Miniemulsion polymerization technology

Explains miniemulsion technology and techniques and why they have many distinct advantages over the conventional emulsion polymerization technology Miniemulsion Polymerization Technology comprises 10 papers by many of the world's experts on the subject. It summarizes the recent advances in mini...

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Main Author Mittal, Vikas
Format eBook Book
LanguageEnglish
Published Salem, MA Scrivener 2010
Hoboken, N.J John Wiley & Sons
John Wiley & Sons, Incorporated
Wiley-Blackwell
Edition1
SeriesWiley-Scrivener
Subjects
Emulsion polymerization
Microencapsulation
Nanoparticles
Online AccessGet full text
ISBN9780470625965
0470625961
9780470922354
0470922354
DOI10.1002/9780470922354

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Abstract Explains miniemulsion technology and techniques and why they have many distinct advantages over the conventional emulsion polymerization technology Miniemulsion Polymerization Technology comprises 10 papers by many of the world's experts on the subject. It summarizes the recent advances in miniemulsion polymerization technology including the advances on the selection of surfactants and co-surfactants, the expansion of miniemulsion technology in various polymers and co-polymer systems, and the use of miniemulsion polymerization for the synthesis of advanced polymer particle morphologies. There have been a large number of texts on emulsion and other forms of polymerization methods, but miniemulsion polymerization, though it provides unique routes for polymer particle synthesis, has been neglected. This edited volume: Details the use of miniemulsion polymerization in encapsulation, core shell functional particles, nitroxide mediated polymerization, atom transfer radical polymerization or radical addition fragmentation chain transfer polymerization, to generate advanced polymer nanoparticles or organic-inorganic composite particles Examines the wide spectrum of commercial possibilities of miniemulsion polymerization Provides both introductory material as well as deep insights into the synthesis of polymer particles
AbstractList Explains miniemulsion technology and techniques and why they have many distinct advantages over the conventional emulsion polymerization technology Miniemulsion Polymerization Technology comprises 10 papers by many of the world's experts on the subject. It summarizes the recent advances in miniemulsion polymerization technology including the advances on the selection of surfactants and co-surfactants, the expansion of miniemulsion technology in various polymers and co-polymer systems, and the use of miniemulsion polymerization for the synthesis of advanced polymer particle morphologies. There have been a large number of texts on emulsion and other forms of polymerization methods, but miniemulsion polymerization, though it provides unique routes for polymer particle synthesis, has been neglected. This edited volume: Details the use of miniemulsion polymerization in encapsulation, core shell functional particles, nitroxide mediated polymerization, atom transfer radical polymerization or radical addition fragmentation chain transfer polymerization, to generate advanced polymer nanoparticles or organic-inorganic composite particles Examines the wide spectrum of commercial possibilities of miniemulsion polymerization Provides both introductory material as well as deep insights into the synthesis of polymer particles
Author Mittal, Vikas
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ISBN 9780470625965
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Notes Includes bibliographical references and index
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Snippet Explains miniemulsion technology and techniques and why they have many distinct advantages over the conventional emulsion polymerization technology...
