High-Temperature Reaction of Kaolin with Sulfuric Acid
A new procedure is described in which kaolin and a small amount of concentrated sulfuric acid are heated in a furnace at temperatures between 150 and 1000 °C. Parameters studied were reaction temperature and time, proton to alumina molar ratio, calcination temperature and time, and amount of water i...
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Published in | Industrial & engineering chemistry research Vol. 41; no. 17; pp. 4168 - 4173 |
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Main Authors | , , |
Format | Journal Article |
Language | English |
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Washington, DC
American Chemical Society
21.08.2002
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Abstract | A new procedure is described in which kaolin and a small amount of concentrated sulfuric acid are heated in a furnace at temperatures between 150 and 1000 °C. Parameters studied were reaction temperature and time, proton to alumina molar ratio, calcination temperature and time, and amount of water in the reaction medium. Al yield grew sharply until reaching a maximum at a reaction temperature of 700 °C and decreasing sharply beyond this temperature. Ti reaction yield values were lower than the Al reaction yield, showing a maximum at 200 °C and decreasing steadily as the reaction temperature was increased. Fe reaction yield showed a maximum in the same range of reaction temperature as Al. Previous calcination of kaolin produced only slight increases in reaction yields. Brunauer−Emmett−Teller (BET) surface area tests indicated an increase of the BET surface area for short reaction times, reaching values above 100 m2/g. Products of the reaction were mostly Al2(SO4)3. |
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AbstractList | A new procedure is described in which kaolin and a small amount of concentrated sulfuric acid are heated in a furnace at temperatures between 150 and 1000 °C. Parameters studied were reaction temperature and time, proton to alumina molar ratio, calcination temperature and time, and amount of water in the reaction medium. Al yield grew sharply until reaching a maximum at a reaction temperature of 700 °C and decreasing sharply beyond this temperature. Ti reaction yield values were lower than the Al reaction yield, showing a maximum at 200 °C and decreasing steadily as the reaction temperature was increased. Fe reaction yield showed a maximum in the same range of reaction temperature as Al. Previous calcination of kaolin produced only slight increases in reaction yields. Brunauer−Emmett−Teller (BET) surface area tests indicated an increase of the BET surface area for short reaction times, reaching values above 100 m2/g. Products of the reaction were mostly Al2(SO4)3. |
Author | Esplugas, Santiago Colina, Fernando G Costa, Jose |
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Cites_doi | 10.1346/CCMN.1970.0180202 10.1002/jctb.280560213 10.1180/claymin.1982.017.3.01 10.1346/CCMN.1969.0170203 10.1038/215844b0 10.1021/ja01269a023 10.1346/CCMN.1962.0110122 10.1179/096797801681468 10.1346/000986002760833774 10.1007/BF02657384 10.1180/claymin.1970.008.3.11 10.1107/S0021889874010375 10.1007/BF01908502 10.1016/0040-6031(91)80085-W 10.1016/0304-386X(92)90008-N |
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Keywords | Conversion rate Reaction product Specific surface area High temperature Experimental study Sulfuric acid Characterization Inorganic acids Aluminium Sulfates Chemical reaction Reaction mechanism Kinetics Kaolin |
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SubjectTerms | Chemistry Exact sciences and technology Inorganic chemistry and origins of life Kinetics and mechanism of reactions |
Title | High-Temperature Reaction of Kaolin with Sulfuric Acid |
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