Introduction of π‑Complexation into Porous Aromatic Framework for Highly Selective Adsorption of Ethylene over Ethane
In this work, we demonstrate for the first time the introduction of π-complexation into a porous aromatic framework (PAF), affording significant increase in ethylene uptake capacity, as illustrated in the context of Ag(I) ion functionalized PAF-1, PAF-1-SO3Ag. IAST calculations using single-compone...
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| Published in | Journal of the American Chemical Society Vol. 136; no. 24; pp. 8654 - 8660 |
|---|---|
| Main Authors | , , , , , , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
United States
American Chemical Society
18.06.2014
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| Subjects | |
| Online Access | Get full text |
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| Abstract | In this work, we demonstrate for the first time the introduction of π-complexation into a porous aromatic framework (PAF), affording significant increase in ethylene uptake capacity, as illustrated in the context of Ag(I) ion functionalized PAF-1, PAF-1-SO3Ag. IAST calculations using single-component-isotherm data and an equimolar ethylene/ethane ratio at 296 K reveal that PAF-1-SO3Ag shows exceptionally high ethylene/ethane adsorption selectivity (S ads: 27 to 125), far surpassing benchmark zeolite and any other MOF reported in literature. The formation of π-complexation between ethylene molecules and Ag(I) ions in PAF-1-SO3Ag has been evidenced by the high isosteric heats of adsorption of C2H4 and also proved by in situ IR spectroscopy studies. Transient breakthrough experiments, supported by simulations, indicate the feasibility of PAF-1-SO3Ag for producing 99.95%+ pure C2H4 in a Pressure Swing Adsorption operation. Our work herein thus suggests a new perspective to functionalizing PAFs and other types of advanced porous materials for highly selective adsorption of ethylene over ethane. |
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| AbstractList | In this work, we demonstrate for the first time the introduction of π-complexation into a porous aromatic framework (PAF), affording significant increase in ethylene uptake capacity, as illustrated in the context of Ag(I) ion functionalized PAF-1, PAF-1-SO3Ag. IAST calculations using single-component-isotherm data and an equimolar ethylene/ethane ratio at 296 K reveal that PAF-1-SO3Ag shows exceptionally high ethylene/ethane adsorption selectivity (Sads: 27 to 125), far surpassing benchmark zeolite and any other MOF reported in literature. The formation of π-complexation between ethylene molecules and Ag(I) ions in PAF-1-SO3Ag has been evidenced by the high isosteric heats of adsorption of C2H4 and also proved by in situ IR spectroscopy studies. Transient breakthrough experiments, supported by simulations, indicate the feasibility of PAF-1-SO3Ag for producing 99.95%+ pure C2H4 in a Pressure Swing Adsorption operation. Our work herein thus suggests a new perspective to functionalizing PAFs and other types of advanced porous materials for highly selective adsorption of ethylene over ethane. In this work, we demonstrate for the first time the introduction of π-complexation into a porous aromatic framework (PAF), affording significant increase in ethylene uptake capacity, as illustrated in the context of Ag(I) ion functionalized PAF-1, PAF-1-SO3Ag. IAST calculations using single-component-isotherm data and an equimolar ethylene/ethane ratio at 296 K reveal that PAF-1-SO3Ag shows exceptionally high ethylene/ethane adsorption selectivity (Sads: 27 to 125), far surpassing benchmark zeolite and any other MOF reported in literature. The formation of π-complexation between ethylene molecules and Ag(I) ions in PAF-1-SO3Ag has been evidenced by the high isosteric heats of adsorption of C2H4 and also proved by in situ IR spectroscopy studies. Transient breakthrough experiments, supported by simulations, indicate the feasibility of PAF-1-SO3Ag for producing 99.95%+ pure C2H4 in a Pressure Swing Adsorption operation. Our work herein thus suggests a new perspective to functionalizing PAFs and other types of advanced porous materials for highly selective adsorption of ethylene over ethane.In this work, we demonstrate for the first time the introduction of π-complexation into a porous aromatic framework (PAF), affording significant increase in ethylene uptake capacity, as illustrated in the context of Ag(I) ion functionalized PAF-1, PAF-1-SO3Ag. IAST calculations using single-component-isotherm data and an equimolar ethylene/ethane ratio at 296 K reveal that PAF-1-SO3Ag shows exceptionally high ethylene/ethane adsorption selectivity (Sads: 27 to 125), far surpassing benchmark zeolite and any other MOF reported in literature. The formation of π-complexation between ethylene molecules and Ag(I) ions in PAF-1-SO3Ag has been evidenced by the high isosteric heats of adsorption of C2H4 and also proved by in situ IR spectroscopy studies. Transient breakthrough experiments, supported by simulations, indicate the feasibility of PAF-1-SO3Ag for producing 99.95%+ pure C2H4 in a Pressure Swing Adsorption operation. Our work herein thus suggests a new perspective to functionalizing PAFs and other types of advanced porous materials for highly selective adsorption of ethylene over ethane. In this work, we demonstrate for the first time the introduction of π-complexation into a porous aromatic framework (PAF), affording significant increase in ethylene uptake capacity, as illustrated in the context of Ag(I) ion functionalized PAF-1, PAF-1-SO3Ag. IAST calculations using single-component-isotherm data and an equimolar