Formation of a Strandlike Polycatenane of Icosahedral Cages for Reversible One-Dimensional Encapsulation of Guests

Self-assembly of ZnCl2 and the ligand 2,4,6-tris(4-pyridyl)pyridine (pytpy) in solution yields [(ZnCl2)12(pytpy)8] n ·xCHCl3, a polycatenane consisting of a strand of mechanically interlocking icosahedral cages with an inner volume of more than 2700 Å3. This can be used to encapsulate guest molecule...

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Published inJournal of the American Chemical Society Vol. 133; no. 26; pp. 10018 - 10021
Main Authors Heine, Johanna, Schmedt auf der Günne, Jörn, Dehnen, Stefanie
Format Journal Article
LanguageEnglish
Published United States American Chemical Society 06.07.2011
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Abstract Self-assembly of ZnCl2 and the ligand 2,4,6-tris(4-pyridyl)pyridine (pytpy) in solution yields [(ZnCl2)12(pytpy)8] n ·xCHCl3, a polycatenane consisting of a strand of mechanically interlocking icosahedral cages with an inner volume of more than 2700 Å3. This can be used to encapsulate guest molecules of appropriate size and polarity, forming a precisely defined three-dimensional array of solvent nanodroplets within the crystalline framework. The dynamic composition of these droplets was studied using quantitative solid-state NMR spectroscopy.
AbstractList Self-assembly of ZnCl(2) and the ligand 2,4,6-tris(4-pyridyl)pyridine (pytpy) in solution yields [(ZnCl(2))(12)(pytpy)(8)](n)·xCHCl(3), a polycatenane consisting of a strand of mechanically interlocking icosahedral cages with an inner volume of more than 2700 Å(3). This can be used to encapsulate guest molecules of appropriate size and polarity, forming a precisely defined three-dimensional array of solvent nanodroplets within the crystalline framework. The dynamic composition of these droplets was studied using quantitative solid-state NMR spectroscopy.
Self-assembly of ZnCl2 and the ligand 2,4,6-tris(4-pyridyl)pyridine (pytpy) in solution yields [(ZnCl2)12(pytpy)8] n ·xCHCl3, a polycatenane consisting of a strand of mechanically interlocking icosahedral cages with an inner volume of more than 2700 Å3. This can be used to encapsulate guest molecules of appropriate size and polarity, forming a precisely defined three-dimensional array of solvent nanodroplets within the crystalline framework. The dynamic composition of these droplets was studied using quantitative solid-state NMR spectroscopy.
Author Heine, Johanna
Dehnen, Stefanie
Schmedt auf der Günne, Jörn
AuthorAffiliation Ludwig-Maximilians-Universität München
Philipps-Universität Marburg
AuthorAffiliation_xml – name: Ludwig-Maximilians-Universität München
– name: Philipps-Universität Marburg
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  givenname: Johanna
  surname: Heine
  fullname: Heine, Johanna
– sequence: 2
  givenname: Jörn
  surname: Schmedt auf der Günne
  fullname: Schmedt auf der Günne, Jörn
– sequence: 3
  givenname: Stefanie
  surname: Dehnen
  fullname: Dehnen, Stefanie
  email: stefanie.dehnen@staff.uni-marburg.de
BackLink https://www.ncbi.nlm.nih.gov/pubmed/21657228$$D View this record in MEDLINE/PubMed
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Snippet Self-assembly of ZnCl2 and the ligand 2,4,6-tris(4-pyridyl)pyridine (pytpy) in solution yields [(ZnCl2)12(pytpy)8] n ·xCHCl3, a polycatenane consisting of a...
Self-assembly of ZnCl(2) and the ligand 2,4,6-tris(4-pyridyl)pyridine (pytpy) in solution yields [(ZnCl(2))(12)(pytpy)(8)](n)·xCHCl(3), a polycatenane...
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StartPage 10018
Title Formation of a Strandlike Polycatenane of Icosahedral Cages for Reversible One-Dimensional Encapsulation of Guests
URI http://dx.doi.org/10.1021/ja2030273
https://www.ncbi.nlm.nih.gov/pubmed/21657228
https://search.proquest.com/docview/883847414
Volume 133
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