Thermogravimetry/gas chromatography/mass spectrometry and thermogravimetry/gas chromatography/Fourier transform infrared spectroscopy: Novel hyphenated methods in thermal analysis
Two doubly hyphenated, thermogravimetry-based analytical techniques are described. Example analyses on poly(alpha-methylstyrene) and wood demonstrate the techniques' capability for monitoring specific minor products and isomers.
Saved in:
| Published in | Analytical chemistry (Washington) Vol. 65; no. 20; pp. 2819 - 2823 |
|---|---|
| Main Authors | , , , , |
| Format | Journal Article |
| Language | English |
| Published |
Washington, DC
American Chemical Society
15.10.1993
|
| Subjects | |
| Online Access | Get full text |
Cover
Loading…
| Abstract | Two doubly hyphenated, thermogravimetry-based analytical techniques are described. Example analyses on poly(alpha-methylstyrene) and wood demonstrate the techniques' capability for monitoring specific minor products and isomers. |
|---|---|
| AbstractList | Two doubly hyphenated, thermogravimetry-based analytical techniques are described. Example analyses on poly(alpha-methylstyrene) and wood demonstrate the techniques' capability for monitoring specific minor products and isomers. Two doubly hyphenated, thermogravimetry-based analytical techniques, viz. TG/GC/MS and TG/GC/IR, are described. A valveless, quartz, heated sample path between TG furnace and GC column minimizes losses of products. Furthermore, combination of a pulsed automated vapor sampling inlet and a transfer line type GC column permits high-speed GC identification of individual TG products while maintaining sufficiently high temporal resolution with the approximately 1-min sampling interval to provide kinetic information about the underlying reaction mechanisms. Example analyses on poly([alpha]-methylstyrene), a styrene-isoprene block copolymer, and wood demonstrate the techniques' capability for monitoring specific minor products and isomers. 32 refs., 5 figs. |
| Author | Dworzanski, Jacek P Buchanan, Richard M Meuzelaar, Henk L. C McClennen, William H Arnold, Neil S |
| Author_xml | – sequence: 1 givenname: William H surname: McClennen fullname: McClennen, William H – sequence: 2 givenname: Richard M surname: Buchanan fullname: Buchanan, Richard M – sequence: 3 givenname: Neil S surname: Arnold fullname: Arnold, Neil S – sequence: 4 givenname: Jacek P surname: Dworzanski fullname: Dworzanski, Jacek P – sequence: 5 givenname: Henk L. C surname: Meuzelaar fullname: Meuzelaar, Henk L. C |
| BackLink | http://pascal-francis.inist.fr/vibad/index.php?action=getRecordDetail&idt=3775577$$DView record in Pascal Francis https://www.osti.gov/biblio/5070066$$D View this record in Osti.gov |