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SubjectTerms Emulsion polymerization
Microencapsulation
Nanoparticles
TableOfContents 8.1 Introduction -- 8.2 General -- 8.3 Kinetic Studies -- 8.4 Traditional and Nonconventional Inverse Latexes -- 8.4.1 Water Soluble Monomers -- 8.4.2 Hydrophobic Monomers -- 8.5 Controlled Radical Miniemulsion Polymerization -- 8.6 Amphiphilic and Associating Copolymers -- 8.7 Conclusion -- 8.8 Acknowledgements -- Abbreviations -- References -- 9 Double Miniemulsion Preparation for Hybrid Latexes -- 9.1 Introduction -- 9.2 Hybrids via Mini-Emulsion Polymerization -- 9.3 Double-Miniemulsion Formation -- 9.4 Stability -- 9.5 Characterization -- 9.6 Applications -- 9.6.1 Effects of Reaction Conditions -- 9.6.1.1 Initiator Dosage -- 9.6.1.2 MMA Monomer Concentration -- 9.6.2 Rheological Properties of Magnetic Emulsion -- 9.6.2.1 Viscosity Versus Time -- 9.6.2.2 Viscosity with/without Magnetic Field -- 9.6.2.3 Applications of Magnetic Polymer Microspheres -- 9.7 Summary -- 9.8 Acknowledgments -- References -- 10 Surfactant Effect in Miniemulsion Polymerization for Biodegradable Latexes -- 10.1 Introduction -- 10.2 Miniemulsion Polymerization of Biodegradable Latexes -- 10.3 Mechanisms of Surfactant Protection of Colloidal Dispersions -- 10.3.1 General Behavior of a Surfactant Molecule at the Interface -- 10.3.2 Mechanism 1: Lowering the Interfacial Tension -- 10.3.3 Mechanism 2: Electrostatic Stabilization -- 10.3.4 Mechanism 3: Steric Stabilization -- 10.4 Effect of Surfactants on Miniemulsion Polymerization -- 10.4.1 Effect of Surfactant Type on the Particle Size and Latex Yield -- 10.4.2 Effect of Surfactant Concentration on Particle Size and Latex Yield -- 10.4.3 Effect of Surfactant on the Stability -- 10.5 Final Remarks -- References -- Index
4.3.2 Miniemulsion Polymerization with Surface-Modified Silica Nanoparticles -- 4.3.3 Miniemulsion Polymerization with Locally Surface-Modified Silica Nanoparticles -- 4.4 Encapsulation of Magnetite Nanoparticles -- 4.4.1 Encapsulation of Magnetite by a Single Miniemulsion Polymerization Process -- 4.4.2 Encapsulation of Magnetite by a Double Miniemulsion Polymerization Process -- 4.5 Conclusions and Future Perspectives -- 4.6 Acknowledgements -- References -- 5 Polymeric Nanocapsules by Interfacial Miniemulsion Polymerization -- 5.1 Introduction -- 5.2 Organic Nanocapsules by Interfacial Miniemulsion Polymerization -- 5.2.1 Thermodynamic Prediction for the Morphology of Organic Nanocapsules -- 5.2.2 Particles Morphology of the System without Added NIPAM and DVB -- 5.2.3 Particles Morphology of the System with DVB -- 5.2.4 Particle Morphology of the System with Added NIPAM and DVB -- 5.2.5 Particle Size and Size Distribution in the Process of Polymerization -- 5.2.6 Mechanism for the Formation of Organic Nanocapsules through Interfacial Miniemulsion Polymerization -- 5.2.7 Influences on the Formation of Organic Nanocapsules through Interfacial Miniemulsion Polymerization -- 5.3 Organic-Inorganic Hybrid Nanocapsules by Interfacial Miniemulsion Polymerization -- 5.3.1 Thermodynamic Analysis and Morphological Prediction -- 5.3.2 Synthesis of Organic-Inorganic Hybrid Nanocapsules under Neutral Conditions -- 5.3.3 Synthesis of Organic-Inorganic Hybrid Nanocapsules under Acidic or Basic Conditions -- 5.3.4 Mechanism Analysis of Organic-Inorganic Hybrid Nanocapsules Formation -- 5.4 Conclusions -- References -- 6 Miniemulsion Polymerization of Vegetable Oil Macromonomers -- 6.1 Introduction and Background -- 6.2 Emulsion Polymerization of Alkyds and Vegetable Oils -- 6.3 (Meth)acrylated Vegetable Oil Derivatives -- 6.4 Vegetable Oil Macromonomers
