Noble Metal-Free Nanoporous High-Entropy Alloys as Highly Efficient Electrocatalysts for Oxygen Evolution Reaction
Developing highly efficient catalysts for oxygen evolution reactions (OER) is a key step for rechargeable metal–oxygen batteries and water splitting. Usually, binary NiFe or ternary NiCoFe nano-alloys are used as the OER catalysts. Herein, combining the precursor alloy design with chemical etching,...
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| Published in | ACS materials letters Vol. 1; no. 5; pp. 526 - 533 |
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| Main Authors | , , , , , , , , |
| Format | Journal Article |
| Language | English |
| Published |
American Chemical Society
04.11.2019
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| Online Access | Get full text |
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| Abstract | Developing highly efficient catalysts for oxygen evolution reactions (OER) is a key step for rechargeable metal–oxygen batteries and water splitting. Usually, binary NiFe or ternary NiCoFe nano-alloys are used as the OER catalysts. Herein, combining the precursor alloy design with chemical etching, a simple dealloying route is developed to controllably incorporate five or more nonprecious metals into one nanostructured alloy with a naturally oxidized surface, that is, nanoporous high entropy alloys (np-HEAs) covered with high-entropy (oxy)hydroxides (HEOs). It is found that the alloy composition plays a dominant role in the OER activity enhancement with the np-AlNiCoFeX (X = Mo, Nb, Cr) combination showing the highest activity. Forming quinary HEAs also greatly enhances the electrochemical cycling stabilities compared with the ternary and quaternary counterparts. The result indicates the significance of synergistically incorporating five or more metal elements in one single-phase nanostructure, which provides more structural and chemical degrees of freedom to boost the catalytic performance, overcoming the restriction of normal binary or ternary alloys. Multinary transition metal-based np-HEA is a new class of promising catalyst for various important reactions. |
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| AbstractList | Developing highly efficient catalysts for oxygen evolution reactions (OER) is a key step for rechargeable metal–oxygen batteries and water splitting. Usually, binary NiFe or ternary NiCoFe nano-alloys are used as the OER catalysts. Herein, combining the precursor alloy design with chemical etching, a simple dealloying route is developed to controllably incorporate five or more nonprecious metals into one nanostructured alloy with a naturally oxidized surface, that is, nanoporous high entropy alloys (np-HEAs) covered with high-entropy (oxy)hydroxides (HEOs). It is found that the alloy composition plays a dominant role in the OER activity enhancement with the np-AlNiCoFeX (X = Mo, Nb, Cr) combination showing the highest activity. Forming quinary HEAs also greatly enhances the electrochemical cycling stabilities compared with the ternary and quaternary counterparts. The result indicates the significance of synergistically incorporating five or more metal elements in one single-phase nanostructure, which provides more structural and chemical degrees of freedom to boost the catalytic performance, overcoming the restriction of normal binary or ternary alloys. Multinary transition metal-based np-HEA is a new class of promising catalyst for various important reactions. |
| Author | Li, Huanglong Sun, Shuhui Lv, Juan Gao, Jiaojiao Xie, Guoqiang Qiu, Hua-Jun Fang, Gang Wen, Yuren Liu, Xingjun |
| AuthorAffiliation | Harbin Institute of Technology School of Materials Science and Engineering University of Science and Technology Beijing Department of Precision Instrument State Key Laboratory of Advanced Welding and Joining |
| AuthorAffiliation_xml | – name: University of Science and Technology Beijing – name: State Key Laboratory of Advanced Welding and Joining – name: Department of Precision Instrument – name: Harbin Institute of Technology – name: School of Materials Science and Engineering |
| Author_xml | – sequence: 1 givenname: Hua-Jun orcidid: 0000-0003-0396-1942 surname: Qiu fullname: Qiu, Hua-Jun email: qiuhuajun@hit.edu.cn organization: School of Materials Science and Engineering – sequence: 2 givenname: Gang surname: Fang fullname: Fang, Gang organization: School of Materials Science and Engineering – sequence: 3 givenname: Jiaojiao surname: Gao fullname: Gao, Jiaojiao organization: School of Materials Science and Engineering – sequence: 4 givenname: Yuren surname: Wen fullname: Wen, Yuren organization: University of Science and Technology Beijing – sequence: 5 givenname: Juan surname: Lv fullname: Lv, Juan organization: Department of Precision Instrument – sequence: 6 givenname: Huanglong orcidid: 0000-0002-1777-7807 surname: Li fullname: Li, Huanglong email: li_huanglong@mail.tsinghua.edu.cn organization: Department of Precision Instrument – sequence: 7 givenname: Guoqiang surname: Xie fullname: Xie, Guoqiang organization: School of Materials Science and Engineering – sequence: 8 givenname: Xingjun surname: Liu fullname: Liu, Xingjun email: lxj@xmu.edu.cn organization: Harbin Institute of Technology – sequence: 9 givenname: Shuhui orcidid: 0000-0002-0508-2944 surname: Sun fullname: Sun, Shuhui |
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| Snippet | Developing highly efficient catalysts for oxygen evolution reactions (OER) is a key step for rechargeable metal–oxygen batteries and water splitting. Usually,... |
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| Title | Noble Metal-Free Nanoporous High-Entropy Alloys as Highly Efficient Electrocatalysts for Oxygen Evolution Reaction |
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