommendations and perspectives Further investigation would be required to give insight into the specific mechanism controlling the adsorption of BSM on kaolinite.
AbstractList The combined pollution of bensulfuron-methyl (BSM) and heavy metal Pb has been a common problem in agro-ecological environment in southern China. As an important natural clay mineral, the kaolinite structure possesses great advantages in many processes due to its high chemical stability and low expansion coefficient. The adsorption of BSM on kaolinite was therefore investigated at varying Pb2+ concentrations (0, 100, 500 and 1,000 mg kg-1) and different pH levels (3, 4 and 5) using the batch equilibration experiment. BSM was purchased from Aldrich Chemical Co. (purity, 98%), used as the model compound in this study. The experimental kaolinite was sampled from Yuhang in Zhejiang Province. The metal salts used in the study are Pb(NO3)2. The kaolinite samples were spiked with Pb at a rate of 100, 500 and 1,000 mg kg-1 air-dried soil, respectively. The adsorption of BSM on kaolinite was investigated using the batch equilibration experiment. The BSM concentration of the filtrate was determined by high-pressure liquid chromatography. The adsorption of BSM on kaolinite could be described by the Freundlich isotherm equation, with the R2 values greater than 0.959 in all experimental treatment. The presence of Pb2+ in kaolinite promoted the adsorption of BSM, and the higher Pb would generally lead to the stronger sorption of BSM by kaolinite based on the observed K f values. The adsorption of BSM on kaolinite declined with the increase of pH, and the spiked Pb2+ aggravated the reduction of adsorption of BSM. The exclusion between BSM and kaolinite was strengthened with the increase of pH, which partially elucidated the adsorption of BSM decreasing with increasing pH of the solution. Some adsorption of Pb2+ took place along the outer hydroxyl plane, therefore releasing H+ ions located there. The spiked Pb2+ would promote the adsorption of BSM onto kaolinite by increasing the hydrogen (H+) ions concentration in solution. The interactions of the heavy metal cations with the kaolinite could affect the structure and other properties such as swelling capacity, compaction capability and the double-layer behaviour of kaolinite. In addition, the substitution of H+ ions for metal ions could change the Van der Wals force within the kaolinite structure. All these might lead to the increased sorption of BSM onto kaolinite at the presence of Pb2+. The addition of Pb2+ and the reduction of pH in solution would enhance the retention of BSM and thus effectively retard BSM from entering the aqueous phase. The mechanisms involved in the promotion effects of the spiked Pb2+ on adsorption might be primarily attributed to the increased hydrogen (H+) ions as a consequence of the addition of Pb2+. Further investigation would be required to give insight into the specific mechanism controlling the adsorption of BSM on kaolinite. (PUBLICATION ABSTRACT)
Background, aim and scope The combined pollution of bensulfuron-methyl (BSM) and heavy metal Pb has been a common problem in agro-ecological environment in southern China. As an important natural clay mineral, the kaolinite structure possesses great advantages in many processes due to its high chemical stability and low expansion coefficient. The adsorption of BSM on kaolinite was therefore investigated at varying Pb²⁺ concentrations (0, 100, 500 and 1,000 mg kg⁻¹) and different pH levels (3, 4 and 5) using the batch equilibration experiment. Materials and methods BSM was purchased from Aldrich Chemical Co. (purity, 98%), used as the model compound in this study. The experimental kaolinite was sampled from Yuhang in Zhejiang Province. The metal salts used in the study are Pb(NO₃)₂. The kaolinite samples were spiked with Pb at a rate of 100, 500 and 1,000 mg kg⁻¹ air-dried soil, respectively. The adsorption of BSM on kaolinite was investigated using the batch equilibration experiment. The BSM concentration of the filtrate was determined by high-pressure liquid chromatography. Results and discussion The adsorption of BSM on kaolinite could be described by the Freundlich isotherm equation, with the R ² values greater than 0.959 in all experimental treatment. The presence of Pb²⁺ in kaolinite promoted the adsorption of BSM, and the higher Pb would generally lead to the stronger sorption of BSM by kaolinite based on the observed K f values. The adsorption of BSM on kaolinite declined with the