Intro -- Miniemulsion Polymerization Technology -- Contents -- Preface -- 1 Miniemulsion Polymerization: An Overview -- 1.1 Introduction to Polymerization Techniques -- 1.2 Emulsion and Miniemulsion Polymerization -- 1.3 Properties of Miniemulsion Polymerization -- 1.4 Controlled Miniemulsion Polymerization -- References -- 2 Multi-Functional Stabilizers in Miniemulsion Polymerization -- 2.1 Introduction -- 2.2 Stability of Initial Monomer Droplets -- 2.3 Stabilizers and Polymerization Processes -- 2.3.1 Mass-Transfer Processes -- 2.3.2 Reactive Stabilizers -- 2.4 Conclusion -- References -- 3 Structured Copolymer Particles by Miniemulsion Polymerization -- 3.1 Introduction -- 3.2 Styrene-Dodecyl Methacrylate/Stearyl Methacrylate -- 3.3 n-Butyl Methacrylate-Crosslinking Monomers -- 3.4 Vinyl Acetate-Butyl Acrylate -- 3.5 Butyl Acrylate-(2-Methacryloxy)ethyl)trimethyl Ammonium Chloride -- 3.6 Butyl Acrylate-Methyl Methacrylate-Vinyl Acetate -- 3.7 Styrene-Acrylic Acid or 2-Aminoethyl Methacrylate Hydrochloride (AEMH) -- 3.8 Styrene-Butyl Acrylate -- 3.9 Styrene-Butadiene Rubber -- 3.10 Fluoroacrylate-LaurylMethylacrylate-Methyl Methacrylate -- 3.11 Polyurethane-Block-Polystyrene -- 3.12 Alkyd-Acrylic -- 3.13 Oil-Acrylate -- 3.14 Urethane-Acrylic -- References -- 4 Encapsulation of Inorganic Nanoparticles by Miniemulsion Polymerization -- 4.1 Introduction -- 4.2 Miniemulsion Polymerization in the Presence of Inorganic Nanoparticles -- 4.2.1 Hydrophobization of Inorganic Nanoparticles -- 4.2.2 Dispersion of Hydrophobized Inorganic Nanoparticles in Monomer Phase -- 4.2.3 Miniemulsification of the Lipophilic Dispersion in Water -- 4.2.4 Polymerization of Droplets -- 4.3 Encapsulation of Silica Nanoparticles -- 4.3.1 Miniemulsion Polymerization with Hydrophilic Silica Nanoparticles
6.5 The Potential for Emulsion of Model Saturated Monomers -- 6.6 Nucleation Mechanisms -- 6.7 Design of Thermosetting Latex Polymers -- 6.8 Classifying Monomer Solubility for Macro and Miniemulsion Polymerization -- 6.9 Soybean Acrylated Monomer Synthesis -- 6.10 Miniemulsion Polymerization -- 6.11 Conclusions -- References -- 7 Controlled/Living Radical Polymerization in Aqueous Miniemulsion -- 7.1 Introduction -- 7.2 Controlled/Living Radical Polymerization in Bulk/Solution: General Considerations -- 7.2.1 CLRP Based on Reversible Termination -- 7.2.1.1 Nitroxide-Mediated Polymerization (NMP) -- 7.2.1.2 Atom Transfer Radical Polymerization (ATRP) -- 7.2.2 CLRP Based on Degenerative Transfer -- 7.2.2.1 Reversible Addition-Fragmentation Chain Transfer (RAFT) -- 7.2.2.2 Iodine Transfer Polymerization (ITP) -- 7.3 Nitroxide-Mediated Miniemulsion Polymerization -- 7.3.1 Oil-Soluble Bicomponent Initiating System -- 7.3.2 Water-Soluble Bicomponent Initiating System -- 7.3.3 Oil-Soluble Monocomponent Initiating System -- 7.3.4 Water-Soluble Monocomponent Initiating System -- 7.4 Atom Transfer Radical Miniemulsion Polymerization -- 7.4.1 Direct ATRP -- 7.4.2 Reverse ATRP -- 7.4.3 Simultaneous Reverse and Normal Initiation (SR&amp -- NI) ATRP -- 7.4.4 Activators Generated by Electron Transfer (AGET) ATRP -- 7.5 Reversible Addition-Fragmentation Chain Transfer Miniemulsion Polymerization -- 7.5.1 Key-Steps for the Success of RAFT Miniemulsion Polymerization -- 7.5.1.1 Inhibition and Retardation -- 7.5.1.2 Colloidal Instability -- 7.5.1.3 Livingness and Controlled Polymerization -- 7.5.2 RAFT Miniemulsion Polymerization of Vinyl Acetate -- 7.5.3 Nanocapsules Synthesized by RAFT Miniemulsion Polymerization -- 7.6 Iodine Transfer Polymerization in Miniemulsion -- 7.7 Conclusion -- References -- 8 Inverse Miniemulsion Polymerization of Unsaturated Monomers
Title Miniemulsion polymerization technology
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