Twelve-Component Free-Standing Nanoporous High-Entropy Alloys for Multifunctional Electrocatalysis

Nanostructured high-entropy alloys (HEAs) with tunable compositions have attracted intensive scientific attention on their unique structural, catalytic, and energy-storage capabilities. In this work, we introduce a straightforward two-step fabrication procedure to synthesize free-standing single pha...

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Published inACS materials letters Vol. 4; no. 1; pp. 181 - 189
Main Authors Yu, Tingting, Zhang, Yanyi, Hu, Yixuan, Hu, Kailong, Lin, Xi, Xie, Guoqiang, Liu, Xingjun, Reddy, Kolan Madhav, Ito, Yoshikazu, Qiu, Hua-Jun
Format Journal Article
LanguageEnglish
Published American Chemical Society 03.01.2022
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Abstract Nanostructured high-entropy alloys (HEAs) with tunable compositions have attracted intensive scientific attention on their unique structural, catalytic, and energy-storage capabilities. In this work, we introduce a straightforward two-step fabrication procedure to synthesize free-standing single phase multicomponent nanoporous HEAs consisting of 12 or 16 different elements including both noble and non-noble metals. The electrocatalytic results reveal that the synergistic elemental combinations of such HEAs with a fine porous structure give rise to enhanced hydrogen evolution reaction (HER) and oxygen reduction reaction (ORR) catalytic activities superior to the commercial Pt/C and, at the same time, enhanced oxygen evolution reaction (OER) catalytic activity over the commercial IrO2 catalyst. The demonstrated multifunctional catalytic performance of these free-standing nanoporous HEAs would facilitate large current densities in the water splitting reactions, rechargeable Zn-air batteries, and many other catalytic, sensing, and energy applications.
AbstractList Nanostructured high-entropy alloys (HEAs) with tunable compositions have attracted intensive scientific attention on their unique structural, catalytic, and energy-storage capabilities. In this work, we introduce a straightforward two-step fabrication procedure to synthesize free-standing single phase multicomponent nanoporous HEAs consisting of 12 or 16 different elements including both noble and non-noble metals. The electrocatalytic results reveal that the synergistic elemental combinations of such HEAs with a fine porous structure give rise to enhanced hydrogen evolution reaction (HER) and oxygen reduction reaction (ORR) catalytic activities superior to the commercial Pt/C and, at the same time, enhanced oxygen evolution reaction (OER) catalytic activity over the commercial IrO2 catalyst. The demonstrated multifunctional catalytic performance of these free-standing nanoporous HEAs would facilitate large current densities in the water splitting reactions, rechargeable Zn-air batteries, and many other catalytic, sensing, and energy applications.
Author Yu, Tingting
Hu, Kailong
Hu, Yixuan
Zhang, Yanyi
Xie, Guoqiang
Qiu, Hua-Jun
Ito, Yoshikazu
Reddy, Kolan Madhav
Liu, Xingjun
Lin, Xi
AuthorAffiliation School of Materials Science and Engineering
Frontier Research Center for Materials Structure, School of Materials Science and Engineering
Institute of Applied Physics, Graduate School of Pure and Applied Sciences
Shenzhen R&D Center for Al-Based Hydrogen Hydrolysis Materials
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  organization: Shenzhen R&D Center for Al-Based Hydrogen Hydrolysis Materials
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Title Twelve-Component Free-Standing Nanoporous High-Entropy Alloys for Multifunctional Electrocatalysis
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