Ordered Mesoporous Cobalt Oxide as Highly Efficient Oxygen Evolution Catalyst
Oxygen evolution from water by use of earth-abundant element-based catalysts is crucial for mass solar fuel production. In this report, a mesoporous cobalt oxide with an ultrahigh surface area (up to 250 m2·g–1) has been fabricated through Mg substitution in the mesoporous Co3O4 spinel, followed by...
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| Published in | Journal of the American Chemical Society Vol. 135; no. 11; pp. 4516 - 4521 |
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| Main Authors | , , |
| Format | Journal Article |
| Language | English |
| Published |
United States
American Chemical Society
20.03.2013
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| Subjects | |
| Online Access | Get full text |
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| Abstract | Oxygen evolution from water by use of earth-abundant element-based catalysts is crucial for mass solar fuel production. In this report, a mesoporous cobalt oxide with an ultrahigh surface area (up to 250 m2·g–1) has been fabricated through Mg substitution in the mesoporous Co3O4 spinel, followed by a Mg-selective leaching process. Approximately a third of Mg cations were removed in the leaching process, resulting in a highly porous cobalt oxide with a significant amount of defects in the spinel structure. The activated mesoporous cobalt oxide exhibited high oxygen evolution activities in both the visible-light-driven [Ru(bpy)3]2+–persulfate system and the Ce4+/Ce3+ chemical water oxidation system. Under a strong acidic environment, a high turnover frequency (TOF) of ∼2.2 × 10–3 s–1 per Co atom was achieved, which is more than twice the TOF of traditional hard-templated, mesoporous Co3O4. |
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| AbstractList | Oxygen evolution from water by use of earth-abundant element-based catalysts is crucial for mass solar fuel production. In this report, a mesoporous cobalt oxide with an ultrahigh surface area (up to 250 m(2)·g(-1)) has been fabricated through Mg substitution in the mesoporous Co3O4 spinel, followed by a Mg-selective leaching process. Approximately a third of Mg cations were removed in the leaching process, resulting in a highly porous cobalt oxide with a significant amount of defects in the spinel structure. The activated mesoporous cobalt oxide exhibited high oxygen evolution activities in both the visible-light-driven [Ru(bpy)3](2+)-persulfate system and the Ce(4+)/Ce(3+) chemical water oxidation system. Under a strong acidic environment, a high turnover frequency (TOF) of ~2.2 × 10(-3) s(-1) per Co atom was achieved, which is more than twice the TOF of traditional hard-templated, mesoporous Co3O4. Oxygen evolution from water by use of earth-abundant element-based catalysts is crucial for mass solar fuel production. In this report, a mesoporous cobalt oxide with an ultrahigh surface area (up to 250 m²·g–¹) has been fabricated through Mg substitution in the mesoporous Co₃O₄ spinel, followed by a Mg-selective leaching process. Approximately a third of Mg cations were removed in the leaching process, resulting in a highly porous cobalt oxide with a significant amount of defects in the spinel structure. The activated mesoporous cobalt oxide exhibited high oxygen evolution activities in both the visible-light-driven [Ru(bpy)₃]²⁺–persulfate system and the Ce⁴⁺/Ce³⁺ chemical water oxidation system. Under a strong acidic environment, a high turnover frequency (TOF) of ∼2.2 × 10–³ s–¹ per Co atom was achieved, which is more than twice the TOF of traditional hard-templated, mesoporous Co₃O₄. Oxygen evolution from water by use of earth-abundant element-based catalysts is crucial for mass solar fuel production. In this report, a mesoporous cobalt oxide with an ultrahigh surface area (up to 250 m2·g–1) has been fabricated through Mg substitution in the mesoporous Co3O4 spinel, followed by a Mg-selective leaching process. Approximately a third of Mg cations were removed in the leaching process, resulting in a highly porous cobalt oxide with a significant amount of defects in the spinel structure. The activated mesoporous cobalt oxide exhibited high oxygen evolution activities in both the visible-light-driven [Ru(bpy)3]2+–persulfate system and the Ce4+/Ce3+ chemical water oxidation system. Under a strong acidic environment, a high turnover frequency (TOF) of ∼2.2 × 10–3 s–1 per Co atom was achieved, which is more than twice the TOF of traditional hard-templated, mesoporous Co3O4. Oxygen evolution from water by use of earth-abundant element-based catalysts is crucial for mass solar fuel production. In this report, a mesoporous cobalt oxide with an ultrahigh surface area (up to 250 m(2)·g(-1)) has been fabricated through Mg substitution in the mesoporous Co3O4 spinel, followed by a Mg-selective leaching process. Approximately a third of Mg cations were removed in the leaching process, resulting in a highly porous cobalt oxide with a significant amount of defects in the spinel structure. The activated mesoporous cobalt oxide exhibited high oxygen evolution activities in both the visible-light-driven [Ru(bpy)3](2+)-persulfate system and the Ce(4+)/Ce(3+) chemical water oxidation system. Under a strong acidic environment, a high turnover frequency (TOF) of ~2.2 × 10(-3) s(-1) per Co atom was achieved, which is more than twice the TOF of traditional hard-templated, mesoporous Co3O4.Oxygen evolution from water by use of earth-abundant element-based catalysts is crucial for mass solar fuel production. In this report, a mesoporous cobalt oxide with an ultrahigh surface area (up to 250 m(2)·g(-1)) has been fabricated through Mg substitution in the mesoporous Co3O4 spinel, followed by a Mg-selective leaching process. Approximately a third of Mg cations were removed in the leaching process, resulting in a highly porous cobalt oxide with a significant amount of defects in the spinel structure. The activated mesoporous cobalt oxide exhibited high oxygen evolution activities in both the visible-light-driven [Ru(bpy)3](2+)-persulfate system and the Ce(4+)/Ce(3+) chemical water oxidation system. Under a strong acidic environment, a high turnover frequency (TOF) of ~2.2 × 10(-3) s(-1) per Co atom was achieved, which is more than twice the TOF of traditional hard-templated, mesoporous Co3O4. |
| Author | Jiao, Feng Hutchings, Gregory S Rosen, Jonathan |
| AuthorAffiliation | University of Delaware |
| AuthorAffiliation_xml | – name: University of Delaware |
| Author_xml | – sequence: 1 givenname: Jonathan surname: Rosen fullname: Rosen, Jonathan – sequence: 2 givenname: Gregory S surname: Hutchings fullname: Hutchings, Gregory S – sequence: 3 givenname: Feng surname: Jiao fullname: Jiao, Feng email: jiao@udel.edu |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/23448405$$D View this record in MEDLINE/PubMed https://www.osti.gov/biblio/1082063$$D View this record in Osti.gov |
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| Title | Ordered Mesoporous Cobalt Oxide as Highly Efficient Oxygen Evolution Catalyst |
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