Enhanced Visible-Light Activity of Titania via Confinement inside Carbon Nanotubes

Titania confined inside carbon nanotubes (CNTs) was synthesized using a restrained hydrolysis method. Raman spectra and magnetic measurements using a SQUID magnetometer suggested the formation of remarkable oxygen vacancies over the encapsulated TiO2 in comparison with nanoparticles dispersed on the...

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Published inJournal of the American Chemical Society Vol. 133; no. 38; pp. 14896 - 14899
Main Authors Chen, Wei, Fan, Zhongli, Zhang, Bei, Ma, Guijun, Takanabe, Kazuhiro, Zhang, Xixiang, Lai, Zhiping
Format Journal Article
LanguageEnglish
Published United States American Chemical Society 28.09.2011
Subjects
Light
Nanotubes, Carbon - chemistry
Particle Size
Surface Properties
Titanium - chemistry
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Abstract Titania confined inside carbon nanotubes (CNTs) was synthesized using a restrained hydrolysis method. Raman spectra and magnetic measurements using a SQUID magnetometer suggested the formation of remarkable oxygen vacancies over the encapsulated TiO2 in comparison with nanoparticles dispersed on the outer surface of CNTs, extending the photoresponse of TiO2 from the UV to the visible-light region. The CNT-confined TiO2 exhibited improved visible-light activity in the degradation of methylene blue (MB) relative to the outside titania and commercial P25, which is attributed to the modification of the electronic structure of TiO2 induced by the unique confinement inside CNTs. These results provide further insight into the effect of confinement within CNTs, and the composites are expected to be promising for applications in visible-light photocatalysis.
AbstractList Titania confined inside carbon nanotubes (CNTs) was synthesized using a restrained hydrolysis method. Raman spectra and magnetic measurements using a SQUID magnetometer suggested the formation of remarkable oxygen vacancies over the encapsulated TiO(2) in comparison with nanoparticles dispersed on the outer surface of CNTs, extending the photoresponse of TiO(2) from the UV to the visible-light region. The CNT-confined TiO(2) exhibited improved visible-light activity in the degradation of methylene blue (MB) relative to the outside titania and commercial P25, which is attributed to the modification of the electronic structure of TiO(2) induced by the unique confinement inside CNTs. These results provide further insight into the effect of confinement within CNTs, and the composites are expected to be promising for applications in visible-light photocatalysis.Titania confined inside carbon nanotubes (CNTs) was synthesized using a restrained hydrolysis method. Raman spectra and magnetic measurements using a SQUID magnetometer suggested the formation of remarkable oxygen vacancies over the encapsulated TiO(2) in comparison with nanoparticles dispersed on the outer surface of CNTs, extending the photoresponse of TiO(2) from the UV to the visible-light region. The CNT-confined TiO(2) exhibited improved visible-light activity in the degradation of methylene blue (MB) relative to the outside titania and commercial P25, which is attributed to the modification of the electronic structure of TiO(2) induced by the unique confinement inside CNTs. These results provide further insight into the effect of confinement within CNTs, and the composites are expected to be promising for applications in visible-light photocatalysis.
Titania confined inside carbon nanotubes (CNTs) was synthesized using a restrained hydrolysis method. Raman spectra and magnetic measurements using a SQUID magnetometer suggested the formation of remarkable oxygen vacancies over the encapsulated TiO2 in comparison with nanoparticles dispersed on the outer surface of CNTs, extending the photoresponse of TiO2 from the UV to the visible-light region. The CNT-confined TiO2 exhibited improved visible-light activity in the degradation of methylene blue (MB) relative to the outside titania and commercial P25, which is attributed to the modification of the electronic structure of TiO2 induced by the unique confinement inside CNTs. These results provide further insight into the effect of confinement within CNTs, and the composites are expected to be promising for applications in visible-light photocatalysis.
Titania confined inside carbon nanotubes (CNTs) was synthesized using a restrained hydrolysis method. Raman spectra and magnetic measurements using a SQUID magnetometer suggested the formation of remarkable oxygen vacancies over the encapsulated TiO(2) in comparison with nanoparticles dispersed on the outer surface of CNTs, extending the photoresponse of TiO(2) from the UV to the visible-light region. The CNT-confined TiO(2) exhibited improved visible-light activity in the degradation of methylene blue (MB) relative to the outside titania and commercial P25, which is attributed to the modification of the electronic structure of TiO(2) induced by the unique confinement inside CNTs. These results provide further insight into the effect of confinement within CNTs, and the composites are expected to be promising for applications in visible-light photocatalysis.
Author Chen, Wei
Zhang, Xixiang
Lai, Zhiping
Fan, Zhongli
Ma, Guijun
Zhang, Bei
Takanabe, Kazuhiro
AuthorAffiliation Imaging and Characterization Laboratory
King Abdullah University of Science and Technology
Chemical and Life Sciences and Engineering Division
AuthorAffiliation_xml – name: King Abdullah University of Science and Technology
– name: Imaging and Characterization Laboratory
– name: Chemical and Life Sciences and Engineering Division
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  givenname: Wei
  surname: Chen
  fullname: Chen, Wei
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  givenname: Zhongli
  surname: Fan
  fullname: Fan, Zhongli
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BackLink https://www.ncbi.nlm.nih.gov/pubmed/21894970$$D View this record in MEDLINE/PubMed
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Snippet Titania confined inside carbon nanotubes (CNTs) was synthesized using a restrained hydrolysis method. Raman spectra and magnetic measurements using a SQUID...
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SubjectTerms Light
Nanotubes, Carbon - chemistry
Particle Size
Surface Properties
Titanium - chemistry
Title Enhanced Visible-Light Activity of Titania via Confinement inside Carbon Nanotubes
URI http://dx.doi.org/10.1021/ja205997x
https://www.ncbi.nlm.nih.gov/pubmed/21894970
https://www.proquest.com/docview/893719810
Volume 133
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