| BookMark | eNqNkctu1TAQhi3USpwWVrxAhJBYoPSMnThO2KGKQqWKcjmoS2uO4zQpSZx63Io8Fy9YH6UXFixYjTTzzT__zBywvdGNlrFXHI44CL5GAwBFicCrZ2zFpYC0KEuxx1Yxn6VCATxnB0RXAJwDL1bsz6a1fnCXHm-7wQY_ry-REtN6N2DYpad2Xg9IlNBkTYjpHZTgWCfhPzpP3I3vrE-Cx5Ea54ekGxuP3tYPemTcNL9Pvrhb2yftPLV2xBDLUbJ1NUV-GYR9HIr9TB29YPsN9mRf3sdD9vPk4-b4c3p2_un0-MNZilmZh1RWXKCs67oS3EJeWRBCcZtXNXCZbctmy4smMk0mtzKTQlrTlE2dI0Bui1xmh-z1ousodJpMF6xpjRvHaFxLiMcsiido8u76xlLQV3Hn6JS04KrMq1LtlN4tkIkLk7eNnnw3oJ81B737nP7rc5F-cy-JZLCP9xpNR48tmVJSKhWxdME6Cvb3Yxn9L12oTEm9-fpDZ9_FxbeLqtQ88m8XHg09mfyXgTtZybru |
| CODEN | ANCHAM |
| CitedBy_id | crossref_primary_10_1016_j_impact_2023_100467 crossref_primary_10_1016_j_chroma_2015_07_091 crossref_primary_10_1016_j_jaap_2018_03_023 crossref_primary_10_1016_S0040_6031_97_00097_X crossref_primary_10_1016_j_apenergy_2011_07_029 crossref_primary_10_1016_j_chroma_2014_09_073 crossref_primary_10_1016_S0040_6031_99_00203_8 crossref_primary_10_1366_0003702963905231 crossref_primary_10_1002_pen_10659 crossref_primary_10_1007_BF02547421 crossref_primary_10_1080_05704929808006777 crossref_primary_10_1016_j_chroma_2014_05_057 crossref_primary_10_1016_S0040_6031_98_00592_9 crossref_primary_10_1080_05704929708003320 crossref_primary_10_1366_0003702981944724 crossref_primary_10_1016_S0165_2370_99_00024_8 crossref_primary_10_1007_s10973_016_5773_3 crossref_primary_10_1016_j_jaap_2017_10_005 crossref_primary_10_1016_S0040_6031_99_00013_1 crossref_primary_10_1016_S0040_6031_98_00496_1 crossref_primary_10_1016_0003_2670_94_85027_5 crossref_primary_10_1016_S0040_6031_00_00675_4 crossref_primary_10_1063_1_1148397 crossref_primary_10_1007_BF01979209 crossref_primary_10_1002_1097_4628_20000815_77_7_1629__AID_APP25_3_0_CO_2_J crossref_primary_10_1021_ie960335i crossref_primary_10_1016_S0021_9673_98_00448_8 crossref_primary_10_1155_2017_4149592 crossref_primary_10_1016_S0040_6031_98_00478_X crossref_primary_10_1016_j_ijms_2008_12_002 crossref_primary_10_3390_f15010008 crossref_primary_10_1016_S0165_2370_96_00956_4 crossref_primary_10_1021_ac801757w crossref_primary_10_1021_ac961265s crossref_primary_10_1021_ac970554t |
| ContentType | Journal Article |
| Copyright | 1994 INIST-CNRS Copyright American Chemical Society Oct 15, 1993 |
| Copyright_xml | – notice: 1994 INIST-CNRS – notice: Copyright American Chemical Society Oct 15, 1993 |
| DBID | BSCLL IQODW AAYXX CITATION 7QF 7QO 7QQ 7SC 7SE 7SP 7SR 7TA 7TB 7TM 7U5 7U7 7U9 8BQ 8FD C1K F28 FR3 H8D H8G H94 JG9 JQ2 KR7 L7M L~C L~D P64 OTOTI |
| DOI | 10.1021/ac00068a019 |
