Hydrophobic Association of Random Copolymers of Sodium 2-(Acrylamido)-2-methylpropanesulfonate and Dodecyl Methacrylate in Water As Studied by Fluorescence and Dynamic Light Scattering
The association behavior of random copolymers of sodium 2-(acrylamido)-2-methylpropanesulfonate (AMPS) and dodecyl methacrylate (DMA) with its content (f DMA) varying from 1 to 15 mol % was investigated by fluorescence and quasielastic light scattering (QELS) techniques in 0.1 M NaCl aqueous solutio...
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Published in | Macromolecules Vol. 32; no. 14; pp. 4631 - 4640 |
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Main Authors | , |
Format | Journal Article |
Language | English |
Published |
Washington, DC
American Chemical Society
13.07.1999
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Abstract | The association behavior of random copolymers of sodium 2-(acrylamido)-2-methylpropanesulfonate (AMPS) and dodecyl methacrylate (DMA) with its content (f DMA) varying from 1 to 15 mol % was investigated by fluorescence and quasielastic light scattering (QELS) techniques in 0.1 M NaCl aqueous solutions. The association behavior of the copolymers was found to depend strongly on f DMA. When f DMA < 3 mol %, some polymer chains exist as unimers with a hydrodynamic radius (R h) of about 5 nm while some polymers form multipolymer aggregates with R h ≈ 100 nm, arising from “hydrophobic cross-linking” by the interpolymer association of dodecyl groups. When f DMA is increased to 9 mol %, interpolymer hydrophobe associations lead to the formation of a multipolymer micelle with R h ≈ 10−13 nm. The aggregation number (N agg) of dodecyl groups in a micelle core was estimated to be about 195. When f DMA is further increased to 15 mol %, R h for the multipolymer micelle markedly increases to 70−180 nm, the size increasing with increasing polymer concentration, whereas N agg remains constant at about 158 independent of the polymer concentration. On the basis of the results from the fluorescence and QELS measurements, a unicore micelle model was proposed for the copolymer with f DMA = 9 mol %, and a bridged micelle model was proposed for the copolymer with f DMA = 15 mol %. |
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AbstractList | The association behavior of random copolymers of sodium 2-(acrylamido)-2-methylpropanesulfonate (AMPS) and dodecyl methacrylate (DMA) with its content (f DMA) varying from 1 to 15 mol % was investigated by fluorescence and quasielastic light scattering (QELS) techniques in 0.1 M NaCl aqueous solutions. The association behavior of the copolymers was found to depend strongly on f DMA. When f DMA < 3 mol %, some polymer chains exist as unimers with a hydrodynamic radius (R h) of about 5 nm while some polymers form multipolymer aggregates with R h ≈ 100 nm, arising from “hydrophobic cross-linking” by the interpolymer association of dodecyl groups. When f DMA is increased to 9 mol %, interpolymer hydrophobe associations lead to the formation of a multipolymer micelle with R h ≈ 10−13 nm. The aggregation number (N agg) of dodecyl groups in a micelle core was estimated to be about 195. When f DMA is further increased to 15 mol %, R h for the multipolymer micelle markedly increases to 70−180 nm, the size increasing with increasing polymer concentration, whereas N agg remains constant at about 158 independent of the polymer concentration. On the basis of the results from the fluorescence and QELS measurements, a unicore micelle model was proposed for the copolymer with f DMA = 9 mol %, and a bridged micelle model was proposed for the copolymer with f DMA = 15 mol %. |
Author | Noda, Tetsuya Morishima, Yotaro |
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Keywords | Alkyl methacrylate copolymer Hydrodynamic radius Property composition relationship Hydrophobic interaction Acrylamide derivative copolymer Experimental study Lateral group Sulfonate copolymer Polyelectrolyte Random copolymer Solution structure Concentration effect Molecular association Hydrophobic group Aqueous solution Micellization |
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Snippet | The association behavior of random copolymers of sodium 2-(acrylamido)-2-methylpropanesulfonate (AMPS) and dodecyl methacrylate (DMA) with its content (f DMA)... |
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SubjectTerms | Applied sciences Exact sciences and technology Organic polymers Physicochemistry of polymers Properties and characterization Solution and gel properties |
Title | Hydrophobic Association of Random Copolymers of Sodium 2-(Acrylamido)-2-methylpropanesulfonate and Dodecyl Methacrylate in Water As Studied by Fluorescence and Dynamic Light Scattering |
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