Mechanochemical Synthesis of High Entropy Oxide Materials under Ambient Conditions: Dispersion of Catalysts via Entropy Maximization
The solid-solution metal oxide (NiMgCuZnCo)O is the first known high-entropy (HE) metal oxide synthesized, forming a poster child of the emerging high-entropy oxide materials, which is derived from high-temperature synthesis methodologies (>900 °C). In this work, we report the mechanochemical syn...
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| Published in | ACS materials letters Vol. 1; no. 1; pp. 83 - 88 |
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| Main Authors | , , , , , , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
American Chemical Society
01.07.2019
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| Online Access | Get full text |
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| Abstract | The solid-solution metal oxide (NiMgCuZnCo)O is the first known high-entropy (HE) metal oxide synthesized, forming a poster child of the emerging high-entropy oxide materials, which is derived from high-temperature synthesis methodologies (>900 °C). In this work, we report the mechanochemical synthesis of this known HE metal oxide (NiMgCuZnCo)O under ambient conditions. The advantage of this approach was further demonstrated by the introduction of up to 5 wt % noble metal into (NiMgCuZnCo)O, as single atoms or nanoclusters, which showed good stability at high temperature and produced a high catalytic activity in the hydrogenation of atmospheric CO2 to CO. The latter work demonstrated the unique advantage of using HE materials to disperse catalysis centers. |
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| AbstractList | The solid-solution metal oxide (NiMgCuZnCo)O is the first known high-entropy (HE) metal oxide synthesized, forming a poster child of the emerging high-entropy oxide materials, which is derived from high-temperature synthesis methodologies (>900 °C). In this work, we report the mechanochemical synthesis of this known HE metal oxide (NiMgCuZnCo)O under ambient conditions. The advantage of this approach was further demonstrated by the introduction of up to 5 wt % noble metal into (NiMgCuZnCo)O, as single atoms or nanoclusters, which showed good stability at high temperature and produced a high catalytic activity in the hydrogenation of atmospheric CO2 to CO. The latter work demonstrated the unique advantage of using HE materials to disperse catalysis centers. |
| Author | Zhang, Zihao Mullins, David R Hu, Xiaobing Bridges, Craig A Unocic, Raymond R Yang, Shi-Ze Sang, Xiahan Dai, Sheng Fu, Jie Lin, Wenwen Zhang, Pengfei Chen, Hao Jafta, Charl J Jie, Kecheng |
| AuthorAffiliation | Department of Chemistry Key Laboratory of Biomass Chemical Engineering of Ministry of Education, College of Chemical and Biological Engineering Chemical Sciences Division Center for Nanophase Materials Sciences Department of Materials Science and Engineering Oak Ridge National Laboratory School of Chemistry and Chemical Engineering The University of Tennessee Shanghai Jiao Tong University |
| AuthorAffiliation_xml | – name: Chemical Sciences Division – name: Shanghai Jiao Tong University – name: Key Laboratory of Biomass Chemical Engineering of Ministry of Education, College of Chemical and Biological Engineering – name: Department of Chemistry – name: School of Chemistry and Chemical Engineering – name: Center for Nanophase Materials Sciences – name: The University of Tennessee – name: Oak Ridge National Laboratory – name: Department of Materials Science and Engineering |
| Author_xml | – sequence: 1 givenname: Hao orcidid: 0000-0002-6658-4198 surname: Chen fullname: Chen, Hao organization: The University of Tennessee – sequence: 2 givenname: Wenwen surname: Lin fullname: Lin, Wenwen organization: Key Laboratory of Biomass Chemical Engineering of Ministry of Education, College of Chemical and Biological Engineering – sequence: 3 givenname: Zihao surname: Zhang fullname: Zhang, Zihao organization: Key Laboratory of Biomass Chemical Engineering of Ministry of Education, College of Chemical and Biological Engineering – sequence: 4 givenname: Kecheng orcidid: 0000-0001-8146-4875 surname: Jie fullname: Jie, Kecheng organization: The University of Tennessee – sequence: 5 givenname: David R orcidid: 0000-0003-3495-7188 surname: Mullins fullname: Mullins, David R organization: Oak Ridge National Laboratory – sequence: 6 givenname: Xiahan orcidid: 0000-0002-2861-6814 surname: Sang fullname: Sang, Xiahan organization: Center for Nanophase Materials Sciences – sequence: 7 givenname: Shi-Ze orcidid: 0000-0002-0421-006X surname: Yang fullname: Yang, Shi-Ze organization: Center for Nanophase Materials Sciences – sequence: 8 givenname: Charl J orcidid: 0000-0002-9773-6799 surname: Jafta fullname: Jafta, Charl J organization: Oak Ridge National Laboratory – sequence: 9 givenname: Craig A orcidid: 0000-0002-3543-463X surname: Bridges fullname: Bridges, Craig A organization: Oak Ridge National Laboratory – sequence: 10 givenname: Xiaobing orcidid: 0000-0002-9233-8118 surname: Hu fullname: Hu, Xiaobing organization: Department of Materials Science and Engineering – sequence: 11 givenname: Raymond R orcidid: 0000-0002-1777-8228 surname: Unocic fullname: Unocic, Raymond R organization: Center for Nanophase Materials Sciences – sequence: 12 givenname: Jie orcidid: 0000-0002-3652-7715 surname: Fu fullname: Fu, Jie email: jiefu@zju.edu.cn organization: Key Laboratory of Biomass Chemical Engineering of Ministry of Education, College of Chemical and Biological Engineering – sequence: 13 givenname: Pengfei orcidid: 0000-0001-7559-7348 surname: Zhang fullname: Zhang, Pengfei email: chemistryzpf@sjtu.edu.cn organization: Shanghai Jiao Tong University – sequence: 14 givenname: Sheng orcidid: 0000-0002-8046-3931 surname: Dai fullname: Dai, Sheng email: dais@ornl.gov organization: The University of Tennessee |
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