ethylene/ethane ratio at 296 K reveal that PAF-1-SO3Ag shows exceptionally high ethylene/ethane adsorption selectivity (S ads: 27 to 125), far surpassing benchmark zeolite and any other MOF reported in literature. The formation of π-complexation between ethylene molecules and Ag(I) ions in PAF-1-SO3Ag has been evidenced by the high isosteric heats of adsorption of C2H4 and also proved by in situ IR spectroscopy studies. Transient breakthrough experiments, supported by simulations, indicate the feasibility of PAF-1-SO3Ag for producing 99.95%+ pure C2H4 in a Pressure Swing Adsorption operation. Our work herein thus suggests a new perspective to functionalizing PAFs and other types of advanced porous materials for highly selective adsorption of ethylene over ethane. In this work, we demonstrate for the first time the introduction of π-complexation into a porous aromatic framework (PAF), affording significant increase in ethylene uptake capacity, as illustrated in the context of Ag(I) ion functionalized PAF-1, PAF-1-SO₃Ag. IAST calculations using single-component-isotherm data and an equimolar ethylene/ethane ratio at 296 K reveal that PAF-1-SO₃Ag shows exceptionally high ethylene/ethane adsorption selectivity (Sₐdₛ: 27 to 125), far surpassing benchmark zeolite and any other MOF reported in literature. The formation of π-complexation between ethylene molecules and Ag(I) ions in PAF-1-SO₃Ag has been evidenced by the high isosteric heats of adsorption of C₂H₄ and also proved by in situ IR spectroscopy studies. Transient breakthrough experiments, supported by simulations, indicate the feasibility of PAF-1-SO₃Ag for producing 99.95%+ pure C₂H₄ in a Pressure Swing Adsorption operation. Our work herein thus suggests a new perspective to functionalizing PAFs and other types of advanced porous materials for highly selective adsorption of ethylene over ethane. |
| Author | Space, Brian Chrzanowski, Matthew Pham, Tony Zhang, Yiming Ma, Dingxuan Han, Yu Ma, Shengqian Li, Baiyan Krishna, Rajamani Shi, Zhan Liu, Jian Thallapally, Praveen K Wu, Zili Liu, Jun Yao, Kexin |
| AuthorAffiliation | Department of Chemistry University of Amsterdam Jilin University Center for Nanophase Material Sciences and Chemical Sciences Division, Oak Ridge National Laboratory State Key Laboratory of Inorganic Synthesis and Preparative Chemistry, College of Chemistry Van’t Hoff Institute for Molecular Sciences University of South Florida King Abdullah University of Science and Technology Advanced Membranes and Porous Materials Center, Physical Sciences and Engineering Division Pacific Northwest National Laboratory |
| AuthorAffiliation_xml | – name: University of Amsterdam – name: Advanced Membranes and Porous Materials Center, Physical Sciences and Engineering Division – name: Department of Chemistry – name: Van’t Hoff Institute for Molecular Sciences – name: Jilin University – name: Pacific Northwest National Laboratory – name: King Abdullah University of Science and Technology – name: Center for Nanophase Material Sciences and Chemical Sciences Division, Oak Ridge National Laboratory – name: University of South Florida – name: State Key Laboratory of Inorganic Synthesis and Preparative Chemistry, College of Chemistry |
| Author_xml | – sequence: 1 givenname: Baiyan surname: Li fullname: Li, Baiyan organization: University of South Florida – sequence: 2 givenname: Yiming surname: Zhang fullname: Zhang, Yiming organization: University of South Florida – sequence: 3 givenname: Rajamani surname: Krishna fullname: Krishna, Rajamani organization: University of Amsterdam – sequence: 4 givenname: Kexin surname: Yao fullname: Yao, Kexin organization: King Abdullah University of Science and Technology – sequence: 5 givenname: Yu surname: Han fullname: Han, Yu organization: King Abdullah University of Science and Technology – sequence: 6 givenname: Zili surname: Wu fullname: Wu, Zili organization: Center for Nanophase Material Sciences and Chemical Sciences Division, Oak Ridge National Laboratory – sequence: 7 givenname: Dingxuan surname: Ma fullname: Ma, Dingxuan organization: Jilin University – sequence: 8 givenname: Zhan surname: Shi fullname: Shi, Zhan organization: Jilin University – sequence: 9 givenname: Tony surname: Pham fullname: Pham, Tony organization: University of South Florida – sequence: 10 givenname: Brian surname: Space fullname: Space, Brian organization: University of South Florida – sequence: 11 givenname: Jian surname: Liu fullname: Liu, Jian organization: Pacific Northwest National Laboratory – sequence: 12 givenname: Praveen K surname: Thallapally fullname: Thallapally, Praveen K organization: Pacific Northwest National Laboratory – sequence: 13 givenname: Jun surname: Liu fullname: Liu, Jun organization: Pacific Northwest National Laboratory – sequence: 14 givenname: Matthew surname: Chrzanowski fullname: Chrzanowski, Matthew organization: University of South Florida – sequence: 15 givenname: Shengqian surname: Ma fullname: Ma, Shengqian email: sqma@usf.edu organization: University of South Florida |
| BackLink | https://www.ncbi.nlm.nih.gov/pubmed/24901372$$D View this record in MEDLINE/PubMed |
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| Snippet | In this work, we demonstrate for the first time the introduction of π-complexation into a porous aromatic framework (PAF), affording significant increase in... |
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| SubjectTerms | adsorption ethane ethylene infrared spectroscopy ions silver zeolites |
| Title | Introduction of π‑Complexation into Porous Aromatic Framework for Highly Selective Adsorption of Ethylene over Ethane |
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