Crystal Structure of the Gold Nanoparticle [N(C8H17)4][Au25(SCH2CH2Ph)18]
We report the crystal structure of the thiolate gold nanoparticle [TOA+][Au25(SCH2CH2Ph)18 -], where TOA+ = N(C8H17)4 +. The crystal structure reveals three types of gold atoms: (a) one central gold atom whose coordination number is 12 (12 bonds to gold atoms); (b) 12 gold atoms that form the verti...
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| Published in | Journal of the American Chemical Society Vol. 130; no. 12; pp. 3754 - 3755 |
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| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
United States
American Chemical Society
26.03.2008
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| Subjects | |
| Online Access | Get full text |
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| Abstract | We report the crystal structure of the thiolate gold nanoparticle [TOA+][Au25(SCH2CH2Ph)18 -], where TOA+ = N(C8H17)4 +. The crystal structure reveals three types of gold atoms: (a) one central gold atom whose coordination number is 12 (12 bonds to gold atoms); (b) 12 gold atoms that form the vertices of an icosahedron around the central atom, whose coordination number is 6 (five bonds to gold atoms and one to a sulfur atom), and (c) 12 gold atoms that are stellated on 12 of the 20 faces of the Au13 icosahedron. The arrangement of the latter gold atoms may be influenced by aurophilic bonding. Together they form six orthogonal semirings, or staples, of −Au2(SCH2CH2Ph)3− in an octahedral arrangement around the Au13 core. |
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| AbstractList | We report the crystal structure of the thiolate gold nanoparticle [TOA+][Au25(SCH2CH2Ph)18 -], where TOA+ = N(C8H17)4 +. The crystal structure reveals three types of gold atoms: (a) one central gold atom whose coordination number is 12 (12 bonds to gold atoms); (b) 12 gold atoms that form the vertices of an icosahedron around the central atom, whose coordination number is 6 (five bonds to gold atoms and one to a sulfur atom), and (c) 12 gold atoms that are stellated on 12 of the 20 faces of the Au13 icosahedron. The arrangement of the latter gold atoms may be influenced by aurophilic bonding. Together they form six orthogonal semirings, or staples, of −Au2(SCH2CH2Ph)3− in an octahedral arrangement around the Au13 core. We report the crystal structure of the thiolate gold nanoparticle [TOA+][Au25(SCH2CH2Ph)18-], where TOA+ = N(C8H17)4+. The crystal structure reveals three types of gold atoms: (a) one central gold atom whose coordination number is 12 (12 bonds to gold atoms); (b) 12 gold atoms that form the vertices of an icosahedron around the central atom, whose coordination number is 6 (five bonds to gold atoms and one to a sulfur atom), and (c) 12 gold atoms that are stellated on 12 of the 20 faces of the Au13 icosahedron. The arrangement of the latter gold atoms may be influenced by aurophilic bonding. Together they form six orthogonal semirings, or staples, of -Au2(SCH2CH2Ph)3- in an octahedral arrangement around the Au13 core. |
| Author | Murray, Royce W White, Peter S Heaven, Michael W Dass, Amala Holt, Kennedy M |
| Author_xml | – sequence: 1 givenname: Michael W surname: Heaven fullname: Heaven, Michael W – sequence: 2 givenname: Amala surname: Dass fullname: Dass, Amala – sequence: 3 givenname: Peter S surname: White fullname: White, Peter S – sequence: 4 givenname: Kennedy M surname: Holt fullname: Holt, Kennedy M – sequence: 5 givenname: Royce W surname: Murray fullname: Murray, Royce W |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/18321116$$D View this record in MEDLINE/PubMed |
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| Snippet | We report the crystal structure of the thiolate gold nanoparticle [TOA+][Au25(SCH2CH2Ph)18 -], where TOA+ = N(C8H17)4 +. The crystal structure reveals three... We report the crystal structure of the thiolate gold nanoparticle [TOA+][Au25(SCH2CH2Ph)18-], where TOA+ = N(C8H17)4+. The crystal structure reveals three... |
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| SubjectTerms | Crystallography, X-Ray Gold - chemistry Ligands Models, Molecular Nanoparticles - chemistry Organogold Compounds - chemistry Sulfhydryl Compounds - chemistry |
| Title | Crystal Structure of the Gold Nanoparticle [N(C8H17)4][Au25(SCH2CH2Ph)18] |
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