increase of pH, and the spiked Pb²⁺ aggravated the reduction of adsorption of BSM. The exclusion between BSM and kaolinite was strengthened with the increase of pH, which partially elucidated the adsorption of BSM decreasing with increasing pH of the solution. Some adsorption of Pb²⁺ took place along the outer hydroxyl plane, therefore releasing H⁺ ions located there. The spiked Pb²⁺ would promote the adsorption of BSM onto kaolinite by increasing the hydrogen (H⁺) ions concentration in solution. The interactions of the heavy metal cations with the kaolinite could affect the structure and other properties such as swelling capacity, compaction capability and the double-layer behaviour of kaolinite. In addition, the substitution of H⁺ ions for metal ions could change the Van der Wals force within the kaolinite structure. All these might lead to the increased sorption of BSM onto kaolinite at the presence of Pb²⁺. Conclusions The addition of Pb²⁺ and the reduction of pH in solution would enhance the retention of BSM and thus effectively retard BSM from entering the aqueous phase. The mechanisms involved in the promotion effects of the spiked Pb²⁺ on adsorption might be primarily attributed to the increased hydrogen (H⁺) ions as a consequence of the addition of Pb²⁺. Recommendations and perspectives Further investigation would be required to give insight into the specific mechanism controlling the adsorption of BSM on kaolinite.
Background, aim and scope: The combined pollution of bensulfuron-methyl (BSM) and heavy metal Pb has been a common problem in agro-ecological environment in southern China. As an important natural clay mineral, the kaolinite structure possesses great advantages in many processes due to its high chemical stability and low expansion coefficient. The adsorption of BSM on kaolinite was therefore investigated at varying Pb super(2+) concentrations (0, 100, 500 and 1,000mg kg super(-1)) and different pH levels (3, 4 and 5) using the batch equilibration experiment. Materials and methods: BSM was purchased from Aldrich Chemical Co. (purity, 98%), used as the model compound in this study. The experimental kaolinite was sampled from Yuhang in Zhejiang Province. The metal salts used in the study are Pb(NO sub(3)) sub(2). The kaolinite samples were spiked with Pb at a rate of 100, 500 and 1,000mg kg super(-1) air-dried soil, respectively. The adsorption of BSM on kaolinite was investigated using the batch equilibration experiment. The BSM concentration of the filtrate was determined by high-pressure liquid chromatography. Results and discussion: The adsorption of BSM on kaolinite could be described by the Freundlich isotherm equation, with the R super(2) values greater than 0.959 in all experimental treatment. The presence of Pb super(2+) in kaolinite promoted the adsorption of BSM, and the higher Pb would generally lead to the stronger sorption of BSM by kaolinite based on the observed K sub(f) values. The adsorption of BSM on kaolinite declined with the increase of pH, and the spiked Pb super(2+) aggravated the reduction of adsorption of BSM. The exclusion between BSM and kaolinite was strengthened with the increase of pH, which partially elucidated the adsorption of BSM decreasing with increasing pH of the solution. Some adsorption of Pb super(2+) took place along the outer hydroxyl plane, therefore releasing H super(+) ions located there. The spiked Pb super(2+) would promote the adsorption of BSM onto kaolinite by increasing the hydrogen (H super(+)) ions concentration in solution. The interactions of the heavy metal cations with the kaolinite could affect the structure and other properties such as swelling capacity, compaction capability and the double-layer behaviour of kaolinite. In addition, the substitution of H super(+) ions for metal ions could change the Van der Wals force within the kaolinite structure. All these might lead to the increased sorption of BSM onto kaolinite at the presence of Pb super(2+). Conclusions: The addition of Pb super(2+) and the reduction of pH in solution would enhance the retention of BSM and thus effectively retard BSM from entering the aqueous phase. The mechanisms involved in the promotion effects of the spiked Pb super(2+) on adsorption might be primarily attributed to the increased hydrogen (H super(+)) ions as a consequence of the addition of Pb super(2+). Recommendations and perspectives: Further investigation would be required to give insight into the specific mechanism controlling the adsorption of BSM on kaolinite.
