Environment-Friendly Bromination of Aromatic Heterocycles Using a Bromide–Bromate Couple in an Aqueous Medium
Selective monobromination of aromatic heterocyclic compounds through in-situ acid activation of 2:1 bromide/bromate couple as a benign brominating reagent is described. The in-situ acid activation of a bromide–bromate couple generates the reactive species BrOH, and it is proved to be an efficient fo...
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| Published in | Industrial & engineering chemistry research Vol. 50; no. 21; pp. 12271 - 12275 |
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| Main Authors | , |
| Format | Journal Article |
| Language | English |
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American Chemical Society
02.11.2011
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| Abstract | Selective monobromination of aromatic heterocyclic compounds through in-situ acid activation of 2:1 bromide/bromate couple as a benign brominating reagent is described. The in-situ acid activation of a bromide–bromate couple generates the reactive species BrOH, and it is proved to be an efficient for the bromination of various heterocycles under mild aqueous conditions without the use of any catalyst. Heterocycles that had electron-rich substituents provided good yields. |
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| AbstractList | Selective monobromination of aromatic heterocyclic compounds through in-situ acid activation of 2:1 bromide/bromate couple as a benign brominating reagent is described. The in-situ acid activation of a bromide–bromate couple generates the reactive species BrOH, and it is proved to be an efficient for the bromination of various heterocycles under mild aqueous conditions without the use of any catalyst. Heterocycles that had electron-rich substituents provided good yields. |
| Author | Joshi, Girdhar Adimurthy, Subbarayappa |
| AuthorAffiliation | Analytical Science Discipline Central Salt & Marine Chemicals Research Institute (CSIR) |
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| SubjectTerms | Activation Applied sciences Aromatic compounds Bromates Bromides Bromination Chemical engineering Exact sciences and technology Heterocyclic compounds Industrial engineering Joining |
| Title | Environment-Friendly Bromination of Aromatic Heterocycles Using a Bromide–Bromate Couple in an Aqueous Medium |
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