Ordered Mesoporous Silica Pyrolyzed from Single-Source Self-Assembled Organic–Inorganic Giant Surfactants

We report the preparation of hexagonal mesoporous silica from single-source giant surfactants constructed via dihydroxyl-functionlized polyhedral oligomeric silsesquioxane (DPOSS) heads and a polystyrene (PS) tail. After thermal annealing, the obtained well-ordered hexagonal hybrid was pyrolyzed to...

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Published inJournal of the American Chemical Society Vol. 143; no. 33; pp. 12935 - 12942
Main Authors Guo, Qing-Yun, Yan, Xiao-Yun, Zhang, Wei, Li, Xing-Han, Xu, Yongsheng, Dai, Shuqi, Liu, Yuchu, Zhang, Bo-xing, Feng, Xueyan, Yin, Jiafu, Han, Di, Huang, Jiahao, Su, Zebin, Liu, Tong, Huang, Mingjun, Hsu, Chih-Hao, Cheng, Stephen Z. D
Format Journal Article
LanguageEnglish
Published American Chemical Society 25.08.2021
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Abstract We report the preparation of hexagonal mesoporous silica from single-source giant surfactants constructed via dihydroxyl-functionlized polyhedral oligomeric silsesquioxane (DPOSS) heads and a polystyrene (PS) tail. After thermal annealing, the obtained well-ordered hexagonal hybrid was pyrolyzed to afford well-ordered mesoporous silica. A high porosity (e.g., 581 m2/g) and a uniform and narrow pore size distribution (e.g., 3.3 nm) were achieved. Mesoporous silica in diverse shapes and morphologies were achieved by processing the precursor. When the PS tail length was increased, the pore size expanded accordingly. Moreover, such pyrolyzed, ordered mesoporous silica can help to increase both efficiency and stability of nanocatalysts.
AbstractList We report the preparation of hexagonal mesoporous silica from single-source giant surfactants constructed via dihydroxyl-functionlized polyhedral oligomeric silsesquioxane (DPOSS) heads and a polystyrene (PS) tail. After thermal annealing, the obtained well-ordered hexagonal hybrid was pyrolyzed to afford well-ordered mesoporous silica. A high porosity (e.g., 581 m2/g) and a uniform and narrow pore size distribution (e.g., 3.3 nm) were achieved. Mesoporous silica in diverse shapes and morphologies were achieved by processing the precursor. When the PS tail length was increased, the pore size expanded accordingly. Moreover, such pyrolyzed, ordered mesoporous silica can help to increase both efficiency and stability of nanocatalysts.
Author Li, Xing-Han
Feng, Xueyan
Yan, Xiao-Yun
Dai, Shuqi
Liu, Tong
Zhang, Wei
Han, Di
Hsu, Chih-Hao
Guo, Qing-Yun
Cheng, Stephen Z. D
Su, Zebin
Xu, Yongsheng
Yin, Jiafu
Huang, Jiahao
Liu, Yuchu
Huang, Mingjun
Zhang, Bo-xing
AuthorAffiliation Department of Polymer Science, School of Polymer Science and Polymer Engineering
South China Advanced Institute for Soft Matter Science and Technology, School of Molecular Science and Engineering
School of Chemical Engineering and Technology
College of Polymer Science and Engineering, State Key Laboratory of Polymer Materials Engineering
Guangdong Provincial Key Laboratory of Functional and Intelligent Hybrid Materials and Devices
AuthorAffiliation_xml – name: College of Polymer Science and Engineering, State Key Laboratory of Polymer Materials Engineering
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  email: scheng@uakron.edu
  organization: Department of Polymer Science, School of Polymer Science and Polymer Engineering
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Snippet We report the preparation of hexagonal mesoporous silica from single-source giant surfactants constructed via dihydroxyl-functionlized polyhedral oligomeric...
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Title Ordered Mesoporous Silica Pyrolyzed from Single-Source Self-Assembled Organic–Inorganic Giant Surfactants
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