| DatabaseName | Istex Pascal-Francis CrossRef Aluminium Industry Abstracts Biotechnology Research Abstracts Ceramic Abstracts Computer and Information Systems Abstracts Corrosion Abstracts Electronics & Communications Abstracts Engineered Materials Abstracts Materials Business File Mechanical & Transportation Engineering Abstracts Nucleic Acids Abstracts Solid State and Superconductivity Abstracts Toxicology Abstracts Virology and AIDS Abstracts METADEX Technology Research Database Environmental Sciences and Pollution Management ANTE: Abstracts in New Technology & Engineering Engineering Research Database Aerospace Database Copper Technical Reference Library AIDS and Cancer Research Abstracts Materials Research Database ProQuest Computer Science Collection Civil Engineering Abstracts Advanced Technologies Database with Aerospace Computer and Information Systems Abstracts Academic Computer and Information Systems Abstracts Professional Biotechnology and BioEngineering Abstracts OSTI.GOV |
| DatabaseTitle | CrossRef Materials Research Database Technology Research Database Computer and Information Systems Abstracts – Academic Mechanical & Transportation Engineering Abstracts Nucleic Acids Abstracts ProQuest Computer Science Collection Computer and Information Systems Abstracts Materials Business File Environmental Sciences and Pollution Management Aerospace Database Copper Technical Reference Library Engineered Materials Abstracts Biotechnology Research Abstracts AIDS and Cancer Research Abstracts Advanced Technologies Database with Aerospace ANTE: Abstracts in New Technology & Engineering Civil Engineering Abstracts Aluminium Industry Abstracts Virology and AIDS Abstracts Toxicology Abstracts Electronics & Communications Abstracts Ceramic Abstracts METADEX Biotechnology and BioEngineering Abstracts Computer and Information Systems Abstracts Professional Solid State and Superconductivity Abstracts Engineering Research Database Corrosion Abstracts |
| DatabaseTitleList | Materials Research Database |
| DeliveryMethod | fulltext_linktorsrc |
| Discipline | Engineering Chemistry |
| EISSN | 1520-6882 |
| EndPage | 2823 |
| ExternalDocumentID | 5070066 5764365 10_1021_ac00068a019 3775577 ark_67375_TPS_3R2WQW98_1 d290763840 |
| GroupedDBID | - .K2 02 08R 186 1AW 1WB 23M 2KS 3EH 3O- 53G 53T 55A 5GY 5RE 5VS 6XO 85S AABXI AAUTI ABDEX ABFLS ABMVS ABOCM ABPPZ ABPTK ABUFD ACGFS ACGOD ACIWK ACJ ACKIV ACNCT ACPRK ACPVT ACS AENEX AETEA AFFDN AFFNX AFMIJ AFRAH AGXLV AIDAL ALMA_UNASSIGNED_HOLDINGS ANTXH AQSVZ BAANH CS3 D0L DZ EBS F20 F5P G8K GJ HR JG JG~ K2 K78 MVM NHB OHM OHT OMK P2P PQEST PQQKQ RNS ROL RXW TAE TAF TN5 UBX