Background, aim and scope The combined pollution of bensulfuron-methyl (BSM) and heavy metal Pb has been a common problem in agro-ecological environment in southern China. As an important natural clay mineral, the kaolinite structure possesses great advantages in many processes due to its high chemical stability and low expansion coefficient. The adsorption of BSM on kaolinite was therefore investigated at varying Pb 2+ concentrations (0, 100, 500 and 1,000 mg kg −1 ) and different pH levels (3, 4 and 5) using the batch equilibration experiment. Materials and methods BSM was purchased from Aldrich Chemical Co. (purity, 98%), used as the model compound in this study. The experimental kaolinite was sampled from Yuhang in Zhejiang Province. The metal salts used in the study are Pb(NO 3 ) 2 . The kaolinite samples were spiked with Pb at a rate of 100, 500 and 1,000 mg kg −1 air-dried soil, respectively. The adsorption of BSM on kaolinite was investigated using the batch equilibration experiment. The BSM concentration of the filtrate was determined by high-pressure liquid chromatography. Results and discussion The adsorption of BSM on kaolinite could be described by the Freundlich isotherm equation, with the R 2 values greater than 0.959 in all experimental treatment. The presence of Pb 2+ in kaolinite promoted the adsorption of BSM, and the higher Pb would generally lead to the stronger sorption of BSM by kaolinite based on the observed K f values. The adsorption of BSM on kaolinite declined with the increase of pH, and the spiked Pb 2+ aggravated the reduction of adsorption of BSM. The exclusion between BSM and kaolinite was strengthened with the increase of pH, which partially elucidated the adsorption of BSM decreasing with increasing pH of the solution. Some adsorption of Pb 2+ took place along the outer hydroxyl plane, therefore releasing H + ions located there. The spiked Pb 2+ would promote the adsorption of BSM onto kaolinite by increasing the hydrogen (H + ) ions concentration in solution. The interactions of the heavy metal cations with the kaolinite could affect the structure and other properties such as swelling capacity, compaction capability and the double-layer behaviour of kaolinite. In addition, the substitution of H + ions for metal ions could change the Van der Wals force within the kaolinite structure. All these might lead to the increased sorption of BSM onto kaolinite at the presence of Pb 2+ . Conclusions The addition of Pb 2+ and the reduction of pH in solution would enhance the retention of BSM and thus effectively retard BSM from entering the aqueous phase. The mechanisms involved in the promotion effects of the spiked Pb 2+ on adsorption might be primarily attributed to the increased hydrogen (H + ) ions as a consequence of the addition of Pb 2+ . Recommendations and perspectives Further investigation would be required to give insight into the specific mechanism controlling the adsorption of BSM on kaolinite.
Author Wu, Wei-Hong
Feng, Zi-Song
Xie, Zheng-Miao
Xu, Jian-Ming
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CitedBy_id crossref_primary_10_4028_www_scientific_net_AMR_281_296
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Keywords Bensulfuron-methyl
Pb
Kaolinite
Isotherm models
Agro-ecological environment
Adorption
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SSID ssj0037161
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Snippet Background, aim and scope The combined pollution of bensulfuron-methyl (BSM) and heavy metal Pb has been a common problem in agro-ecological environment in...
Background, aim and scope The combined pollution of bensulfuron-methyl (BSM) and heavy metal Pb has been a common problem in agro-ecological environment in...
The combined pollution of bensulfuron-methyl (BSM) and heavy metal Pb has been a common problem in agro-ecological environment in southern China. As an...
Background, aim and scope: The combined pollution of bensulfuron-methyl (BSM) and heavy metal Pb has been a common problem in agro-ecological environment in...
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fao
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Publisher
StartPage 476
SubjectTerms Adsorption
Agriculture
Cations
Contamination
Earth and Environmental Science
Environment
Environmental Physics
Filtrate
Heavy metals
Kaolinite
Liquid chromatography
Metal ions
Metals
Minerals
Pollution
Sec 3 • Remediation & Manage of Contaminated Lands • Research Article
Soil Science & Conservation
Soils
Sorption
Studies
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Title Adsorption of bensulfuron-methyl on kaolinite as influenced by Pb contamination
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