Phosphine-Free Perfluoro-Tagged Palladium Nanoparticles Supported on Fluorous Silica Gel:  Application to the Heck Reaction

The immobilization of phosphine-free perfluoro-tagged palladium nanoparticles Pd-1 on fluorous silica gel (FSG) and their utilization in the Heck reaction have been investigated. High yields of vinylic substitution products have been obtained. Recycling studies have shown that the solid-supported pa...

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Published inOrganic letters Vol. 10; no. 4; pp. 561 - 564
Main Authors Bernini, Roberta, Cacchi, Sandro, Fabrizi, Giancarlo, Forte, Giovanni, Niembro, Sandra, Petrucci, Francesco, Pleixats, Roser, Prastaro, Alessandro, Sebastián, Rosa Maria, Soler, Roger, Tristany, Mar, Vallribera, Adelina
Format Journal Article
LanguageEnglish
Published WASHINGTON American Chemical Society 21.02.2008
Amer Chemical Soc
Subjects
Chemistry
Chemistry, Organic
Physical Sciences
Science & Technology
REUSABLE CATALYST
SUZUKI
PD
COUPLING REACTIONS
CARBON AEROGELS
ACETATE
MIZOROKI-HECK
POLYUREA MICROCAPSULES
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Abstract The immobilization of phosphine-free perfluoro-tagged palladium nanoparticles Pd-1 on fluorous silica gel (FSG) and their utilization in the Heck reaction have been investigated. High yields of vinylic substitution products have been obtained. Recycling studies have shown that the solid-supported palladium catalyst can be readily recovered and reused several times without significant loss of activity. Reactions and recovery of the solid-supported palladium catalyst system can be carried out in the presence of air, without any particular precaution.
AbstractList The immobilization of phosphine-free perfluoro-tagged palladium nanoparticles Pd-1 on fluorous silica gel (FSG) and their utilization in the Heck reaction have been investigated. High yields of vinylic substitution products have been obtained. Recycling studies have shown that the solid-supported palladium catalyst can be readily recovered and reused several times without significant loss of activity. Reactions and recovery of the solid-supported palladium catalyst system can be carried out in the presence of air, without any particular precaution.
Author Cacchi, Sandro
Pleixats, Roser
Bernini, Roberta
Petrucci, Francesco
Sebastián, Rosa Maria
Tristany, Mar
Niembro, Sandra
Vallribera, Adelina
Prastaro, Alessandro
Forte, Giovanni
Soler, Roger
Fabrizi, Giancarlo
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  surname: Bernini
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  givenname: Giancarlo
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  givenname: Giovanni
  surname: Forte
  fullname: Forte, Giovanni
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  givenname: Sandra
  surname: Niembro
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  givenname: Francesco
  surname: Petrucci
  fullname: Petrucci, Francesco
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  givenname: Roser
  surname: Pleixats
  fullname: Pleixats, Roser
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  givenname: Alessandro
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  givenname: Adelina
  surname: Vallribera
  fullname: Vallribera, Adelina
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Issue 4
Keywords REUSABLE CATALYST
SUZUKI
PD
COUPLING REACTIONS
CARBON AEROGELS
ACETATE
MIZOROKI-HECK
POLYUREA MICROCAPSULES
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Snippet The immobilization of phosphine-free perfluoro-tagged palladium nanoparticles Pd-1 on fluorous silica gel (FSG) and their utilization in the Heck reaction have...
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SubjectTerms Chemistry
Chemistry, Organic
Physical Sciences
Science & Technology
Title Phosphine-Free Perfluoro-Tagged Palladium Nanoparticles Supported on Fluorous Silica Gel:  Application to the Heck Reaction
URI http://dx.doi.org/10.1021/ol7024845
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