UHB UKR UNC UQL VOH VQA W1F WH7 X X6Y XFK YXE YZZ ZCG ZE2 ZGI --- -DZ -~X .DC .GJ .HR 6J9 6TJ ABHFT ABHMW ABJNI ACBEA ACGFO ACKOT ACQAM AHGAQ BSCLL GGK KZ1 UBC VF5 VG9 XOL XSW YYP ZCA ~02 4.4 7~N ABFRP ABQRX ABUCX ADHLV AEESW AFDAS AFEFF BKOMP ED~ EJD GNL IH9 IHE IQODW LG6 LMP UI2 YQI YQJ AAHBH AAYXX CITATION 7QF 7QO 7QQ 7SC 7SE 7SP 7SR 7TA 7TB 7TM 7U5 7U7 7U9 8BQ 8FD C1K F28 FR3 H8D H8G H94 JG9 JQ2 KR7 L7M L~C L~D P64 OTOTI |
| ID | FETCH-LOGICAL-a384t-5912a5ddd921e049e02271e49d0153b8fb16f912f35b53525ecf8fd4a004e6453 |
| IEDL.DBID | ACS |
| ISSN | 0003-2700 |
| IngestDate | Thu May 18 22:21:51 EDT 2023 Wed Sep 25 01:50:31 EDT 2024 Fri Aug 23 01:05:30 EDT 2024 Sun Oct 29 17:09:38 EDT 2023 Wed Jan 17 04:53:20 EST 2024 Thu Aug 27 13:41:59 EDT 2020 |
| IsPeerReviewed | true |
| IsScholarly | true |
| Issue | 20 |
| Keywords | Fourier transformation Wood Coupled method Reaction product Thermogravimetry Instrumentation Polymer Isomer Infrared spectrometry Gas chromatography Reaction mechanism Thermal analysis Kinetics Measurement method Mass spectrometry |
| Language | English |
| License | CC BY 4.0 |
| LinkModel | DirectLink |
| MergedId | FETCHMERGED-LOGICAL-a384t-5912a5ddd921e049e02271e49d0153b8fb16f912f35b53525ecf8fd4a004e6453 |
| Notes | ark:/67375/TPS-3R2WQW98-1 istex:942A7AA1048D9F7F6130934BB5A175B38DB1495D |
| PQID | 217849875 |
| PQPubID | 45400 |
| PageCount | 5 |
| ParticipantIDs | osti_scitechconnect_5070066 proquest_journals_217849875 crossref_primary_10_1021_ac00068a019 pascalfrancis_primary_3775577 istex_primary_ark_67375_TPS_3R2WQW98_1 acs_journals_10_1021_ac00068a019 |
| ProviderPackageCode | JG~ 55A AABXI ACJ AGXLV W1F ANTXH ACS .K2 ABMVS 1WB BAANH AQSVZ |
| PublicationCentury | 1900 |
| PublicationDate | 1993-10-15 |
| PublicationDateYYYYMMDD | 1993-10-15 |
| PublicationDate_xml | – month: 10 year: 1993 text: 1993-10-15 day: 15 |
| PublicationDecade | 1990 |
| PublicationPlace | Washington, DC |
| PublicationPlace_xml | – name: Washington, DC – name: Washington – name: United States |
| PublicationTitle | Analytical chemistry (Washington) |
| PublicationTitleAlternate | Anal. Chem |
| PublicationYear | 1993 |
| Publisher | American Chemical Society |
| Publisher_xml | – name: American Chemical Society |
| SSID | ssj0011016 |
| Score | 1.6449049 |
| Snippet | Two doubly hyphenated, thermogravimetry-based analytical techniques are described. Example analyses on poly(alpha-methylstyrene) and wood demonstrate the... Two doubly hyphenated, thermogravimetry-based analytical techniques, viz. TG/GC/MS and TG/GC/IR, are described. A valveless, quartz, heated sample path between... |
| SourceID | osti proquest crossref pascalfrancis istex acs |
| SourceType | Open Access Repository Aggregation Database Index Database Publisher |
| StartPage | 2819 |
| SubjectTerms | 360602 - Other Materials- Structure & Phase Studies 400100 - Analytical & Separations Chemistry ALKYLATED AROMATICS Analytical chemistry AROMATICS CHEMICAL ANALYSIS Chemical and thermal methods CHEMICAL REACTION KINETICS Chemistry CHROMATOGRAPHY COPOLYMERS DETECTION DIENES Exact sciences and technology FOURIER TRANSFORM SPECTROMETERS GAS CHROMATOGRAPHY GRAVIMETRIC ANALYSIS HYDROCARBONS IMPURITIES INFRARED SPECTRA INFRARED SPECTROMETERS INORGANIC, ORGANIC, PHYSICAL AND ANALYTICAL CHEMISTRY ISOMERS ISOPRENE KINETICS MASS SPECTROSCOPY MATERIALS MATERIALS SCIENCE MEASURING INSTRUMENTS MONITORING ORGANIC COMPOUNDS ORGANIC POLYMERS PETROCHEMICALS PETROLEUM PRODUCTS PLASTICS POLYENES POLYMERS POLYOLEFINS POLYSTYRENE POLYVINYLS PULSE TECHNIQUES QUANTITATIVE CHEMICAL ANALYSIS REACTION KINETICS RESOLUTION SAMPLING SEPARATION PROCESSES SPECTRA SPECTROMETERS SPECTROSCOPY STYRENE SYNTHETIC MATERIALS THERMAL ANALYSIS THERMAL GRAVIMETRIC ANALYSIS WOOD |
| Title | Thermogravimetry/gas chromatography/mass spectrometry and thermogravimetry/gas chromatography/Fourier transform infrared spectroscopy: Novel hyphenated methods in thermal analysis |
| URI | http://dx.doi.org/10.1021/ac00068a019 https://api.istex.fr/ark:/67375/TPS-3R2WQW98-1/fulltext.pdf https://www.proquest.com/docview/217849875/abstract/ https://www.osti.gov/biblio/5070066 |
| Volume | 65 |
| hasFullText | 1 |
| inHoldings | 1 |
| isFullTextHit | |
| isPrint | |
| link | http://utb.summon.serialssolutions.com/2.0.0/link/0/eLvHCXMwjV3LbtQwFL1C7QK64FGoGEqRF1V3aWvHzjjs0IhRxaKCPtTuLMePthpmBiVpRfktfpB785i-EHQ3UuxknJxrnysfnwuwmRYZpj3DLHF4OZEBf1nESaKj8IhpLqJtVL772d6x_HKqTm9ENPd38AXfsY6mVG13ydxzWZB2kBjQ6HCxWUAJaF8Yj_ZRu2N49zrT8uOqO8vPMr3JnzgZzzGcSBVpK3wxsa1o8WByblac8QsY9-d2WqHJZPuyLrbdr4c2jv8ezEt43nFO9qkFySt4Emar8HTUl3pbhZVbroSv4TdCp5ySbOvqYhqo7siZrZg7L-fIbjuH650pkm7WHNMkvwNsxOzMs_oRPcdtlTxW95SZIchL0sH396OTMtcf2f78Knxn59ekQkNG7Flb7brC9u2DcEy281R5A8fjz0ejvaSr7ZDYVMs6UTkXVnnvc8EDZimBrAx5kLlHfpIWOhY8i9gmpqogBxoVXNTRS4tBHTKp0jVYms1n4S0wHVwhuBf5roxSDYdW54izFBM9j1zYyQEw_PCmi83KNNvugptb32IAmz0qzI_W5ePvzbYaxCza2HJCwrihMkdfD016IE6-neTa8AGsE6QMshiy4nWkWXK1Qe5NFG8AG3eQtrgdBo3CAWDvHnk3_xpTRy1zzC7f_X846_Cs0WWS8Ea9h6W6vAwbyJ3q4kMTOX8AIoUVUQ |
| link.rule.ids | 230,315,786,790,891,2782,27109,27957,27958,57093,57143 |
| linkProvider | American Chemical Society |
| linkToHtml | http://utb.summon.serialssolutions.com/2.0.0/link/0/eLvHCXMwjV1Nb9QwEB1V7aFwKFBAbEvBh4oTaZvEThxu1YrVAu0K6FbtzXJsh1bt7qIkrSh_q3-QGSfZfoBEbytl7LWTN_YbefwGYDPOEwx70iQw-DjgDn9pxEkgi8gipsOo0D7Ld5QMD_nnY3G8AO-7uzA4iAp7qvwh_o26QLitDa2sUu-QxueSSDESJyLUP5ifGVAc2tXHo-PU9jbevca0C5nqzi60RC_0F67JM_QqSo7UFb6foils8dca7TeewRPYnw_Z55ucbV3U-Zb5fU_N8aFzegorLQNluw1knsGCm67Ccr8r_LYKj29pFD6HawRSOaEkrsvTiaMqJD90xcxJOUOu2-pdb0-QgjN_aZPUD9CI6all9QNaDpqaeazuCDRDyJeUFd_1R_dmrj6w0ezSnbOTK8pJQ35sWVP7ukL75o9wTrpVWHkBh4OP4_4waCs9BDqWvA5EFkZaWGuzKHQYszgSNgwdzyyylTiXRR4mBdoUschJj0Y4U8jCco0u7hIu4pewOJ1N3Stg0pk8Cm2U7fCCizTVMkPUxRj2WWTGhveA4adQradWyh_CR6G69S16sNmBQ_1sND_-bfbOA2duo8szSpNLhRp_PVDx9-jo21EmVdiDdUKWQk5DwryGMphMrZCJE-HrwcYdwM27QxcSOAFs3QHwZtQYSEqeYay59v_pvIXl4Xh_T-19Gn1Zh0c-Y5NScsRrWKzLC7eBrKrO33hn-gN1eB28 |
| linkToPdf | http://utb.summon.serialssolutions.com/2.0.0/link/0/eLvHCXMwlV1ZT9wwEB4hkHo89KBF3VJaP6C-BdaJnXX6hras6KEVFBC8WY6PUtHdRUlApX-LP9iZHMvRSm3fVsrYayff2N_I428A1pM8xbBnkEYWH0fC4y-DOIlUiB1imsfB1Fm-43TnUHw8lscL0O_uwuAgSuyprA_xyavPXGgVBvimsbS6KtMnnc8lSaW7iQwN9-fnBhSLdjXy6Ei1vZF3pzHtRLa8tRMt0Uv9gevyDD2LEiRNie8oNMUtflun681n9Bj25sOuc05ON86rfMP-vKPo-D_zegKPWibKthroPIUFP12G-8OuANwyPLyhVfgMrhBQxYSSuS6-TTxVI_lqSmZPihly3lb3enOCVJzVlzdJBQGNmJk6Vv1Dy1FTO49VHZFmCP2CsuO7_uj-zOU7Np5d-O_s5JJy05AnO9bUwC7RvvkjnJNplVaew-Fo-2C4E7UVHyKTKFFFMuOxkc65LOYeYxdPAofci8wha0lyFXKeBrQJicxJl0Z6G1RwwqCr-1TIZAUWp7OpfwFMeZvH3MVZXwQhBwOjMkRfguGfQ4ZsRQ8Yfg7demyp68P4mOsb36IH6x1A9Fmj_fFns7c1eOY2pjildLmB1Ae7-zr5Eh_tHWVK8x6sEro0chsS6LWUyWQrjYyciF8P1m6Bbt4dupLECWDrDoTXo8aAUokMY86Xf5_OG7i3-36kP38Yf1qFB3XiJmXmyFewWBXnfg3JVZW_rv3pF3REIDY |
| openUrl | ctx_ver=Z39.88-2004&ctx_enc=info%3Aofi%2Fenc%3AUTF-8&rfr_id=info%3Asid%2Fsummon.serialssolutions.com&rft_val_fmt=info%3Aofi%2Ffmt%3Akev%3Amtx%3Ajournal&rft.genre=article&rft.atitle=Thermogravimetry%2Fgas+chromatography%2Fmass+spectrometry+and+thermogravimetry%2Fgas+chromatography%2FFourier+transform+infrared+spectroscopy%3A+Novel+hyphenated+methods+in+thermal+analysis&rft.jtitle=Analytical+chemistry+%28Washington%29&rft.au=McClennen%2C+William+H&rft.au=Buchanan%2C+Richard+M&rft.au=Arnold%2C+Neil+S&rft.au=Dworzanski%2C+Jacek+P&rft.date=1993-10-15&rft.pub=American+Chemical+Society&rft.issn=0003-2700&rft.eissn=1520-6882&rft.volume=65&rft.issue=20&rft.spage=2819&rft_id=info:doi/10.1021%2Fac00068a019&rft.externalDBID=NO_FULL_TEXT&rft.externalDocID=5764365 |
| thumbnail_l | http://covers-cdn.summon.serialssolutions.com/index.aspx?isbn=/lc.gif&issn=0003-2700&client=summon |
| thumbnail_m | http://covers-cdn.summon.serialssolutions.com/index.aspx?isbn=/mc.gif&issn=0003-2700&client=summon |
| thumbnail_s | http://covers-cdn.summon.serialssolutions.com/index.aspx?isbn=/sc.gif&issn=0003-2700&client=summon |